Synthesis, Characterization and Thermal Study of Polyimides Derived from Polystyrene

A novel polyimides of polystyrene with high thermal stability were prepared by the reaction of aminated polystyrene with Benzophenone tetracarboxylic dianhydride. The aminated polystyrene were prepared from the nitration of polystyrene followed by chemical reduction of its nitro groups. Infrared (FT...

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Main Author: Abdulsalam A. Shyaa
Format: Article
Language:English
Published: University of Anbar 2012-10-01
Series:مجلة جامعة الانبار للعلوم الصرفة
Subjects:
Online Access:https://juaps.uoanbar.edu.iq/article_62770_af73e94fd59a8d0385185e93584063e1.pdf
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author Abdulsalam A. Shyaa
author_facet Abdulsalam A. Shyaa
author_sort Abdulsalam A. Shyaa
collection DOAJ
description A novel polyimides of polystyrene with high thermal stability were prepared by the reaction of aminated polystyrene with Benzophenone tetracarboxylic dianhydride. The aminated polystyrene were prepared from the nitration of polystyrene followed by chemical reduction of its nitro groups. Infrared (FT-IR) spectra and thermogravimetric analysis (TGA) were used to characterize polymers . The prepared polymer exhibit good thermal and thermooxidative stability at polymer decomposition temperature greater than 550°C in air atmosphere . Another attractive feature is their high char yields 75% at 650°C in air atmosphere.
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spelling doaj.art-f1b712063bb14fb29208fe41320579d12023-12-28T21:55:58ZengUniversity of Anbarمجلة جامعة الانبار للعلوم الصرفة1991-89412706-67032012-10-0161212710.37652/juaps.2012.6277062770Synthesis, Characterization and Thermal Study of Polyimides Derived from PolystyreneAbdulsalam A. Shyaa0Al-Mustansiriya University - College Of Science.A novel polyimides of polystyrene with high thermal stability were prepared by the reaction of aminated polystyrene with Benzophenone tetracarboxylic dianhydride. The aminated polystyrene were prepared from the nitration of polystyrene followed by chemical reduction of its nitro groups. Infrared (FT-IR) spectra and thermogravimetric analysis (TGA) were used to characterize polymers . The prepared polymer exhibit good thermal and thermooxidative stability at polymer decomposition temperature greater than 550°C in air atmosphere . Another attractive feature is their high char yields 75% at 650°C in air atmosphere.https://juaps.uoanbar.edu.iq/article_62770_af73e94fd59a8d0385185e93584063e1.pdfsynthesischaracterizationthermalpolyimidespolystyrene
spellingShingle Abdulsalam A. Shyaa
Synthesis, Characterization and Thermal Study of Polyimides Derived from Polystyrene
مجلة جامعة الانبار للعلوم الصرفة
synthesis
characterization
thermal
polyimides
polystyrene
title Synthesis, Characterization and Thermal Study of Polyimides Derived from Polystyrene
title_full Synthesis, Characterization and Thermal Study of Polyimides Derived from Polystyrene
title_fullStr Synthesis, Characterization and Thermal Study of Polyimides Derived from Polystyrene
title_full_unstemmed Synthesis, Characterization and Thermal Study of Polyimides Derived from Polystyrene
title_short Synthesis, Characterization and Thermal Study of Polyimides Derived from Polystyrene
title_sort synthesis characterization and thermal study of polyimides derived from polystyrene
topic synthesis
characterization
thermal
polyimides
polystyrene
url https://juaps.uoanbar.edu.iq/article_62770_af73e94fd59a8d0385185e93584063e1.pdf
work_keys_str_mv AT abdulsalamashyaa synthesischaracterizationandthermalstudyofpolyimidesderivedfrompolystyrene