Environment-Friendly Preparation of Reaction-Bonded Silicon Carbide by Addition of Boron in the Silicon Melt

Reaction-bonded silicon carbide ceramics were sintered by infiltration of Si and B–Si alloy under an argon atmosphere at different temperatures. The element boron was added to the silicon melt to form a B–Si alloy first. The mechanical properties of samples were improved by infiltration of the B–Si...

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Main Authors: Maoqiang Rui, Yaxiang Zhang, Jing Ye
Format: Article
Language:English
Published: MDPI AG 2021-02-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/14/5/1090
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author Maoqiang Rui
Yaxiang Zhang
Jing Ye
author_facet Maoqiang Rui
Yaxiang Zhang
Jing Ye
author_sort Maoqiang Rui
collection DOAJ
description Reaction-bonded silicon carbide ceramics were sintered by infiltration of Si and B–Si alloy under an argon atmosphere at different temperatures. The element boron was added to the silicon melt to form a B–Si alloy first. The mechanical properties of samples were improved by infiltration of the B–Si melt. The samples infiltrated with the Si-only melt were found to be very sensitive to experimental temperature. The bending strengths of 58.6 and 317.0 MPa were achieved at 1530 and 1570 °C, respectively. The sample made by infiltration of B–Si alloy was successfully sintered at 1530 °C. The relative density of the sample was more than 90%. The infiltration of B–Si alloy reduced the sintering temperature and the bending strength reached 326.9 MPa. The infiltration mechanism of B–Si alloy is discussed herein.
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spelling doaj.art-f51f3645be1d4e478de50df8052b376e2023-12-11T18:36:20ZengMDPI AGMaterials1996-19442021-02-01145109010.3390/ma14051090Environment-Friendly Preparation of Reaction-Bonded Silicon Carbide by Addition of Boron in the Silicon MeltMaoqiang Rui0Yaxiang Zhang1Jing Ye2School of Material Science and Engineering, Wuhan University of Technology, Wuhan 430070, ChinaSchool of Material Science and Engineering, Wuhan University of Technology, Wuhan 430070, ChinaSchool of Material Science and Engineering, Wuhan University of Technology, Wuhan 430070, ChinaReaction-bonded silicon carbide ceramics were sintered by infiltration of Si and B–Si alloy under an argon atmosphere at different temperatures. The element boron was added to the silicon melt to form a B–Si alloy first. The mechanical properties of samples were improved by infiltration of the B–Si melt. The samples infiltrated with the Si-only melt were found to be very sensitive to experimental temperature. The bending strengths of 58.6 and 317.0 MPa were achieved at 1530 and 1570 °C, respectively. The sample made by infiltration of B–Si alloy was successfully sintered at 1530 °C. The relative density of the sample was more than 90%. The infiltration of B–Si alloy reduced the sintering temperature and the bending strength reached 326.9 MPa. The infiltration mechanism of B–Si alloy is discussed herein.https://www.mdpi.com/1996-1944/14/5/1090reaction-bonded silicon carbideB–Si alloyinfiltration
spellingShingle Maoqiang Rui
Yaxiang Zhang
Jing Ye
Environment-Friendly Preparation of Reaction-Bonded Silicon Carbide by Addition of Boron in the Silicon Melt
Materials
reaction-bonded silicon carbide
B–Si alloy
infiltration
title Environment-Friendly Preparation of Reaction-Bonded Silicon Carbide by Addition of Boron in the Silicon Melt
title_full Environment-Friendly Preparation of Reaction-Bonded Silicon Carbide by Addition of Boron in the Silicon Melt
title_fullStr Environment-Friendly Preparation of Reaction-Bonded Silicon Carbide by Addition of Boron in the Silicon Melt
title_full_unstemmed Environment-Friendly Preparation of Reaction-Bonded Silicon Carbide by Addition of Boron in the Silicon Melt
title_short Environment-Friendly Preparation of Reaction-Bonded Silicon Carbide by Addition of Boron in the Silicon Melt
title_sort environment friendly preparation of reaction bonded silicon carbide by addition of boron in the silicon melt
topic reaction-bonded silicon carbide
B–Si alloy
infiltration
url https://www.mdpi.com/1996-1944/14/5/1090
work_keys_str_mv AT maoqiangrui environmentfriendlypreparationofreactionbondedsiliconcarbidebyadditionofboroninthesiliconmelt
AT yaxiangzhang environmentfriendlypreparationofreactionbondedsiliconcarbidebyadditionofboroninthesiliconmelt
AT jingye environmentfriendlypreparationofreactionbondedsiliconcarbidebyadditionofboroninthesiliconmelt