Process optimization for acid-amine coupling: a catalytic approach
Proficient routes were devised for coupling different aromatic/aliphatic acids with amines to form amide linkage using various catalysts. Under the optimized reaction conditions, highest conversion was possible without formation of any by-products. All synthesized compounds were purified us...
| Main Authors: | , , , , |
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| Format: | Article |
| Language: | English |
| Published: |
Growing Science
2023-01-01
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| Series: | Current Chemistry Letters |
| Online Access: | http://www.growingscience.com/ccl/Vol12/ccl_2022_36.pdf |
| _version_ | 1811241492283392000 |
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| author | Ranjitsinh C. Dabhi Unnati P. Patel Vaibhavi B. Rathod Siddharth N. Shah Jayesh J. Maru |
| author_facet | Ranjitsinh C. Dabhi Unnati P. Patel Vaibhavi B. Rathod Siddharth N. Shah Jayesh J. Maru |
| author_sort | Ranjitsinh C. Dabhi |
| collection | DOAJ |
| description | Proficient routes were devised for coupling different aromatic/aliphatic acids with amines to form amide linkage using various catalysts. Under the optimized reaction conditions, highest conversion was possible without formation of any by-products. All synthesized compounds were purified using column chromatography and characterized by mass spectrometry, nuclear magnetic resonance spectrometry and liquid chromatography-mass spectrometric analysis. |
| first_indexed | 2024-04-12T13:36:58Z |
| format | Article |
| id | doaj.art-f2ec408af0174c04a7e2a73d08fcc75f |
| institution | Directory Open Access Journal |
| issn | 1927-7296 1927-730X |
| language | English |
| last_indexed | 2024-04-12T13:36:58Z |
| publishDate | 2023-01-01 |
| publisher | Growing Science |
| record_format | Article |
| series | Current Chemistry Letters |
| spelling | doaj.art-f2ec408af0174c04a7e2a73d08fcc75f2022-12-22T03:30:58ZengGrowing ScienceCurrent Chemistry Letters1927-72961927-730X2023-01-0112113314010.5267/j.ccl.2022.8.010Process optimization for acid-amine coupling: a catalytic approachRanjitsinh C. DabhiUnnati P. PatelVaibhavi B. RathodSiddharth N. ShahJayesh J. Maru Proficient routes were devised for coupling different aromatic/aliphatic acids with amines to form amide linkage using various catalysts. Under the optimized reaction conditions, highest conversion was possible without formation of any by-products. All synthesized compounds were purified using column chromatography and characterized by mass spectrometry, nuclear magnetic resonance spectrometry and liquid chromatography-mass spectrometric analysis.http://www.growingscience.com/ccl/Vol12/ccl_2022_36.pdf |
| spellingShingle | Ranjitsinh C. Dabhi Unnati P. Patel Vaibhavi B. Rathod Siddharth N. Shah Jayesh J. Maru Process optimization for acid-amine coupling: a catalytic approach Current Chemistry Letters |
| title | Process optimization for acid-amine coupling: a catalytic approach |
| title_full | Process optimization for acid-amine coupling: a catalytic approach |
| title_fullStr | Process optimization for acid-amine coupling: a catalytic approach |
| title_full_unstemmed | Process optimization for acid-amine coupling: a catalytic approach |
| title_short | Process optimization for acid-amine coupling: a catalytic approach |
| title_sort | process optimization for acid amine coupling a catalytic approach |
| url | http://www.growingscience.com/ccl/Vol12/ccl_2022_36.pdf |
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