PHASE FORMATION IN NiTiAl10 POWDER MIXTURE DURING HEATING TO 1100 °C

In this paper the comparison of NiTiAl10 wt. % with the binary NiTi46 wt. % prepared by powder metallurgy was researched. The method of combustion synthesis was carried out under following conditions: sintering temperature of 800 °C and 1100 °C and heating rate approx. 300 °C.min-1. The addition of...

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Main Authors: Pavel Salvetr, Andrea Školáková, Pavel Novák, Dalibor Vojtěch
Format: Article
Language:English
Published: SciCell s.r.o. 2018-06-01
Series:Acta Metallurgica Slovaca
Subjects:
Online Access:https://journals.scicell.org/index.php/AMS/article/view/267
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author Pavel Salvetr
Andrea Školáková
Pavel Novák
Dalibor Vojtěch
author_facet Pavel Salvetr
Andrea Školáková
Pavel Novák
Dalibor Vojtěch
author_sort Pavel Salvetr
collection DOAJ
description In this paper the comparison of NiTiAl10 wt. % with the binary NiTi46 wt. % prepared by powder metallurgy was researched. The method of combustion synthesis was carried out under following conditions: sintering temperature of 800 °C and 1100 °C and heating rate approx. 300 °C.min-1. The addition of aluminium to NiTi46 wt. % powder mixture completely changed the temperature of combustion synthesis and phase evolution during sintering. The reactions into Ni-Ti-Al powder mixture started below the melting temperature of aluminium and the new phases were formed in the material. The process of reactive sintering was studied by differential thermal analysis using the heating rate of 30 °C.min-1 and 100 °C.min-1. A combination of induction furnace and optical pyrometer. The addition of aluminium influenced microstructure significantly and increased the hardness of samples.
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spelling doaj.art-f31c76d05a4f4501861beafec728b1052022-12-22T02:51:47ZengSciCell s.r.o.Acta Metallurgica Slovaca1335-15321338-11562018-06-0124210.12776/ams.v24i2.1081PHASE FORMATION IN NiTiAl10 POWDER MIXTURE DURING HEATING TO 1100 °CPavel SalvetrAndrea ŠkolákováPavel NovákDalibor VojtěchIn this paper the comparison of NiTiAl10 wt. % with the binary NiTi46 wt. % prepared by powder metallurgy was researched. The method of combustion synthesis was carried out under following conditions: sintering temperature of 800 °C and 1100 °C and heating rate approx. 300 °C.min-1. The addition of aluminium to NiTi46 wt. % powder mixture completely changed the temperature of combustion synthesis and phase evolution during sintering. The reactions into Ni-Ti-Al powder mixture started below the melting temperature of aluminium and the new phases were formed in the material. The process of reactive sintering was studied by differential thermal analysis using the heating rate of 30 °C.min-1 and 100 °C.min-1. A combination of induction furnace and optical pyrometer. The addition of aluminium influenced microstructure significantly and increased the hardness of samples.https://journals.scicell.org/index.php/AMS/article/view/267Self-propagating high-temperature synthesisPowder metallurgy (PM)Differential thermal analysis (DTA),Intermetallics
spellingShingle Pavel Salvetr
Andrea Školáková
Pavel Novák
Dalibor Vojtěch
PHASE FORMATION IN NiTiAl10 POWDER MIXTURE DURING HEATING TO 1100 °C
Acta Metallurgica Slovaca
Self-propagating high-temperature synthesis
Powder metallurgy (PM)
Differential thermal analysis (DTA),
Intermetallics
title PHASE FORMATION IN NiTiAl10 POWDER MIXTURE DURING HEATING TO 1100 °C
title_full PHASE FORMATION IN NiTiAl10 POWDER MIXTURE DURING HEATING TO 1100 °C
title_fullStr PHASE FORMATION IN NiTiAl10 POWDER MIXTURE DURING HEATING TO 1100 °C
title_full_unstemmed PHASE FORMATION IN NiTiAl10 POWDER MIXTURE DURING HEATING TO 1100 °C
title_short PHASE FORMATION IN NiTiAl10 POWDER MIXTURE DURING HEATING TO 1100 °C
title_sort phase formation in nitial10 powder mixture during heating to 1100 °c
topic Self-propagating high-temperature synthesis
Powder metallurgy (PM)
Differential thermal analysis (DTA),
Intermetallics
url https://journals.scicell.org/index.php/AMS/article/view/267
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AT andreaskolakova phaseformationinnitial10powdermixtureduringheatingto1100c
AT pavelnovak phaseformationinnitial10powdermixtureduringheatingto1100c
AT daliborvojtech phaseformationinnitial10powdermixtureduringheatingto1100c