Alkylresorcinols in rye (Secale cereale L.) grains. V. Chromatographic analysis of 5-n-alk(en)ylresorcinols during their preparation

Analysis of 5-n-alk(en)ylresorcinols during the coarse of their preparation from rye grains showed that changes of the composition of 5-n-alkylresorcinol homologues in acetone oil; raw preparation, and alkylresorcinol fraiction obtained after chromatography on silica gel, were insignificant. About 2...

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Main Authors: Arkadiusz Kozubek, Franciszek Tłuścik, Wanda Mejbaum-Katzenellenebogen
Format: Article
Language:English
Published: Polish Botanical Society 2014-01-01
Series:Acta Societatis Botanicorum Poloniae
Online Access:https://pbsociety.org.pl/journals/index.php/asbp/article/view/3275
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author Arkadiusz Kozubek
Franciszek Tłuścik
Wanda Mejbaum-Katzenellenebogen
author_facet Arkadiusz Kozubek
Franciszek Tłuścik
Wanda Mejbaum-Katzenellenebogen
author_sort Arkadiusz Kozubek
collection DOAJ
description Analysis of 5-n-alk(en)ylresorcinols during the coarse of their preparation from rye grains showed that changes of the composition of 5-n-alkylresorcinol homologues in acetone oil; raw preparation, and alkylresorcinol fraiction obtained after chromatography on silica gel, were insignificant. About 20% of alk(en)-ylresorcinals were washed out from acetone oil with pentane. Over 50% of alk(en)ylresorcinols eluted by pentane constituted homologues with unsaturated hydrocarbon chains (5-n-alkenylresorcinols). Preparation obtained after chromatagraphic separation constituted a mixtureof 5-n-alk(en)ylresorcinols width saturated hydrocarbon chains (5-n-alkylresorcinols).
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spelling doaj.art-f60fa55555a44854bb5977685b05b2172022-12-21T23:11:01ZengPolish Botanical SocietyActa Societatis Botanicorum Poloniae2083-94802014-01-0150463764310.5586/asbp.1981.0852753Alkylresorcinols in rye (Secale cereale L.) grains. V. Chromatographic analysis of 5-n-alk(en)ylresorcinols during their preparationArkadiusz Kozubek0Franciszek Tłuścik1Wanda Mejbaum-Katzenellenebogen2Wrocław UniversityWrocław UniversityWrocław UniversityAnalysis of 5-n-alk(en)ylresorcinols during the coarse of their preparation from rye grains showed that changes of the composition of 5-n-alkylresorcinol homologues in acetone oil; raw preparation, and alkylresorcinol fraiction obtained after chromatography on silica gel, were insignificant. About 20% of alk(en)-ylresorcinals were washed out from acetone oil with pentane. Over 50% of alk(en)ylresorcinols eluted by pentane constituted homologues with unsaturated hydrocarbon chains (5-n-alkenylresorcinols). Preparation obtained after chromatagraphic separation constituted a mixtureof 5-n-alk(en)ylresorcinols width saturated hydrocarbon chains (5-n-alkylresorcinols).https://pbsociety.org.pl/journals/index.php/asbp/article/view/3275
spellingShingle Arkadiusz Kozubek
Franciszek Tłuścik
Wanda Mejbaum-Katzenellenebogen
Alkylresorcinols in rye (Secale cereale L.) grains. V. Chromatographic analysis of 5-n-alk(en)ylresorcinols during their preparation
Acta Societatis Botanicorum Poloniae
title Alkylresorcinols in rye (Secale cereale L.) grains. V. Chromatographic analysis of 5-n-alk(en)ylresorcinols during their preparation
title_full Alkylresorcinols in rye (Secale cereale L.) grains. V. Chromatographic analysis of 5-n-alk(en)ylresorcinols during their preparation
title_fullStr Alkylresorcinols in rye (Secale cereale L.) grains. V. Chromatographic analysis of 5-n-alk(en)ylresorcinols during their preparation
title_full_unstemmed Alkylresorcinols in rye (Secale cereale L.) grains. V. Chromatographic analysis of 5-n-alk(en)ylresorcinols during their preparation
title_short Alkylresorcinols in rye (Secale cereale L.) grains. V. Chromatographic analysis of 5-n-alk(en)ylresorcinols during their preparation
title_sort alkylresorcinols in rye secale cereale l grains v chromatographic analysis of 5 n alk en ylresorcinols during their preparation
url https://pbsociety.org.pl/journals/index.php/asbp/article/view/3275
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AT franciszektłuscik alkylresorcinolsinryesecalecerealelgrainsvchromatographicanalysisof5nalkenylresorcinolsduringtheirpreparation
AT wandamejbaumkatzenellenebogen alkylresorcinolsinryesecalecerealelgrainsvchromatographicanalysisof5nalkenylresorcinolsduringtheirpreparation