Synthesis, Characterization and Thermal Study of Polyimides Derived from Polystyrene
A novel polyimides of polystyrene with high thermal stability were prepared by the reaction of aminated polystyrene with Benzophenone tetracarboxylic dianhydride. The aminated polystyrene were prepared from the nitration of polystyrene followed by chemical reduction of its nitro groups. Infrared (FT...
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Format: | Article |
Language: | English |
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University of Anbar
2012-10-01
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Series: | مجلة جامعة الانبار للعلوم الصرفة |
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Online Access: | https://juaps.uoanbar.edu.iq/article_62770_af73e94fd59a8d0385185e93584063e1.pdf |
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author | Abdulsalam A. Shyaa |
author_facet | Abdulsalam A. Shyaa |
author_sort | Abdulsalam A. Shyaa |
collection | DOAJ |
description | A novel polyimides of polystyrene with high thermal stability were prepared by the reaction of aminated polystyrene with Benzophenone tetracarboxylic dianhydride. The aminated polystyrene were prepared from the nitration of polystyrene followed by chemical reduction of its nitro groups. Infrared (FT-IR) spectra and thermogravimetric analysis (TGA) were used to characterize polymers . The prepared polymer exhibit good thermal and thermooxidative stability at polymer decomposition temperature greater than 550°C in air atmosphere . Another attractive feature is their high char yields 75% at 650°C in air atmosphere. |
first_indexed | 2024-03-08T18:48:34Z |
format | Article |
id | doaj.art-f1b712063bb14fb29208fe41320579d1 |
institution | Directory Open Access Journal |
issn | 1991-8941 2706-6703 |
language | English |
last_indexed | 2024-03-08T18:48:34Z |
publishDate | 2012-10-01 |
publisher | University of Anbar |
record_format | Article |
series | مجلة جامعة الانبار للعلوم الصرفة |
spelling | doaj.art-f1b712063bb14fb29208fe41320579d12023-12-28T21:55:58ZengUniversity of Anbarمجلة جامعة الانبار للعلوم الصرفة1991-89412706-67032012-10-0161212710.37652/juaps.2012.6277062770Synthesis, Characterization and Thermal Study of Polyimides Derived from PolystyreneAbdulsalam A. Shyaa0Al-Mustansiriya University - College Of Science.A novel polyimides of polystyrene with high thermal stability were prepared by the reaction of aminated polystyrene with Benzophenone tetracarboxylic dianhydride. The aminated polystyrene were prepared from the nitration of polystyrene followed by chemical reduction of its nitro groups. Infrared (FT-IR) spectra and thermogravimetric analysis (TGA) were used to characterize polymers . The prepared polymer exhibit good thermal and thermooxidative stability at polymer decomposition temperature greater than 550°C in air atmosphere . Another attractive feature is their high char yields 75% at 650°C in air atmosphere.https://juaps.uoanbar.edu.iq/article_62770_af73e94fd59a8d0385185e93584063e1.pdfsynthesischaracterizationthermalpolyimidespolystyrene |
spellingShingle | Abdulsalam A. Shyaa Synthesis, Characterization and Thermal Study of Polyimides Derived from Polystyrene مجلة جامعة الانبار للعلوم الصرفة synthesis characterization thermal polyimides polystyrene |
title | Synthesis, Characterization and Thermal Study of Polyimides Derived from Polystyrene |
title_full | Synthesis, Characterization and Thermal Study of Polyimides Derived from Polystyrene |
title_fullStr | Synthesis, Characterization and Thermal Study of Polyimides Derived from Polystyrene |
title_full_unstemmed | Synthesis, Characterization and Thermal Study of Polyimides Derived from Polystyrene |
title_short | Synthesis, Characterization and Thermal Study of Polyimides Derived from Polystyrene |
title_sort | synthesis characterization and thermal study of polyimides derived from polystyrene |
topic | synthesis characterization thermal polyimides polystyrene |
url | https://juaps.uoanbar.edu.iq/article_62770_af73e94fd59a8d0385185e93584063e1.pdf |
work_keys_str_mv | AT abdulsalamashyaa synthesischaracterizationandthermalstudyofpolyimidesderivedfrompolystyrene |