Preparation and Performance of Ultra-Fine High Activity Composite Micronized Powder from Multi-Solid Waste

The composite micronized powder is prepared by using blast furnace slag (BFS), water-quenched manganese slag (WQMS), manganese tailing slag (MTS) and desulfurization gypsum (DG) and grinding aid (GA) through orthogonal test optimization design. The effect of the doping amount of each solid waste on...

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Main Authors: Penghuai Wang, Yang Ming, Ping Chen, Dengke Huang, Qiyang Zhu, Hao Ren, Xinheng Li
Format: Article
Language:English
Published: MDPI AG 2023-12-01
Series:Applied Sciences
Subjects:
Online Access:https://www.mdpi.com/2076-3417/13/24/13155
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author Penghuai Wang
Yang Ming
Ping Chen
Dengke Huang
Qiyang Zhu
Hao Ren
Xinheng Li
author_facet Penghuai Wang
Yang Ming
Ping Chen
Dengke Huang
Qiyang Zhu
Hao Ren
Xinheng Li
author_sort Penghuai Wang
collection DOAJ
description The composite micronized powder is prepared by using blast furnace slag (BFS), water-quenched manganese slag (WQMS), manganese tailing slag (MTS) and desulfurization gypsum (DG) and grinding aid (GA) through orthogonal test optimization design. The effect of the doping amount of each solid waste on the fluidity, activity at different ages and resistance to chloride ion penetration of the composite micropowder was studied systematically, and the exothermic characteristics of hydration of the composite micropowder with the optimal ratio were tested. The results showed that the amount of MTS dosing was the most significant factor among the four factors on the activity index of composite micronized powder at 7 d and 28 d. The activity index at 28 d decreased and then increased with the increase in MTS dosing; the amount of BFS dosing was the most significant factor affecting the fluidity and chloride ion permeation resistance of composite micronized powder. With an increase in BFS dosing, the fluidity ratio of composite micronized powder increased and then decreased; the electric flux of the matrix decreased, and the chloride ion permeation resistance increased. The optimal ratio of composite powder with the highest 28 d activity is 35% BFS, 30% MTS, 0.3% GA, 5% DG and 30% WQMS. The hydration rate and cumulative heat release of the slurry prepared with the optimal ratio of composite micronized powder to cement (1:1) are lower than those of pure cement slurry. The microstructure of the mortar test block prepared with a 1:1 composite of cement is more compact than that of the pure cement mortar test block, and the pores are fewer.
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spelling doaj.art-f196da9397b94c91b5cbc42d5f58ec362023-12-22T13:51:39ZengMDPI AGApplied Sciences2076-34172023-12-0113241315510.3390/app132413155Preparation and Performance of Ultra-Fine High Activity Composite Micronized Powder from Multi-Solid WastePenghuai Wang0Yang Ming1Ping Chen2Dengke Huang3Qiyang Zhu4Hao Ren5Xinheng Li6College of Materials Science and Engineering, Guilin University of Technology, Guilin 541004, ChinaGuangxi Key Laboratory of Green Building Materials and Construction, Guilin 541004, ChinaGuangxi Key Laboratory of Green Building Materials and Construction, Guilin 541004, ChinaCollege of Materials Science and Engineering, Guilin University of Technology, Guilin 541004, ChinaCollege of Materials Science and Engineering, Guilin University of Technology, Guilin 541004, ChinaCollege of Materials Science and Engineering, Guilin University of Technology, Guilin 541004, ChinaCollege of Materials Science and Engineering, Guilin University of Technology, Guilin 541004, ChinaThe composite micronized powder is prepared by using blast furnace slag (BFS), water-quenched manganese slag (WQMS), manganese tailing slag (MTS) and desulfurization gypsum (DG) and grinding aid (GA) through orthogonal test optimization design. The effect of the doping amount of each solid waste on the fluidity, activity at different ages and resistance to chloride ion penetration of the composite micropowder was studied systematically, and the exothermic characteristics of hydration of the composite micropowder with the optimal ratio were tested. The results showed that the amount of MTS dosing was the most significant factor among the four factors on the activity index of composite micronized powder at 7 d and 28 d. The activity index at 28 d decreased and then increased with the increase in MTS dosing; the amount of BFS dosing was the most significant factor affecting the fluidity and chloride ion permeation resistance of composite micronized powder. With an increase in BFS dosing, the fluidity ratio of composite micronized powder increased and then decreased; the electric flux of the matrix decreased, and the chloride ion permeation resistance increased. The optimal ratio of composite powder with the highest 28 d activity is 35% BFS, 30% MTS, 0.3% GA, 5% DG and 30% WQMS. The hydration rate and cumulative heat release of the slurry prepared with the optimal ratio of composite micronized powder to cement (1:1) are lower than those of pure cement slurry. The microstructure of the mortar test block prepared with a 1:1 composite of cement is more compact than that of the pure cement mortar test block, and the pores are fewer.https://www.mdpi.com/2076-3417/13/24/13155multi-solid wasteflowabilitymechanical propertieshydration propertiesorthogonal test
spellingShingle Penghuai Wang
Yang Ming
Ping Chen
Dengke Huang
Qiyang Zhu
Hao Ren
Xinheng Li
Preparation and Performance of Ultra-Fine High Activity Composite Micronized Powder from Multi-Solid Waste
Applied Sciences
multi-solid waste
flowability
mechanical properties
hydration properties
orthogonal test
title Preparation and Performance of Ultra-Fine High Activity Composite Micronized Powder from Multi-Solid Waste
title_full Preparation and Performance of Ultra-Fine High Activity Composite Micronized Powder from Multi-Solid Waste
title_fullStr Preparation and Performance of Ultra-Fine High Activity Composite Micronized Powder from Multi-Solid Waste
title_full_unstemmed Preparation and Performance of Ultra-Fine High Activity Composite Micronized Powder from Multi-Solid Waste
title_short Preparation and Performance of Ultra-Fine High Activity Composite Micronized Powder from Multi-Solid Waste
title_sort preparation and performance of ultra fine high activity composite micronized powder from multi solid waste
topic multi-solid waste
flowability
mechanical properties
hydration properties
orthogonal test
url https://www.mdpi.com/2076-3417/13/24/13155
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