Preparation and characterization of silver nanoparticles using aniline
UV–Vis spectroscopy, transmission electron microscopy (TEM) and selected area electron diffraction (SAED) have been employed to characterize silver nanoparticles (AgNPs) using aniline and silver nitrate as reductant and oxidant, respectively. A broad surface resonance plasmon (SRP) band appears at 4...
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Elsevier
2017-05-01
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Series: | Arabian Journal of Chemistry |
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Online Access: | http://www.sciencedirect.com/science/article/pii/S1878535213001214 |
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author | Zaheer Khan Javed Ijaz Hussain Athar Adil Hashmi Shaeel Ahmed AL-Thabaiti |
author_facet | Zaheer Khan Javed Ijaz Hussain Athar Adil Hashmi Shaeel Ahmed AL-Thabaiti |
author_sort | Zaheer Khan |
collection | DOAJ |
description | UV–Vis spectroscopy, transmission electron microscopy (TEM) and selected area electron diffraction (SAED) have been employed to characterize silver nanoparticles (AgNPs) using aniline and silver nitrate as reductant and oxidant, respectively. A broad surface resonance plasmon (SRP) band appears at 400 nm, indicating that the AgNPs are spherical. The TEM images show that AgNPs aggregated in an unsymmetrical manner, leading to the formation of beautiful silver nanocrystals. Aniline adsorbed onto the surface of Ag-nanocrystals through electrostatic, van der Walls forces and hydrogen bonding. Cetyltrimethylammonium bromide (CTAB) acted as a stabilizer and/or capping agent. |
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format | Article |
id | doaj.art-ecedf56343e445a9b04bfb17940d9233 |
institution | Directory Open Access Journal |
issn | 1878-5352 |
language | English |
last_indexed | 2024-12-22T20:56:53Z |
publishDate | 2017-05-01 |
publisher | Elsevier |
record_format | Article |
series | Arabian Journal of Chemistry |
spelling | doaj.art-ecedf56343e445a9b04bfb17940d92332022-12-21T18:12:56ZengElsevierArabian Journal of Chemistry1878-53522017-05-0110S2S1506S151110.1016/j.arabjc.2013.05.001Preparation and characterization of silver nanoparticles using anilineZaheer Khan0Javed Ijaz Hussain1Athar Adil Hashmi2Shaeel Ahmed AL-Thabaiti3Department of Chemistry, Jamia Millia Islamia (Central University), New Delhi 110 025, IndiaDepartment of Chemistry, Jamia Millia Islamia (Central University), New Delhi 110 025, IndiaDepartment of Chemistry, Jamia Millia Islamia (Central University), New Delhi 110 025, IndiaDepartment of Chemistry, Faculty of Science, King Abdulaziz University, P.O. Box 80203, Jeddah 21413, Saudi ArabiaUV–Vis spectroscopy, transmission electron microscopy (TEM) and selected area electron diffraction (SAED) have been employed to characterize silver nanoparticles (AgNPs) using aniline and silver nitrate as reductant and oxidant, respectively. A broad surface resonance plasmon (SRP) band appears at 400 nm, indicating that the AgNPs are spherical. The TEM images show that AgNPs aggregated in an unsymmetrical manner, leading to the formation of beautiful silver nanocrystals. Aniline adsorbed onto the surface of Ag-nanocrystals through electrostatic, van der Walls forces and hydrogen bonding. Cetyltrimethylammonium bromide (CTAB) acted as a stabilizer and/or capping agent.http://www.sciencedirect.com/science/article/pii/S1878535213001214MorphologyAg-nanoparticlesOxidationAnilineCTAB |
spellingShingle | Zaheer Khan Javed Ijaz Hussain Athar Adil Hashmi Shaeel Ahmed AL-Thabaiti Preparation and characterization of silver nanoparticles using aniline Arabian Journal of Chemistry Morphology Ag-nanoparticles Oxidation Aniline CTAB |
title | Preparation and characterization of silver nanoparticles using aniline |
title_full | Preparation and characterization of silver nanoparticles using aniline |
title_fullStr | Preparation and characterization of silver nanoparticles using aniline |
title_full_unstemmed | Preparation and characterization of silver nanoparticles using aniline |
title_short | Preparation and characterization of silver nanoparticles using aniline |
title_sort | preparation and characterization of silver nanoparticles using aniline |
topic | Morphology Ag-nanoparticles Oxidation Aniline CTAB |
url | http://www.sciencedirect.com/science/article/pii/S1878535213001214 |
work_keys_str_mv | AT zaheerkhan preparationandcharacterizationofsilvernanoparticlesusinganiline AT javedijazhussain preparationandcharacterizationofsilvernanoparticlesusinganiline AT atharadilhashmi preparationandcharacterizationofsilvernanoparticlesusinganiline AT shaeelahmedalthabaiti preparationandcharacterizationofsilvernanoparticlesusinganiline |