Carbon electrode sensitivity enhancement for lead detection using polypyrrole, ionic liquid, and nafion composite

This paper concerns enhancing a lead detection sensor using a combination of polypyrrole (PPy), Nafion (N), and ionic liquid (IL) with thick-film or screen-printing technology on sensitive material-based carbon electrodes. Electrode characterization using a scanning electron microscope (SEM) was con...

Full description

Bibliographic Details
Main Authors: Zanu Saputra, Robeth Viktoria Manurung, Aminuddin Debataraja, Muhammad Iqbal Nugraha, Tien-Fu Lu
Format: Article
Language:English
Published: Indonesian Institute of Sciences 2022-07-01
Series:Journal of Mechatronics, Electrical Power, and Vehicular Technology
Subjects:
Online Access:https://mev.lipi.go.id/mev/article/view/544
_version_ 1828063443014385664
author Zanu Saputra
Robeth Viktoria Manurung
Aminuddin Debataraja
Muhammad Iqbal Nugraha
Tien-Fu Lu
author_facet Zanu Saputra
Robeth Viktoria Manurung
Aminuddin Debataraja
Muhammad Iqbal Nugraha
Tien-Fu Lu
author_sort Zanu Saputra
collection DOAJ
description This paper concerns enhancing a lead detection sensor using a combination of polypyrrole (PPy), Nafion (N), and ionic liquid (IL) with thick-film or screen-printing technology on sensitive material-based carbon electrodes. Electrode characterization using a scanning electron microscope (SEM) was conducted to see the morphology of sensitive materials, showing that the spherical particles were distributed evenly on the electrode surface. Analysis using energy dispersive spectroscopy (EDS) shows that the element's atomic composition is 84.92 %, 8.81 %, 6.26 %, and 0.01 % for carbon, nitrogen, oxygen, and bismuth, respectively. Potentiostat measurement with the ambient temperature of 25 °C on a standard lead solution with concentration ranging from 0.05 to 0.5 mg/l yields an average output voltage ranging from 2.16 to 2.27 V. It can be concluded that the sensor is able to detect lead with a sensitivity of 0.21 V in each addition of solution concentration (mg/l) and give an 84 % concentration contribution to the voltage.
first_indexed 2024-04-10T22:44:25Z
format Article
id doaj.art-f15938aeead74dc38c3be372fb6d3b35
institution Directory Open Access Journal
issn 2087-3379
2088-6985
language English
last_indexed 2024-04-10T22:44:25Z
publishDate 2022-07-01
publisher Indonesian Institute of Sciences
record_format Article
series Journal of Mechatronics, Electrical Power, and Vehicular Technology
spelling doaj.art-f15938aeead74dc38c3be372fb6d3b352023-01-15T16:43:09ZengIndonesian Institute of SciencesJournal of Mechatronics, Electrical Power, and Vehicular Technology2087-33792088-69852022-07-011319510010.14203/j.mev.2022.v13.95-100282Carbon electrode sensitivity enhancement for lead detection using polypyrrole, ionic liquid, and nafion compositeZanu Saputra0Robeth Viktoria Manurung1Aminuddin Debataraja2Muhammad Iqbal Nugraha3Tien-Fu Lu4Politeknik Manufaktur Negeri Bangka BelitungResearch Center for Telecommunication, National Research and Innovation Agency (BRIN)Politeknik Negeri JakartaPoliteknik Manufaktur Negeri Bangka BelitungThe University of AdelaideThis paper concerns enhancing a lead detection sensor using a combination of polypyrrole (PPy), Nafion (N), and ionic liquid (IL) with thick-film or screen-printing technology on sensitive material-based carbon electrodes. Electrode characterization using a scanning electron microscope (SEM) was conducted to see the morphology of sensitive materials, showing that the spherical particles were distributed evenly on the electrode surface. Analysis using energy dispersive spectroscopy (EDS) shows that the element's atomic composition is 84.92 %, 8.81 %, 6.26 %, and 0.01 % for carbon, nitrogen, oxygen, and bismuth, respectively. Potentiostat measurement with the ambient temperature of 25 °C on a standard lead solution with concentration ranging from 0.05 to 0.5 mg/l yields an average output voltage ranging from 2.16 to 2.27 V. It can be concluded that the sensor is able to detect lead with a sensitivity of 0.21 V in each addition of solution concentration (mg/l) and give an 84 % concentration contribution to the voltage.https://mev.lipi.go.id/mev/article/view/544lead detectionthick filmpolypyrrolenafionionic liquid.
spellingShingle Zanu Saputra
Robeth Viktoria Manurung
Aminuddin Debataraja
Muhammad Iqbal Nugraha
Tien-Fu Lu
Carbon electrode sensitivity enhancement for lead detection using polypyrrole, ionic liquid, and nafion composite
Journal of Mechatronics, Electrical Power, and Vehicular Technology
lead detection
thick film
polypyrrole
nafion
ionic liquid.
title Carbon electrode sensitivity enhancement for lead detection using polypyrrole, ionic liquid, and nafion composite
title_full Carbon electrode sensitivity enhancement for lead detection using polypyrrole, ionic liquid, and nafion composite
title_fullStr Carbon electrode sensitivity enhancement for lead detection using polypyrrole, ionic liquid, and nafion composite
title_full_unstemmed Carbon electrode sensitivity enhancement for lead detection using polypyrrole, ionic liquid, and nafion composite
title_short Carbon electrode sensitivity enhancement for lead detection using polypyrrole, ionic liquid, and nafion composite
title_sort carbon electrode sensitivity enhancement for lead detection using polypyrrole ionic liquid and nafion composite
topic lead detection
thick film
polypyrrole
nafion
ionic liquid.
url https://mev.lipi.go.id/mev/article/view/544
work_keys_str_mv AT zanusaputra carbonelectrodesensitivityenhancementforleaddetectionusingpolypyrroleionicliquidandnafioncomposite
AT robethviktoriamanurung carbonelectrodesensitivityenhancementforleaddetectionusingpolypyrroleionicliquidandnafioncomposite
AT aminuddindebataraja carbonelectrodesensitivityenhancementforleaddetectionusingpolypyrroleionicliquidandnafioncomposite
AT muhammadiqbalnugraha carbonelectrodesensitivityenhancementforleaddetectionusingpolypyrroleionicliquidandnafioncomposite
AT tienfulu carbonelectrodesensitivityenhancementforleaddetectionusingpolypyrroleionicliquidandnafioncomposite