Deuterium retention and blistering in tungsten foils

To investigate deuterium retention and the onset of blistering, deuterium was implanted in cold rolled tungsten foils at fluences ranging from 3 ×1020 to 3 ×1022D/m2. Ion energies were 300eV and 2000eV in order to be below and above the tungsten theoretical damage energy threshold. While energy depe...

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Main Authors: C.N. Taylor, M. Shimada, B.J. Merrill
Format: Article
Language:English
Published: Elsevier 2017-08-01
Series:Nuclear Materials and Energy
Online Access:http://www.sciencedirect.com/science/article/pii/S2352179116301314
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author C.N. Taylor
M. Shimada
B.J. Merrill
author_facet C.N. Taylor
M. Shimada
B.J. Merrill
author_sort C.N. Taylor
collection DOAJ
description To investigate deuterium retention and the onset of blistering, deuterium was implanted in cold rolled tungsten foils at fluences ranging from 3 ×1020 to 3 ×1022D/m2. Ion energies were 300eV and 2000eV in order to be below and above the tungsten theoretical damage energy threshold. While energy dependent phenomena were observed, blistering occurs regardless of ion energy. Both plastically and elastically deformed blisters were found, as manifest in before and after micrographs. The fraction of plastically deformed blisters did not saturate at the fluences used in these studies. However, the size of the largest blister that relaxed during TDS does saturate at ∼7µm. A simple conceptual model is presented, which proposes that the deuterium released from elastically deformed blisters appears at ∼600K in the thermal desorption spectra, which is consistent with large vacancy clusters. Keywords: Tungsten, Deuterium, Retention, Blistering, Thermal desorption spectroscopy
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spelling doaj.art-eec4d7bd1b2048b98ee4e33f63838be92022-12-22T03:52:51ZengElsevierNuclear Materials and Energy2352-17912017-08-0112689693Deuterium retention and blistering in tungsten foilsC.N. Taylor0M. Shimada1B.J. Merrill2Corresponding author.; Fusion Safety Program, Idaho National Laboratory, Idaho Falls, ID 83415, USAFusion Safety Program, Idaho National Laboratory, Idaho Falls, ID 83415, USAFusion Safety Program, Idaho National Laboratory, Idaho Falls, ID 83415, USATo investigate deuterium retention and the onset of blistering, deuterium was implanted in cold rolled tungsten foils at fluences ranging from 3 ×1020 to 3 ×1022D/m2. Ion energies were 300eV and 2000eV in order to be below and above the tungsten theoretical damage energy threshold. While energy dependent phenomena were observed, blistering occurs regardless of ion energy. Both plastically and elastically deformed blisters were found, as manifest in before and after micrographs. The fraction of plastically deformed blisters did not saturate at the fluences used in these studies. However, the size of the largest blister that relaxed during TDS does saturate at ∼7µm. A simple conceptual model is presented, which proposes that the deuterium released from elastically deformed blisters appears at ∼600K in the thermal desorption spectra, which is consistent with large vacancy clusters. Keywords: Tungsten, Deuterium, Retention, Blistering, Thermal desorption spectroscopyhttp://www.sciencedirect.com/science/article/pii/S2352179116301314
spellingShingle C.N. Taylor
M. Shimada
B.J. Merrill
Deuterium retention and blistering in tungsten foils
Nuclear Materials and Energy
title Deuterium retention and blistering in tungsten foils
title_full Deuterium retention and blistering in tungsten foils
title_fullStr Deuterium retention and blistering in tungsten foils
title_full_unstemmed Deuterium retention and blistering in tungsten foils
title_short Deuterium retention and blistering in tungsten foils
title_sort deuterium retention and blistering in tungsten foils
url http://www.sciencedirect.com/science/article/pii/S2352179116301314
work_keys_str_mv AT cntaylor deuteriumretentionandblisteringintungstenfoils
AT mshimada deuteriumretentionandblisteringintungstenfoils
AT bjmerrill deuteriumretentionandblisteringintungstenfoils