| Summary: | Additive Manufacturing (AM) of multimaterial components is a promising way of fabricating parts with improved functional properties. It allows for the combination of materials with different properties into a single component. The Ti<sub>2</sub>AlNb-based intermetallic alloy provides high temperature strength, while the Ti-6Al-4V (Ti64) alloy has good fracture toughness, ductility, and a relatively low cost. A combination of these alloys into a single component can be used to produce advanced multimaterial parts. In this work, Ti<sub>2</sub>AlNb/Ti-6Al-4V bimetallic structures were fabricated from pre-alloyed powders using the Selective Laser Melting (SLM) process. The effects of high-temperature substrate preheating, post-processing by annealing, and hot isostatic pressing on defect formation, the microstructural evolution of the interface area, and the mechanical properties of the bimetallic samples were investigated. High-temperature substrate preheating during the SLM process was necessary to prevent reheat cracking of the Ti<sub>2</sub>AlNb part, while annealing and hot isostatic pressing post-processing improved the chemical and microstructural homogeneity of the transition zone and enhanced the tensile properties of the bimetallic structure.
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