Alkylresorcinols in rye (Secale cereale L.) grains. V. Chromatographic analysis of 5-n-alk(en)ylresorcinols during their preparation
Analysis of 5-n-alk(en)ylresorcinols during the coarse of their preparation from rye grains showed that changes of the composition of 5-n-alkylresorcinol homologues in acetone oil; raw preparation, and alkylresorcinol fraiction obtained after chromatography on silica gel, were insignificant. About 2...
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Format: | Article |
Language: | English |
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Polish Botanical Society
2014-01-01
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Series: | Acta Societatis Botanicorum Poloniae |
Online Access: | https://pbsociety.org.pl/journals/index.php/asbp/article/view/3275 |
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author | Arkadiusz Kozubek Franciszek Tłuścik Wanda Mejbaum-Katzenellenebogen |
author_facet | Arkadiusz Kozubek Franciszek Tłuścik Wanda Mejbaum-Katzenellenebogen |
author_sort | Arkadiusz Kozubek |
collection | DOAJ |
description | Analysis of 5-n-alk(en)ylresorcinols during the coarse of their preparation from rye grains showed that changes of the composition of 5-n-alkylresorcinol homologues in acetone oil; raw preparation, and alkylresorcinol fraiction obtained after chromatography on silica gel, were insignificant. About 20% of alk(en)-ylresorcinals were washed out from acetone oil with pentane. Over 50% of alk(en)ylresorcinols eluted by pentane constituted homologues with unsaturated hydrocarbon chains (5-n-alkenylresorcinols). Preparation obtained after chromatagraphic separation constituted a mixtureof 5-n-alk(en)ylresorcinols width saturated hydrocarbon chains (5-n-alkylresorcinols). |
first_indexed | 2024-12-14T07:41:56Z |
format | Article |
id | doaj.art-f60fa55555a44854bb5977685b05b217 |
institution | Directory Open Access Journal |
issn | 2083-9480 |
language | English |
last_indexed | 2024-12-14T07:41:56Z |
publishDate | 2014-01-01 |
publisher | Polish Botanical Society |
record_format | Article |
series | Acta Societatis Botanicorum Poloniae |
spelling | doaj.art-f60fa55555a44854bb5977685b05b2172022-12-21T23:11:01ZengPolish Botanical SocietyActa Societatis Botanicorum Poloniae2083-94802014-01-0150463764310.5586/asbp.1981.0852753Alkylresorcinols in rye (Secale cereale L.) grains. V. Chromatographic analysis of 5-n-alk(en)ylresorcinols during their preparationArkadiusz Kozubek0Franciszek Tłuścik1Wanda Mejbaum-Katzenellenebogen2Wrocław UniversityWrocław UniversityWrocław UniversityAnalysis of 5-n-alk(en)ylresorcinols during the coarse of their preparation from rye grains showed that changes of the composition of 5-n-alkylresorcinol homologues in acetone oil; raw preparation, and alkylresorcinol fraiction obtained after chromatography on silica gel, were insignificant. About 20% of alk(en)-ylresorcinals were washed out from acetone oil with pentane. Over 50% of alk(en)ylresorcinols eluted by pentane constituted homologues with unsaturated hydrocarbon chains (5-n-alkenylresorcinols). Preparation obtained after chromatagraphic separation constituted a mixtureof 5-n-alk(en)ylresorcinols width saturated hydrocarbon chains (5-n-alkylresorcinols).https://pbsociety.org.pl/journals/index.php/asbp/article/view/3275 |
spellingShingle | Arkadiusz Kozubek Franciszek Tłuścik Wanda Mejbaum-Katzenellenebogen Alkylresorcinols in rye (Secale cereale L.) grains. V. Chromatographic analysis of 5-n-alk(en)ylresorcinols during their preparation Acta Societatis Botanicorum Poloniae |
title | Alkylresorcinols in rye (Secale cereale L.) grains. V. Chromatographic analysis of 5-n-alk(en)ylresorcinols during their preparation |
title_full | Alkylresorcinols in rye (Secale cereale L.) grains. V. Chromatographic analysis of 5-n-alk(en)ylresorcinols during their preparation |
title_fullStr | Alkylresorcinols in rye (Secale cereale L.) grains. V. Chromatographic analysis of 5-n-alk(en)ylresorcinols during their preparation |
title_full_unstemmed | Alkylresorcinols in rye (Secale cereale L.) grains. V. Chromatographic analysis of 5-n-alk(en)ylresorcinols during their preparation |
title_short | Alkylresorcinols in rye (Secale cereale L.) grains. V. Chromatographic analysis of 5-n-alk(en)ylresorcinols during their preparation |
title_sort | alkylresorcinols in rye secale cereale l grains v chromatographic analysis of 5 n alk en ylresorcinols during their preparation |
url | https://pbsociety.org.pl/journals/index.php/asbp/article/view/3275 |
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