X-Shaped Thallium oxide nanostructures as a high performance photocatalyst for degradation of Cephalexin

In this study, we present an approach to synthesize Tl2O3 nanoparticles using a simple co-precipitation method that leads to the formation of X-shaped particles. The sample was characterized by XRD measurements, field emission scanning electron microscopy (FESEM), diffuse reflectance spectroscopy, X...

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Main Authors: Arezo Mohammadkhani, Azar Bagheri GH, Saeed Rayati
Format: Article
Language:English
Published: Iranian Research Organization for Science and Technology (IROST) 2019-08-01
Series:Journal of Particle Science and Technology
Subjects:
Online Access:https://jpst.irost.ir/article_885_5f7bdb4e2fc790c1cc6c76e809721af4.pdf
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author Arezo Mohammadkhani
Azar Bagheri GH
Saeed Rayati
author_facet Arezo Mohammadkhani
Azar Bagheri GH
Saeed Rayati
author_sort Arezo Mohammadkhani
collection DOAJ
description In this study, we present an approach to synthesize Tl2O3 nanoparticles using a simple co-precipitation method that leads to the formation of X-shaped particles. The sample was characterized by XRD measurements, field emission scanning electron microscopy (FESEM), diffuse reflectance spectroscopy, X-ray photoelectron spectroscopy (XPS), Fourier transform infrared (FT-IR), and ultraviolet-visible (UV-VIS). The absorption spectrum of the sample showed that the optical band gap was 3.5 eV. The prepared photocatalyst was used in the photocatalytic degradation of Cephalexin (CPX) using irradiation, and the optimum parameters that were obtained were 0.2 g.L-1 of the photocatalyst at pH 5.5 and an irradiation time of 15 minutes.
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spelling doaj.art-ef69e23a6f884554bfc43d1b41c768d02023-05-10T08:25:50ZengIranian Research Organization for Science and Technology (IROST)Journal of Particle Science and Technology2423-40872423-40792019-08-015211712210.22104/jpst.2019.3610.1149885X-Shaped Thallium oxide nanostructures as a high performance photocatalyst for degradation of CephalexinArezo Mohammadkhani0Azar Bagheri GH1Saeed Rayati2Department of Chemistry, Central Tehran Branch, Islamic Azad University, Tehran, IranDepartment of Chemistry, Central Tehran Branch, Islamic Azad University, Tehran, IranDepartment of Chemistry, K. N. Toosi University of Technology, Tehran, IranIn this study, we present an approach to synthesize Tl2O3 nanoparticles using a simple co-precipitation method that leads to the formation of X-shaped particles. The sample was characterized by XRD measurements, field emission scanning electron microscopy (FESEM), diffuse reflectance spectroscopy, X-ray photoelectron spectroscopy (XPS), Fourier transform infrared (FT-IR), and ultraviolet-visible (UV-VIS). The absorption spectrum of the sample showed that the optical band gap was 3.5 eV. The prepared photocatalyst was used in the photocatalytic degradation of Cephalexin (CPX) using irradiation, and the optimum parameters that were obtained were 0.2 g.L-1 of the photocatalyst at pH 5.5 and an irradiation time of 15 minutes.https://jpst.irost.ir/article_885_5f7bdb4e2fc790c1cc6c76e809721af4.pdftl2o3cephalexinphotocatalitic activityband gapco-precipitation method
spellingShingle Arezo Mohammadkhani
Azar Bagheri GH
Saeed Rayati
X-Shaped Thallium oxide nanostructures as a high performance photocatalyst for degradation of Cephalexin
Journal of Particle Science and Technology
tl2o3
cephalexin
photocatalitic activity
band gap
co-precipitation method
title X-Shaped Thallium oxide nanostructures as a high performance photocatalyst for degradation of Cephalexin
title_full X-Shaped Thallium oxide nanostructures as a high performance photocatalyst for degradation of Cephalexin
title_fullStr X-Shaped Thallium oxide nanostructures as a high performance photocatalyst for degradation of Cephalexin
title_full_unstemmed X-Shaped Thallium oxide nanostructures as a high performance photocatalyst for degradation of Cephalexin
title_short X-Shaped Thallium oxide nanostructures as a high performance photocatalyst for degradation of Cephalexin
title_sort x shaped thallium oxide nanostructures as a high performance photocatalyst for degradation of cephalexin
topic tl2o3
cephalexin
photocatalitic activity
band gap
co-precipitation method
url https://jpst.irost.ir/article_885_5f7bdb4e2fc790c1cc6c76e809721af4.pdf
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AT azarbagherigh xshapedthalliumoxidenanostructuresasahighperformancephotocatalystfordegradationofcephalexin
AT saeedrayati xshapedthalliumoxidenanostructuresasahighperformancephotocatalystfordegradationofcephalexin