Isolation of Cherry Seed Oil Using Conventional Techniques and Supercritical Fluid Extraction
This study aims to compare the suitability of three extraction techniques (cold pressing, Soxhlet and supercritical fluid extraction (SFE)) to isolate oil from cherry seeds. Oils were examined in terms of extraction yield, fatty acids profile, tocopherols yield and antioxidant activity. Additionally...
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MDPI AG
2022-12-01
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author | Ivana Dimić Branimir Pavlić Slađana Rakita Aleksandra Cvetanović Kljakić Zoran Zeković Nemanja Teslić |
author_facet | Ivana Dimić Branimir Pavlić Slađana Rakita Aleksandra Cvetanović Kljakić Zoran Zeković Nemanja Teslić |
author_sort | Ivana Dimić |
collection | DOAJ |
description | This study aims to compare the suitability of three extraction techniques (cold pressing, Soxhlet and supercritical fluid extraction (SFE)) to isolate oil from cherry seeds. Oils were examined in terms of extraction yield, fatty acids profile, tocopherols yield and antioxidant activity. Additionally, influence of SFE parameters was evaluated using one-factor-at-a-time design with pressure (200–350 bar), temperature (40–70 °C), flow rate (0.2–0.4 kg/h) and particle size (<800 µm and >800 µm). Oil yields ranged from 2.50% to 13.02%, whereas the highest yield was achieved with SFE. Samples were rich in polyunsaturated fatty acids, regardless of the applied extraction technique. The main fatty acids were linoleic (46.32–47.29%), oleic (40.89–41.65%), palmitic (6.56–8.00%) and stearic (2.21–2.30%) acid. Total tocopherols yield was between 16.63 mg/100 g oil and 60.61 mg/100 g oil, and highest yield was achieved with SFE. Among the tocopherols, γ-tocopherol was the most abundant, followed by α-, δ- and β-tocopherol. Antioxidant activity was determined using 1,1-diphenyl-2-picrylhydrazyl (DPPH) and 2,2’-azinobis-(3-ethylbenzothiazoline-6-sulfonic) cation (ABTS) assays, and the results indicated that SFE extracts exhibited better or comparable antioxidant potential compared to traditional techniques. The comparison between modern and conventional extractions for oil recovery demonstrates pros and cons for the possibility of industrial application. |
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publishDate | 2022-12-01 |
publisher | MDPI AG |
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spelling | doaj.art-eed9957712d642ba8623656cf35ab81f2023-11-16T15:21:08ZengMDPI AGFoods2304-81582022-12-011211110.3390/foods12010011Isolation of Cherry Seed Oil Using Conventional Techniques and Supercritical Fluid ExtractionIvana Dimić0Branimir Pavlić1Slađana Rakita2Aleksandra Cvetanović Kljakić3Zoran Zeković4Nemanja Teslić5Faculty of Technology, University of Novi Sad, Blvd. cara Lazara 1, 21000 Novi Sad, SerbiaFaculty of Technology, University of Novi Sad, Blvd. cara Lazara 1, 21000 Novi Sad, SerbiaInstitute of Food Technology, University of Novi Sad, Blvd. cara Lazara 1, 21000 Novi Sad, SerbiaFaculty of Technology, University of Novi Sad, Blvd. cara Lazara 1, 21000 Novi Sad, SerbiaFaculty of Technology, University of Novi Sad, Blvd. cara Lazara 1, 21000 Novi Sad, SerbiaInstitute of Food Technology, University of Novi Sad, Blvd. cara Lazara 1, 21000 Novi Sad, SerbiaThis study aims to compare the suitability of three extraction techniques (cold pressing, Soxhlet and supercritical fluid extraction (SFE)) to isolate oil from cherry seeds. Oils were examined in terms of extraction yield, fatty acids profile, tocopherols yield and antioxidant activity. Additionally, influence of SFE parameters was evaluated using one-factor-at-a-time design with pressure (200–350 bar), temperature (40–70 °C), flow rate (0.2–0.4 kg/h) and particle size (<800 µm and >800 µm). Oil yields ranged from 2.50% to 13.02%, whereas the highest yield was achieved with SFE. Samples were rich in polyunsaturated fatty acids, regardless of the applied extraction technique. The main fatty acids were linoleic (46.32–47.29%), oleic (40.89–41.65%), palmitic (6.56–8.00%) and stearic (2.21–2.30%) acid. Total tocopherols yield was between 16.63 mg/100 g oil and 60.61 mg/100 g oil, and highest yield was achieved with SFE. Among the tocopherols, γ-tocopherol was the most abundant, followed by α-, δ- and β-tocopherol. Antioxidant activity was determined using 1,1-diphenyl-2-picrylhydrazyl (DPPH) and 2,2’-azinobis-(3-ethylbenzothiazoline-6-sulfonic) cation (ABTS) assays, and the results indicated that SFE extracts exhibited better or comparable antioxidant potential compared to traditional techniques. The comparison between modern and conventional extractions for oil recovery demonstrates pros and cons for the possibility of industrial application.https://www.mdpi.com/2304-8158/12/1/11sour cherry seed oil<i>Prunus cerasus</i> L.extraction techniqueschemical compositionantioxidant activity |
spellingShingle | Ivana Dimić Branimir Pavlić Slađana Rakita Aleksandra Cvetanović Kljakić Zoran Zeković Nemanja Teslić Isolation of Cherry Seed Oil Using Conventional Techniques and Supercritical Fluid Extraction Foods sour cherry seed oil <i>Prunus cerasus</i> L. extraction techniques chemical composition antioxidant activity |
title | Isolation of Cherry Seed Oil Using Conventional Techniques and Supercritical Fluid Extraction |
title_full | Isolation of Cherry Seed Oil Using Conventional Techniques and Supercritical Fluid Extraction |
title_fullStr | Isolation of Cherry Seed Oil Using Conventional Techniques and Supercritical Fluid Extraction |
title_full_unstemmed | Isolation of Cherry Seed Oil Using Conventional Techniques and Supercritical Fluid Extraction |
title_short | Isolation of Cherry Seed Oil Using Conventional Techniques and Supercritical Fluid Extraction |
title_sort | isolation of cherry seed oil using conventional techniques and supercritical fluid extraction |
topic | sour cherry seed oil <i>Prunus cerasus</i> L. extraction techniques chemical composition antioxidant activity |
url | https://www.mdpi.com/2304-8158/12/1/11 |
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