Microstructure and surface texture driven improvement in in-vitro response of laser surface processed AZ31B magnesium alloy

The present work explored effects of laser surface melting on microstructure and surface topography evolution in AZ31B magnesium alloy. Thermokinetic effects experienced by the material during laser surface melting were simulated using a multiphysics finite element model. Microstructure and phase ev...

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Main Authors: Tso-Chang Wu, Sameehan S. Joshi, Yee-Hsien Ho, Mangesh V. Pantawane, Subhasis Sinha, Narendra B. Dahotre
Format: Article
Language:English
Published: KeAi Communications Co., Ltd. 2021-07-01
Series:Journal of Magnesium and Alloys
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2213956720302280
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author Tso-Chang Wu
Sameehan S. Joshi
Yee-Hsien Ho
Mangesh V. Pantawane
Subhasis Sinha
Narendra B. Dahotre
author_facet Tso-Chang Wu
Sameehan S. Joshi
Yee-Hsien Ho
Mangesh V. Pantawane
Subhasis Sinha
Narendra B. Dahotre
author_sort Tso-Chang Wu
collection DOAJ
description The present work explored effects of laser surface melting on microstructure and surface topography evolution in AZ31B magnesium alloy. Thermokinetic effects experienced by the material during laser surface melting were simulated using a multiphysics finite element model. Microstructure and phase evolution were examined using scanning electron microscopy, X-ray diffraction, and electron back scatter diffraction. Surface topography was evaluated using white light interferometry. The interaction of surface melted samples with simulated body fluid was monitored by contact angle measurements and immersion studies up to 7 days. Laser surface melting led to formation of a refined microstructure with predominantly basal crystallographic texture. Concurrently, the amount of β phase (Mg17Al12) increased with an increase in the laser fluence. β phase preferentially decorated the cell boundaries. In terms of topography, the surface became progressively rougher with an increase in laser fluence. As a result, upon immersion in simulated body fluid, the laser surface melted samples showed an improved wettability, corrosion resistance, and precipitation of mineral having composition closer to the hydroxyapatite bone mineral compared to the untreated sample.
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spelling doaj.art-ec97117d1ecc4ef784a8484a607fcc022024-04-16T22:16:00ZengKeAi Communications Co., Ltd.Journal of Magnesium and Alloys2213-95672021-07-019414061418Microstructure and surface texture driven improvement in in-vitro response of laser surface processed AZ31B magnesium alloyTso-Chang Wu0Sameehan S. Joshi1Yee-Hsien Ho2Mangesh V. Pantawane3Subhasis Sinha4Narendra B. Dahotre5Department of Materials Science and Engineering, University of North Texas, 3940 N Elm St, Denton, TX 76207, USADepartment of Materials Science and Engineering, University of North Texas, 3940 N Elm St, Denton, TX 76207, USA; Center for Agile and Adaptive Additive Manufacturing, University of North Texas, 3940 N Elm St, Denton, TX 76207, USADepartment of Materials Science and Engineering, University of North Texas, 3940 N Elm St, Denton, TX 76207, USA; Center for Agile and Adaptive Additive Manufacturing, University of North Texas, 3940 N Elm St, Denton, TX 76207, USADepartment of Materials Science and Engineering, University of North Texas, 3940 N Elm St, Denton, TX 76207, USA; Center for Agile and Adaptive Additive Manufacturing, University of North Texas, 3940 N Elm St, Denton, TX 76207, USADepartment of Materials Science and Engineering, University of North Texas, 3940 N Elm St, Denton, TX 76207, USA; Department of Metallurgical Engineering, Indian Institute of Technology (BHU), Varanasi, Uttar Pradesh 221005, IndiaCorresponding author at: Department of Materials Science and Engineering, University of North Texas, 3940 N Elm St, Denton, TX 76207, USA.; Department of Materials Science and Engineering, University of North Texas, 3940 N Elm St, Denton, TX 76207, USA; Center for Agile and Adaptive Additive Manufacturing, University of North Texas, 3940 N Elm St, Denton, TX 76207, USAThe present work explored effects of laser surface melting on microstructure and surface topography evolution in AZ31B magnesium alloy. Thermokinetic effects experienced by the material during laser surface melting were simulated using a multiphysics finite element model. Microstructure and phase evolution were examined using scanning electron microscopy, X-ray diffraction, and electron back scatter diffraction. Surface topography was evaluated using white light interferometry. The interaction of surface melted samples with simulated body fluid was monitored by contact angle measurements and immersion studies up to 7 days. Laser surface melting led to formation of a refined microstructure with predominantly basal crystallographic texture. Concurrently, the amount of β phase (Mg17Al12) increased with an increase in the laser fluence. β phase preferentially decorated the cell boundaries. In terms of topography, the surface became progressively rougher with an increase in laser fluence. As a result, upon immersion in simulated body fluid, the laser surface melted samples showed an improved wettability, corrosion resistance, and precipitation of mineral having composition closer to the hydroxyapatite bone mineral compared to the untreated sample.http://www.sciencedirect.com/science/article/pii/S2213956720302280Laser surface meltingMagnesium alloyLaser surface engineeringBiomineralization
spellingShingle Tso-Chang Wu
Sameehan S. Joshi
Yee-Hsien Ho
Mangesh V. Pantawane
Subhasis Sinha
Narendra B. Dahotre
Microstructure and surface texture driven improvement in in-vitro response of laser surface processed AZ31B magnesium alloy
Journal of Magnesium and Alloys
Laser surface melting
Magnesium alloy
Laser surface engineering
Biomineralization
title Microstructure and surface texture driven improvement in in-vitro response of laser surface processed AZ31B magnesium alloy
title_full Microstructure and surface texture driven improvement in in-vitro response of laser surface processed AZ31B magnesium alloy
title_fullStr Microstructure and surface texture driven improvement in in-vitro response of laser surface processed AZ31B magnesium alloy
title_full_unstemmed Microstructure and surface texture driven improvement in in-vitro response of laser surface processed AZ31B magnesium alloy
title_short Microstructure and surface texture driven improvement in in-vitro response of laser surface processed AZ31B magnesium alloy
title_sort microstructure and surface texture driven improvement in in vitro response of laser surface processed az31b magnesium alloy
topic Laser surface melting
Magnesium alloy
Laser surface engineering
Biomineralization
url http://www.sciencedirect.com/science/article/pii/S2213956720302280
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