A New Supported Manganese-Based Coordination Complex as a Nano-Catalyst for the Synthesis of Indazolophthalazinetriones and Investigation of Its Antibacterial Activity

A new magnetic supported manganese-based coordination complex (Fe<sub>3</sub>O<sub>4</sub>@SiO<sub>2</sub>@CPTMS@MBOL@ Mn) was prepared in consecutive stages and characterized via various techniques (VSM, SEM, TEM, XRD, FT-IR, EDX, TG-DTA, and ICP). To evaluate it...

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Main Authors: Maryam Ariannezhad, Davood Habibi, Somayyeh Heydari, Vahideh Khorramabadi
Format: Article
Language:English
Published: MDPI AG 2021-07-01
Series:Chemistry
Subjects:
Online Access:https://www.mdpi.com/2624-8549/3/3/56
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author Maryam Ariannezhad
Davood Habibi
Somayyeh Heydari
Vahideh Khorramabadi
author_facet Maryam Ariannezhad
Davood Habibi
Somayyeh Heydari
Vahideh Khorramabadi
author_sort Maryam Ariannezhad
collection DOAJ
description A new magnetic supported manganese-based coordination complex (Fe<sub>3</sub>O<sub>4</sub>@SiO<sub>2</sub>@CPTMS@MBOL@ Mn) was prepared in consecutive stages and characterized via various techniques (VSM, SEM, TEM, XRD, FT-IR, EDX, TG-DTA, and ICP). To evaluate its application, it was used for synthesis of divers Indazolophthalazinetriones in a simple procedure via the one-pot three-component condensation reaction of aldehydes, dimedone, and phthalhydrazide in ethanol under reflux conditions. The Mn catalyst can be recycled without any noticeable loss in catalytic activity. Additionally, the antibacterial properties of the nano-catalyst were studied against some bacterial strains.
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spelling doaj.art-f59e7529748046a9a6fa7609b2299d882023-11-22T12:28:04ZengMDPI AGChemistry2624-85492021-07-013378379910.3390/chemistry3030056A New Supported Manganese-Based Coordination Complex as a Nano-Catalyst for the Synthesis of Indazolophthalazinetriones and Investigation of Its Antibacterial ActivityMaryam Ariannezhad0Davood Habibi1Somayyeh Heydari2Vahideh Khorramabadi3Department of Organic Chemistry, Faculty of Chemistry, Bu-Ali Sina University, Hamedan 6517838683, IranDepartment of Organic Chemistry, Faculty of Chemistry, Bu-Ali Sina University, Hamedan 6517838683, IranDepartment of Organic Chemistry, Faculty of Chemistry, Bu-Ali Sina University, Hamedan 6517838683, IranDepartment of Organic Chemistry, Faculty of Chemistry, Bu-Ali Sina University, Hamedan 6517838683, IranA new magnetic supported manganese-based coordination complex (Fe<sub>3</sub>O<sub>4</sub>@SiO<sub>2</sub>@CPTMS@MBOL@ Mn) was prepared in consecutive stages and characterized via various techniques (VSM, SEM, TEM, XRD, FT-IR, EDX, TG-DTA, and ICP). To evaluate its application, it was used for synthesis of divers Indazolophthalazinetriones in a simple procedure via the one-pot three-component condensation reaction of aldehydes, dimedone, and phthalhydrazide in ethanol under reflux conditions. The Mn catalyst can be recycled without any noticeable loss in catalytic activity. Additionally, the antibacterial properties of the nano-catalyst were studied against some bacterial strains.https://www.mdpi.com/2624-8549/3/3/56aldehydedimedoneindazolophthalazinetrionephthalhydrazideMn-supported nano-catalyst
spellingShingle Maryam Ariannezhad
Davood Habibi
Somayyeh Heydari
Vahideh Khorramabadi
A New Supported Manganese-Based Coordination Complex as a Nano-Catalyst for the Synthesis of Indazolophthalazinetriones and Investigation of Its Antibacterial Activity
Chemistry
aldehyde
dimedone
indazolophthalazinetrione
phthalhydrazide
Mn-supported nano-catalyst
title A New Supported Manganese-Based Coordination Complex as a Nano-Catalyst for the Synthesis of Indazolophthalazinetriones and Investigation of Its Antibacterial Activity
title_full A New Supported Manganese-Based Coordination Complex as a Nano-Catalyst for the Synthesis of Indazolophthalazinetriones and Investigation of Its Antibacterial Activity
title_fullStr A New Supported Manganese-Based Coordination Complex as a Nano-Catalyst for the Synthesis of Indazolophthalazinetriones and Investigation of Its Antibacterial Activity
title_full_unstemmed A New Supported Manganese-Based Coordination Complex as a Nano-Catalyst for the Synthesis of Indazolophthalazinetriones and Investigation of Its Antibacterial Activity
title_short A New Supported Manganese-Based Coordination Complex as a Nano-Catalyst for the Synthesis of Indazolophthalazinetriones and Investigation of Its Antibacterial Activity
title_sort new supported manganese based coordination complex as a nano catalyst for the synthesis of indazolophthalazinetriones and investigation of its antibacterial activity
topic aldehyde
dimedone
indazolophthalazinetrione
phthalhydrazide
Mn-supported nano-catalyst
url https://www.mdpi.com/2624-8549/3/3/56
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