A New Supported Manganese-Based Coordination Complex as a Nano-Catalyst for the Synthesis of Indazolophthalazinetriones and Investigation of Its Antibacterial Activity
A new magnetic supported manganese-based coordination complex (Fe<sub>3</sub>O<sub>4</sub>@SiO<sub>2</sub>@CPTMS@MBOL@ Mn) was prepared in consecutive stages and characterized via various techniques (VSM, SEM, TEM, XRD, FT-IR, EDX, TG-DTA, and ICP). To evaluate it...
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MDPI AG
2021-07-01
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author | Maryam Ariannezhad Davood Habibi Somayyeh Heydari Vahideh Khorramabadi |
author_facet | Maryam Ariannezhad Davood Habibi Somayyeh Heydari Vahideh Khorramabadi |
author_sort | Maryam Ariannezhad |
collection | DOAJ |
description | A new magnetic supported manganese-based coordination complex (Fe<sub>3</sub>O<sub>4</sub>@SiO<sub>2</sub>@CPTMS@MBOL@ Mn) was prepared in consecutive stages and characterized via various techniques (VSM, SEM, TEM, XRD, FT-IR, EDX, TG-DTA, and ICP). To evaluate its application, it was used for synthesis of divers Indazolophthalazinetriones in a simple procedure via the one-pot three-component condensation reaction of aldehydes, dimedone, and phthalhydrazide in ethanol under reflux conditions. The Mn catalyst can be recycled without any noticeable loss in catalytic activity. Additionally, the antibacterial properties of the nano-catalyst were studied against some bacterial strains. |
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institution | Directory Open Access Journal |
issn | 2624-8549 |
language | English |
last_indexed | 2024-03-10T07:48:54Z |
publishDate | 2021-07-01 |
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spelling | doaj.art-f59e7529748046a9a6fa7609b2299d882023-11-22T12:28:04ZengMDPI AGChemistry2624-85492021-07-013378379910.3390/chemistry3030056A New Supported Manganese-Based Coordination Complex as a Nano-Catalyst for the Synthesis of Indazolophthalazinetriones and Investigation of Its Antibacterial ActivityMaryam Ariannezhad0Davood Habibi1Somayyeh Heydari2Vahideh Khorramabadi3Department of Organic Chemistry, Faculty of Chemistry, Bu-Ali Sina University, Hamedan 6517838683, IranDepartment of Organic Chemistry, Faculty of Chemistry, Bu-Ali Sina University, Hamedan 6517838683, IranDepartment of Organic Chemistry, Faculty of Chemistry, Bu-Ali Sina University, Hamedan 6517838683, IranDepartment of Organic Chemistry, Faculty of Chemistry, Bu-Ali Sina University, Hamedan 6517838683, IranA new magnetic supported manganese-based coordination complex (Fe<sub>3</sub>O<sub>4</sub>@SiO<sub>2</sub>@CPTMS@MBOL@ Mn) was prepared in consecutive stages and characterized via various techniques (VSM, SEM, TEM, XRD, FT-IR, EDX, TG-DTA, and ICP). To evaluate its application, it was used for synthesis of divers Indazolophthalazinetriones in a simple procedure via the one-pot three-component condensation reaction of aldehydes, dimedone, and phthalhydrazide in ethanol under reflux conditions. The Mn catalyst can be recycled without any noticeable loss in catalytic activity. Additionally, the antibacterial properties of the nano-catalyst were studied against some bacterial strains.https://www.mdpi.com/2624-8549/3/3/56aldehydedimedoneindazolophthalazinetrionephthalhydrazideMn-supported nano-catalyst |
spellingShingle | Maryam Ariannezhad Davood Habibi Somayyeh Heydari Vahideh Khorramabadi A New Supported Manganese-Based Coordination Complex as a Nano-Catalyst for the Synthesis of Indazolophthalazinetriones and Investigation of Its Antibacterial Activity Chemistry aldehyde dimedone indazolophthalazinetrione phthalhydrazide Mn-supported nano-catalyst |
title | A New Supported Manganese-Based Coordination Complex as a Nano-Catalyst for the Synthesis of Indazolophthalazinetriones and Investigation of Its Antibacterial Activity |
title_full | A New Supported Manganese-Based Coordination Complex as a Nano-Catalyst for the Synthesis of Indazolophthalazinetriones and Investigation of Its Antibacterial Activity |
title_fullStr | A New Supported Manganese-Based Coordination Complex as a Nano-Catalyst for the Synthesis of Indazolophthalazinetriones and Investigation of Its Antibacterial Activity |
title_full_unstemmed | A New Supported Manganese-Based Coordination Complex as a Nano-Catalyst for the Synthesis of Indazolophthalazinetriones and Investigation of Its Antibacterial Activity |
title_short | A New Supported Manganese-Based Coordination Complex as a Nano-Catalyst for the Synthesis of Indazolophthalazinetriones and Investigation of Its Antibacterial Activity |
title_sort | new supported manganese based coordination complex as a nano catalyst for the synthesis of indazolophthalazinetriones and investigation of its antibacterial activity |
topic | aldehyde dimedone indazolophthalazinetrione phthalhydrazide Mn-supported nano-catalyst |
url | https://www.mdpi.com/2624-8549/3/3/56 |
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