Characterization of an Extruded Mg-Dy-Nd Alloy during Stress Corrosion with C-Ring Tests

This study focuses on the characterization of the failure behavior of an extruded Mg10Dy1Nd alloy during stress corrosion. The microstructure, hardness, strength and corrosion behavior of binary alloys Mg10Dy and Mg1Nd are compared to those of the ternary alloy system. The ternary alloy Mg-Dy-Nd tha...

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Main Authors: Petra Maier, Benjamin Clausius, Jens Wicke, Norbert Hort
Format: Article
Language:English
Published: MDPI AG 2020-04-01
Series:Metals
Subjects:
Online Access:https://www.mdpi.com/2075-4701/10/5/584
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author Petra Maier
Benjamin Clausius
Jens Wicke
Norbert Hort
author_facet Petra Maier
Benjamin Clausius
Jens Wicke
Norbert Hort
author_sort Petra Maier
collection DOAJ
description This study focuses on the characterization of the failure behavior of an extruded Mg10Dy1Nd alloy during stress corrosion. The microstructure, hardness, strength and corrosion behavior of binary alloys Mg10Dy and Mg1Nd are compared to those of the ternary alloy system. The ternary alloy Mg-Dy-Nd that is not fully recrystallized has the highest hardness but lacks ductility. The investigated alloys twin during plastic deformation. Static C-ring tests in Ringer solution were used to evaluate the stress corrosion properties, and stress corrosion could not be found. None of the alloys failed by fracturing, but corrosion pits formed to various extents. These corrosion pits were elliptical in shape and located below the surface. Some of the pits reduced the remaining wall thickness significantly, but the stress increased by the notch effect did not lead to crack initiation. Furthermore, the C-ring specimen was subjected to compressive loading until fracture. Whereas the Mg1Nd alloy showed ductile behavior, the alloys containing Dy fractured on the tensile side. The crack initiation and growth were mainly influenced by the twin boundaries. The Mg10Dy1Nd alloy had an inhomogeneous microstructure and low ductility, which resulted in a lower fracture toughness than that of the Mg10Dy alloy. There were features that indicate hydrogen-assisted fracture. Although adding Nd decreased the fracture toughness, it reduced the grain size and had a positive influence on the corrosion rate during immersion testing.
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spelling doaj.art-ed630efc717a431ca577b99240c92a5a2023-11-19T23:03:18ZengMDPI AGMetals2075-47012020-04-0110558410.3390/met10050584Characterization of an Extruded Mg-Dy-Nd Alloy during Stress Corrosion with C-Ring TestsPetra Maier0Benjamin Clausius1Jens Wicke2Norbert Hort3School of Mechanical Engineering, University of Applied Sciences Stralsund, 18435 Stralsund, GermanySchool of Mechanical Engineering, University of Applied Sciences Stralsund, 18435 Stralsund, GermanySchool of Mechanical Engineering, University of Applied Sciences Stralsund, 18435 Stralsund, GermanyHelmholtz-Zentrum Geesthacht, Magnesium Innovation Center, 21502 Geesthacht, GermanyThis study focuses on the characterization of the failure behavior of an extruded Mg10Dy1Nd alloy during stress corrosion. The microstructure, hardness, strength and corrosion behavior of binary alloys Mg10Dy and Mg1Nd are compared to those of the ternary alloy system. The ternary alloy Mg-Dy-Nd that is not fully recrystallized has the highest hardness but lacks ductility. The investigated alloys twin during plastic deformation. Static C-ring tests in Ringer solution were used to evaluate the stress corrosion properties, and stress corrosion could not be found. None of the alloys failed by fracturing, but corrosion pits formed to various extents. These corrosion pits were elliptical in shape and located below the surface. Some of the pits reduced the remaining wall thickness significantly, but the stress increased by the notch effect did not lead to crack initiation. Furthermore, the C-ring specimen was subjected to compressive loading until fracture. Whereas the Mg1Nd alloy showed ductile behavior, the alloys containing Dy fractured on the tensile side. The crack initiation and growth were mainly influenced by the twin boundaries. The Mg10Dy1Nd alloy had an inhomogeneous microstructure and low ductility, which resulted in a lower fracture toughness than that of the Mg10Dy alloy. There were features that indicate hydrogen-assisted fracture. Although adding Nd decreased the fracture toughness, it reduced the grain size and had a positive influence on the corrosion rate during immersion testing.https://www.mdpi.com/2075-4701/10/5/584magnesiumMg-Dy-NdC-ring teststress corrosioncorrosion morphology
spellingShingle Petra Maier
Benjamin Clausius
Jens Wicke
Norbert Hort
Characterization of an Extruded Mg-Dy-Nd Alloy during Stress Corrosion with C-Ring Tests
Metals
magnesium
Mg-Dy-Nd
C-ring test
stress corrosion
corrosion morphology
title Characterization of an Extruded Mg-Dy-Nd Alloy during Stress Corrosion with C-Ring Tests
title_full Characterization of an Extruded Mg-Dy-Nd Alloy during Stress Corrosion with C-Ring Tests
title_fullStr Characterization of an Extruded Mg-Dy-Nd Alloy during Stress Corrosion with C-Ring Tests
title_full_unstemmed Characterization of an Extruded Mg-Dy-Nd Alloy during Stress Corrosion with C-Ring Tests
title_short Characterization of an Extruded Mg-Dy-Nd Alloy during Stress Corrosion with C-Ring Tests
title_sort characterization of an extruded mg dy nd alloy during stress corrosion with c ring tests
topic magnesium
Mg-Dy-Nd
C-ring test
stress corrosion
corrosion morphology
url https://www.mdpi.com/2075-4701/10/5/584
work_keys_str_mv AT petramaier characterizationofanextrudedmgdyndalloyduringstresscorrosionwithcringtests
AT benjaminclausius characterizationofanextrudedmgdyndalloyduringstresscorrosionwithcringtests
AT jenswicke characterizationofanextrudedmgdyndalloyduringstresscorrosionwithcringtests
AT norberthort characterizationofanextrudedmgdyndalloyduringstresscorrosionwithcringtests