Crystal structures of 2-[(4,6-diaminopyrimidin-2-yl)sulfanyl]-N-(3-nitrophenyl)acetamide monohydrate and N-(2-chlorophenyl)-2-[(4,6-diaminopyrimidin-2-yl)sulfanyl]acetamide

Crystal structures of 2-[(4,6-diaminopyrimidin-2-yl)sulfanyl]-N-(3-nitrophenyl)acetamide monohydrate and N-(2-chlorophenyl)-2-[(4,6-diaminopyrimidin-2-yl)sulfanyl]acetamide

The title compounds, C12H12N6O3S·H2O, (I), and C12H12ClN5OS, (II), are 2-[(4,6-diaminopyrimidin-2-yl)sulfanyl]acetamides. Compound (I) crystallized as a monohydrate. In both compounds, the molecules have a folded conformation, with the pyrimidine ring being inclined to the benzene ring by 56.18 (6)°...

Full description

Bibliographic Details
Main Authors:	S. Subasri, Ajay Kumar Timiri, Nayan Sinha Barji, Venkatesan Jayaprakash, Viswanathan Vijayan, Devadasan Velmurugan
Format:	Article
Language:	English
Published:	International Union of Crystallography 2016-08-01
Series:	Acta Crystallographica Section E: Crystallographic Communications
Subjects:	crystal structure acetamides intramolecular N—H...O and N—H...Cl hydrogen bonds network framework
Online Access:	http://scripts.iucr.org/cgi-bin/paper?S2056989016011658

Similar Items

2-[(4,6-Diaminopyrimidin-2-yl)sulfanyl]-N-(2-methylphenyl)acetamide
by: S. Subasri, et al.
Published: (2014-08-01)

Crystal structures of 2-[(4,6-diaminopyrimidin-2-yl)sulfanyl]-N-(naphthalen-1-yl)acetamide and 2-[(4,6-diaminopyrimidin-2-yl)sulfanyl]-N-(4-fluorophenyl)acetamide
by: S. Subasri, et al.
Published: (2017-02-01)

2-[(4,6-Diaminopyrimidin-2-yl)sulfanyl]-N-(4-methoxyphenyl)acetamide
by: Manisha Choudhury, et al.
Published: (2018-04-01)

2-Chloro-N-[4-(4-chlorophenyl)-1,3-thiazol-2-yl]acetamide
by: K. Saravanan, et al.
Published: (2016-06-01)

Bis(4,6-diaminopyrimidin-2-yl) disulfide dimethyl sufoxide disolvate
by: Maria Gdaniec, et al.
Published: (2008-09-01)

Crystal structures of two C,N-disubstituted acetamides: 2-(4-chlorophenyl)-N-(2-iodophenyl)acetamide and 2-(4-chlorophenyl)-N-(pyrazin-2-yl)acetamide
by: Badiadka Narayana, et al.
Published: (2016-09-01)

N-(4,6-Dimethoxypyrimidin-2-yl)-2-(3-methylphenyl)acetamide
by: A. S. Praveen, et al.
Published: (2012-01-01)

Design and synthesis of some novel 2-(3-methyl-2-oxoquinoxalin-1(2H)-yl)-N-(4-(substituted)phenyl)acetamide derivatives for biological evaluation as anticonvulsant agents
by: Mohamed-Kamal Ibrahim, et al.
Published: (2013-06-01)

2-{[5-(Diphenylmethyl)-1,3,4-oxadiazol-2-yl]sulfanyl}-N-(pyrazin-2-yl)acetamide
by: Balladka Kunhanna Sarojini, et al.
Published: (2013-05-01)

N-[3-Methyl-1-phenyl-1-(1H-tetrazol-1-yl)butan-2-yl]acetamide
by: Selvaraj Geetha, et al.
Published: (2016-11-01)

<i>N</i>-[3-(Chloromethyl)-1,2-benzisoxazol-5-yl]acetamide
by: Evgeniy N. Khodot, et al.
Published: (2022-06-01)

2-[(2-Aminophenyl)sulfanyl]-N-(4-methoxyphenyl)acetamide
by: Shahzad Murtaza, et al.
Published: (2012-06-01)

Crystal structure of N-[4-amino-5-cyano-6-(methylsulfanyl)pyridin-2-yl]acetamide hemihydrate
by: Mehmet Akkurt, et al.
Published: (2015-03-01)

Effect of 2-chloro-N-(4-fluoro-3-nitrophenyl)acetamide in combination with antibacterial drugs against Klebsiella pneumoniae
by: LAÍSA V. CORDEIRO, et al.
Published: (2023-03-01)

2-Azido-N-(4-methylphenyl)acetamide
by: Mohcine Missioui, et al.
Published: (2022-07-01)

N-(4-Methoxy-2-nitrophenyl)-2-(3-methyl-2-oxo-1,2-dihydroquinoxalin-1-yl)acetamide
by: Mohcine Missioui, et al.
Published: (2023-03-01)

Thermochemistry, Bond Energies and Internal Rotor Potentials of Acetic Acid Hydrazide, Acetamide, <i>N</i>-Methyl Acetamide (NMA) and Radicals
by: Sumit Charaya, et al.
Published: (2021-03-01)

