Synthesis of bis-quinoxaline derivatives using Tonsil clay as a catalyst

A convenient and efficient synthesis of new bis-quinoxaline is described, involving condensation of 1,2-diamines with 9-ethyl-3,6-di(1,2-dioxoethyl)carbazole in the presence of Tonsil clay, a readily available and inexpensive catalyst. The structures of all new products were identified by 1H-NMR, 1...

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Main Authors: M. Badali, J. Khalafy, M. Aghazadeh, R. H. Prager
Format: Article
Language:English
Published: Chemical Society of Ethiopia 2016-02-01
Series:Bulletin of the Chemical Society of Ethiopia
Subjects:
Online Access:http://www.ajol.info/index.php/bcse/article/view/129775
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author M. Badali
J. Khalafy
M. Aghazadeh
R. H. Prager
author_facet M. Badali
J. Khalafy
M. Aghazadeh
R. H. Prager
author_sort M. Badali
collection DOAJ
description A convenient and efficient synthesis of new bis-quinoxaline is described, involving condensation of 1,2-diamines with 9-ethyl-3,6-di(1,2-dioxoethyl)carbazole in the presence of Tonsil clay, a readily available and inexpensive catalyst. The structures of all new products were identified by 1H-NMR, 13C-NMR and FT-IR spectral data and microanalysis. DOI: http://dx.doi.org/10.4314/bcse.v30i1.12
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spelling doaj.art-f2b33b706ea1444d98b85d0427972b422022-12-22T03:47:34ZengChemical Society of EthiopiaBulletin of the Chemical Society of Ethiopia1011-39241726-801X2016-02-01301129136http://dx.doi.org/10.4314/bcse.v30i1.12Synthesis of bis-quinoxaline derivatives using Tonsil clay as a catalystM. BadaliJ. KhalafyM. AghazadehR. H. PragerA convenient and efficient synthesis of new bis-quinoxaline is described, involving condensation of 1,2-diamines with 9-ethyl-3,6-di(1,2-dioxoethyl)carbazole in the presence of Tonsil clay, a readily available and inexpensive catalyst. The structures of all new products were identified by 1H-NMR, 13C-NMR and FT-IR spectral data and microanalysis. DOI: http://dx.doi.org/10.4314/bcse.v30i1.12http://www.ajol.info/index.php/bcse/article/view/129775bis-Quinoxalinebis-GlyoxalGreen chemistry12-DiamineTonsil clay
spellingShingle M. Badali
J. Khalafy
M. Aghazadeh
R. H. Prager
Synthesis of bis-quinoxaline derivatives using Tonsil clay as a catalyst
Bulletin of the Chemical Society of Ethiopia
bis-Quinoxaline
bis-Glyoxal
Green chemistry
1
2-Diamine
Tonsil clay
title Synthesis of bis-quinoxaline derivatives using Tonsil clay as a catalyst
title_full Synthesis of bis-quinoxaline derivatives using Tonsil clay as a catalyst
title_fullStr Synthesis of bis-quinoxaline derivatives using Tonsil clay as a catalyst
title_full_unstemmed Synthesis of bis-quinoxaline derivatives using Tonsil clay as a catalyst
title_short Synthesis of bis-quinoxaline derivatives using Tonsil clay as a catalyst
title_sort synthesis of bis quinoxaline derivatives using tonsil clay as a catalyst
topic bis-Quinoxaline
bis-Glyoxal
Green chemistry
1
2-Diamine
Tonsil clay
url http://www.ajol.info/index.php/bcse/article/view/129775
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AT jkhalafy synthesisofbisquinoxalinederivativesusingtonsilclayasacatalyst
AT maghazadeh synthesisofbisquinoxalinederivativesusingtonsilclayasacatalyst
AT rhprager synthesisofbisquinoxalinederivativesusingtonsilclayasacatalyst