Cyclic Mechanical Fatigue Lifetime of Bi<sub>0.5</sub>Na<sub>0.5</sub>TiO<sub>3</sub>-Based Eco-Piezoceramics

The mechanical strength and cyclic fatigue behavior of PIC700 commercial eco-piezoceramic disks are investigated under biaxial loading on unpoled and poled samples. The bending strength of unpoled samples was higher than those of poled ones. Fatigue tests were conducted under a load ratio of 10 at a...

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Main Authors: José F. Bartolomé, Luis E. Fuentes-Cobas, Álvaro García, Alfredo Jacas, Lorena Pardo
Format: Article
Language:English
Published: MDPI AG 2021-07-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/14/15/4113
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author José F. Bartolomé
Luis E. Fuentes-Cobas
Álvaro García
Alfredo Jacas
Lorena Pardo
author_facet José F. Bartolomé
Luis E. Fuentes-Cobas
Álvaro García
Alfredo Jacas
Lorena Pardo
author_sort José F. Bartolomé
collection DOAJ
description The mechanical strength and cyclic fatigue behavior of PIC700 commercial eco-piezoceramic disks are investigated under biaxial loading on unpoled and poled samples. The bending strength of unpoled samples was higher than those of poled ones. Fatigue tests were conducted under a load ratio of 10 at a frequency of 20 Hz with a sinusoidal waveform. The curve fitting for the S-N fatigue diagram is used to predict the lifetime of these eco-piezoceramics and describe their fatigue behavior. It was also found that the unpoled samples exhibited higher fatigue resistance than the poled ones. The fatigue limit of maximum load for ten million cycles of unpoled and poled samples was estimated to be 160 and 135 MPa, respectively. The detailed observations of the fatigue fracture surfaces by scanning electron microscopy (SEM) indicated that a wavy surface with a mixture of transgranular and intergranular fractures occurred preferentially in the case of the poled material. On the other hand, transgranular fractures seem to be predominant in the unpoled samples. It appears that the poling process causes the change in failure characteristics due to domain orientation that leaves an anisotropic stress field in the material. The poled ceramics possess a local stress concentration created by the orientation under the electric poling field of the 90° ferroelectric–ferroelastic domains. Under this local stress concentration, a microstructural degeneration is induced by domain switching under the cyclic load that accelerates crack growth, thereby reducing fatigue lifetime.
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spelling doaj.art-f3d2ab12590b4a7c8a20dd6ba90dd91a2023-11-22T05:51:54ZengMDPI AGMaterials1996-19442021-07-011415411310.3390/ma14154113Cyclic Mechanical Fatigue Lifetime of Bi<sub>0.5</sub>Na<sub>0.5</sub>TiO<sub>3</sub>-Based Eco-PiezoceramicsJosé F. Bartolomé0Luis E. Fuentes-Cobas1Álvaro García2Alfredo Jacas3Lorena Pardo4Instituto de Ciencia de Materiales de Madrid, CSIC, 28049 Madrid, SpainCentro de Investigación en Materiales Avanzados, S.C., Chihuahua 31136, MexicoInstituto de Ciencia de Materiales de Madrid, CSIC, 28049 Madrid, SpainInstituto de Ciencia de Materiales de Madrid, CSIC, 28049 Madrid, SpainInstituto de Ciencia de Materiales de Madrid, CSIC, 28049 Madrid, SpainThe mechanical strength and cyclic fatigue behavior of PIC700 commercial eco-piezoceramic disks are investigated under biaxial loading on unpoled and poled samples. The bending strength of unpoled samples was higher than those of poled ones. Fatigue tests were conducted under a load ratio of 10 at a frequency of 20 Hz with a sinusoidal waveform. The curve fitting for the S-N fatigue diagram is used to predict the lifetime of these eco-piezoceramics and describe their fatigue behavior. It was also found that the unpoled samples exhibited higher fatigue resistance than the poled ones. The fatigue limit of maximum load for ten million cycles of unpoled and poled samples was estimated to be 160 and 135 MPa, respectively. The detailed observations of the fatigue fracture surfaces by scanning electron microscopy (SEM) indicated that a wavy surface with a mixture of transgranular and intergranular fractures occurred preferentially in the case of the poled material. On the other hand, transgranular fractures seem to be predominant in the unpoled samples. It appears that the poling process causes the change in failure characteristics due to domain orientation that leaves an anisotropic stress field in the material. The poled ceramics possess a local stress concentration created by the orientation under the electric poling field of the 90° ferroelectric–ferroelastic domains. Under this local stress concentration, a microstructural degeneration is induced by domain switching under the cyclic load that accelerates crack growth, thereby reducing fatigue lifetime.https://www.mdpi.com/1996-1944/14/15/4113bismuth sodium titanatebarium titanatepiezoelectricitydielectric propertiespolingmechanical properties
spellingShingle José F. Bartolomé
Luis E. Fuentes-Cobas
Álvaro García
Alfredo Jacas
Lorena Pardo
Cyclic Mechanical Fatigue Lifetime of Bi<sub>0.5</sub>Na<sub>0.5</sub>TiO<sub>3</sub>-Based Eco-Piezoceramics
Materials
bismuth sodium titanate
barium titanate
piezoelectricity
dielectric properties
poling
mechanical properties
title Cyclic Mechanical Fatigue Lifetime of Bi<sub>0.5</sub>Na<sub>0.5</sub>TiO<sub>3</sub>-Based Eco-Piezoceramics
title_full Cyclic Mechanical Fatigue Lifetime of Bi<sub>0.5</sub>Na<sub>0.5</sub>TiO<sub>3</sub>-Based Eco-Piezoceramics
title_fullStr Cyclic Mechanical Fatigue Lifetime of Bi<sub>0.5</sub>Na<sub>0.5</sub>TiO<sub>3</sub>-Based Eco-Piezoceramics
title_full_unstemmed Cyclic Mechanical Fatigue Lifetime of Bi<sub>0.5</sub>Na<sub>0.5</sub>TiO<sub>3</sub>-Based Eco-Piezoceramics
title_short Cyclic Mechanical Fatigue Lifetime of Bi<sub>0.5</sub>Na<sub>0.5</sub>TiO<sub>3</sub>-Based Eco-Piezoceramics
title_sort cyclic mechanical fatigue lifetime of bi sub 0 5 sub na sub 0 5 sub tio sub 3 sub based eco piezoceramics
topic bismuth sodium titanate
barium titanate
piezoelectricity
dielectric properties
poling
mechanical properties
url https://www.mdpi.com/1996-1944/14/15/4113
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