Convergent synthesis of new N -substituted 2-{[5-(1H -indol-3-ylmethyl)-1,3,4-oxadiazol-2-yl]sulfanyl}acetamides as suitable therapeutic agents
by: Kaniz Rubab, et al.
Published: (2015-12-01)

Importance of N-3-(methylthiopropyl) acetamide and 3-methylthiopropionic acid in wines
by: A. Anocibar Beloqui, et al.
Published: (1995-03-01)

Scientific Opinion of Flavouring Group Evaluation 411 (FGE.411): 2‐(4‐methylphenoxy)‐N‐(1H‐pyrazol‐3‐yl)‐N‐(thiophen‐2‐ylmethyl)acetamide from chemical group 30 (miscellaneous substances)
by: EFSA Panel on Food Additives and Flavourings (FAF), et al.
Published: (2018-10-01)

2-[(5-Amino-1,3,4-thiadiazol-2-yl)sulfanyl]-N-(2,4,5-trichlorophenyl)acetamide
by: S. Madan Kumar, et al.
Published: (2016-07-01)

Crystal structure and Hirshfeld surface analysis of 2-[(1,3-benzoxazol-2-yl)sulfanyl]-N-(2-methoxyphenyl)acetamide
by: Abdullah Aydin, et al.
Published: (2019-10-01)

Synthesis, spectral analysis and anti-bacterial study of N-substituted derivatives of 2-(5-(1-(phenylsulfonyl)piperidin-4-yl)-1,3,4-oxadiazol-2-ylthio)acetamide
by: Hira Khalid, et al.
Published: (2016-09-01)

1-(4-Nitrophenyl)-2-({4-phenyl-5-[(p-tolyloxy)methyl]-4H-1,2,4-triazol-3-yl}sulfanyl)acetamide
by: Elham A. Al-Taifi, et al.
Published: (2016-10-01)

Crystal structure and Hirshfeld surface analysis of 2-chloro-N-(4-methoxyphenyl)acetamide
by: Mohcine Missioui, et al.
Published: (2022-07-01)

Crystal structure of 2-cyano-N-(furan-2-ylmethyl)acetamide
by: Shivanna Subhadramma, et al.
Published: (2015-07-01)

N-(4-Bromophenyl)-2-[(1-cyclohexylmethyl-1H-1,2,4-triazol-3-yl)sulfanyl]acetamide
by: Yue-Ping Wang, et al.
Published: (2012-05-01)

Synthesis, crystal structure and Hirshfeld surface analysis of N-(4-fluorophenyl)-N-isopropyl-2-(methylsulfonyl)acetamide
by: Doreswamy Geetha, et al.
Published: (2023-05-01)

2-{[5-(4-Chlorophenoxymethyl)-4-phenyl-4H-1,2,4-triazol-3-yl]sulfanyl}-N-(4-nitrophenyl)acetamide
by: Joel T. Mague, et al.
Published: (2016-03-01)

The mechanism and pharmacodynamics of 2-((1H-indol-3-yl)thio/sulfinyl)-N-pheny acetamide derivative as a novel inhibitor against human respiratory syncytial virus
by: Ningning Cheng, et al.
Published: (2022-12-01)

N-(2-Chlorophenyl)-2-(4,6-dimethylpyrimidin-2-ylsulfanyl)acetamide
by: Hong Qiu, et al.
Published: (2009-05-01)

Simple preparation of new N-aryl-N-(3-indolmethyl) acetamides and their spectroscopic analysis
by: José A. Henao, et al.
Published: (2009-12-01)

2,3,5,6-Tetrakis{[(pyridin-2-yl)sulfanyl]methyl}pyrazine
by: Tokouré Assoumatine, et al.
Published: (2016-12-01)

Synthesis of a 2-nitroimidazole derivative N-(4-[18F]fluorobenzyl)-2-(2-nitro-1H-imidazol-1-yl)-acetamide ([18 F]FBNA) as PET radiotracer for imaging tumor hypoxia
by: Arian Pérez Nario, et al.
Published: (2022-06-01)

N-(Thiazol-2-yl)acetamide
by: Uzma Yunus, et al.
Published: (2008-08-01)

N-(2,6-Dichlorophenyl)-2-(naphthalen-1-yl)acetamide
by: Hoong-Kun Fun, et al.
Published: (2012-05-01)

Synthesis, potential anticonvulsant and antidepressant effects of 2-(5-methyl-2,3-dioxoindolin-1-yl)acetamide derivatives
by: Xinghua Zhen, et al.
Published: (2015-07-01)

Synthesis of new 2-{2,3-dihydro-1,4-benzodioxin-6-yl[(4-methylphenyl) sulfonyl]amino}-N-(un/substituted-phenyl)acetamides as α-glucosidase and acetylcholinesterase inhibitors and their in silico study
by: Muhammad Athar Abbasi, et al.

[2+2+2] Annulation of <i>N</i>-(1-Naphthyl)acetamide with Two Alkynoates via Cleavage of Adjacent C–H and C–N Bonds Catalyzed by an Electron-Deficient Rhodium(III) Complex
by: Jyunichi Terasawa, et al.
Published: (2018-12-01)

N-(2-Chlorophenyl)-2-({5-[4-(methylsulfanyl)benzyl]-4-phenyl-4H-1,2,4-triazol-3-yl}sulfanyl)acetamide
by: Hoong-Kun Fun, et al.
Published: (2011-08-01)