Synthesis and Characterization of Titania-Rice Husk Silica Composites as Photocatalyst

This article describes the synthesis of titania-silica composites by a sol-gel method using a mixture of silica of rice husk and titanium butoxide sols. Microstructures were examined at calcination temperature in the range of 500 to 700 °C, with temperatures interval of 50 °C. The sintered catalysts...

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Main Authors: Posman Manurung, Rudy Situmeang, Ediman Ginting, Indra Pardede
Format: Article
Language:English
Published: Department of Chemistry, Universitas Gadjah Mada 2015-03-01
Series:Indonesian Journal of Chemistry
Subjects:
Online Access:https://jurnal.ugm.ac.id/ijc/article/view/21221
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author Posman Manurung
Rudy Situmeang
Ediman Ginting
Indra Pardede
author_facet Posman Manurung
Rudy Situmeang
Ediman Ginting
Indra Pardede
author_sort Posman Manurung
collection DOAJ
description This article describes the synthesis of titania-silica composites by a sol-gel method using a mixture of silica of rice husk and titanium butoxide sols. Microstructures were examined at calcination temperature in the range of 500 to 700 °C, with temperatures interval of 50 °C. The sintered catalysts were subsequently tested for photodegradation of methylene blue (MB) under ultraviolet and sunlight rays. Physical characteristics were analyzed using X-ray diffraction (XRD), scanning electron microscopy (SEM)/energy dispersive X-ray spectroscopy (EDS), and Brunauer-Emmett-Teller (BET). The XRD results did not show the presence of silica crystal phase in each sample. The results showed that the highest BET surface area of samples was obtained at the temperature of 650 °C. In sample calcined 500 °C, the activity of the catalyst on MB was relatively similar in both sunlight and ultraviolet rays.
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spelling doaj.art-f46a24278e5648c296b9a3befbf7f31f2022-12-21T19:55:11ZengDepartment of Chemistry, Universitas Gadjah MadaIndonesian Journal of Chemistry1411-94202460-15782015-03-01151364210.22146/ijc.2122114319Synthesis and Characterization of Titania-Rice Husk Silica Composites as PhotocatalystPosman Manurung0Rudy Situmeang1Ediman Ginting2Indra Pardede3Department of Physics, Lampung University, Jl. Sumantri Brojonegoro No. 1, Bandar Lampung 35145Department of Chemistry, Lampung University, Jl. Sumantri Brojonegoro No. 1, Bandar Lampung 35145Department of Physics, Lampung University, Jl. Sumantri Brojonegoro No. 1, Bandar Lampung 35145Department of Physics, Lampung University, Jl. Sumantri Brojonegoro No. 1, Bandar Lampung 35145This article describes the synthesis of titania-silica composites by a sol-gel method using a mixture of silica of rice husk and titanium butoxide sols. Microstructures were examined at calcination temperature in the range of 500 to 700 °C, with temperatures interval of 50 °C. The sintered catalysts were subsequently tested for photodegradation of methylene blue (MB) under ultraviolet and sunlight rays. Physical characteristics were analyzed using X-ray diffraction (XRD), scanning electron microscopy (SEM)/energy dispersive X-ray spectroscopy (EDS), and Brunauer-Emmett-Teller (BET). The XRD results did not show the presence of silica crystal phase in each sample. The results showed that the highest BET surface area of samples was obtained at the temperature of 650 °C. In sample calcined 500 °C, the activity of the catalyst on MB was relatively similar in both sunlight and ultraviolet rays.https://jurnal.ugm.ac.id/ijc/article/view/21221rice husk silicatitaniaphotocatalysisdye
spellingShingle Posman Manurung
Rudy Situmeang
Ediman Ginting
Indra Pardede
Synthesis and Characterization of Titania-Rice Husk Silica Composites as Photocatalyst
Indonesian Journal of Chemistry
rice husk silica
titania
photocatalysis
dye
title Synthesis and Characterization of Titania-Rice Husk Silica Composites as Photocatalyst
title_full Synthesis and Characterization of Titania-Rice Husk Silica Composites as Photocatalyst
title_fullStr Synthesis and Characterization of Titania-Rice Husk Silica Composites as Photocatalyst
title_full_unstemmed Synthesis and Characterization of Titania-Rice Husk Silica Composites as Photocatalyst
title_short Synthesis and Characterization of Titania-Rice Husk Silica Composites as Photocatalyst
title_sort synthesis and characterization of titania rice husk silica composites as photocatalyst
topic rice husk silica
titania
photocatalysis
dye
url https://jurnal.ugm.ac.id/ijc/article/view/21221
work_keys_str_mv AT posmanmanurung synthesisandcharacterizationoftitaniaricehusksilicacompositesasphotocatalyst
AT rudysitumeang synthesisandcharacterizationoftitaniaricehusksilicacompositesasphotocatalyst
AT edimanginting synthesisandcharacterizationoftitaniaricehusksilicacompositesasphotocatalyst
AT indrapardede synthesisandcharacterizationoftitaniaricehusksilicacompositesasphotocatalyst