Microstructure and mechanical properties of NbC–Ni cermets prepared by microwave sintering

This study shows the application of microwave sintering (MS) on preparing NbC–10Ni and NbC–12Ni cermets, as well as the effect of its microstructure, phase formation, and mechanical properties. Results indicated that NbC–Ni cermets with a fine and uniform structure can be obtained by MS in a relativ...

Full description

Bibliographic Details
Main Authors: Tang Siwen, Zhang Hao, Yang Zhifu, Liu Qian, Lv Zheng, Ouyang Cong, Qiu Xinyi
Format: Article
Language:English
Published: De Gruyter 2022-08-01
Series:High Temperature Materials and Processes
Subjects:
Online Access:https://doi.org/10.1515/htmp-2022-0049
_version_ 1828108534151118848
author Tang Siwen
Zhang Hao
Yang Zhifu
Liu Qian
Lv Zheng
Ouyang Cong
Qiu Xinyi
author_facet Tang Siwen
Zhang Hao
Yang Zhifu
Liu Qian
Lv Zheng
Ouyang Cong
Qiu Xinyi
author_sort Tang Siwen
collection DOAJ
description This study shows the application of microwave sintering (MS) on preparing NbC–10Ni and NbC–12Ni cermets, as well as the effect of its microstructure, phase formation, and mechanical properties. Results indicated that NbC–Ni cermets with a fine and uniform structure can be obtained by MS in a relatively short time. And the sintering temperature greatly influenced the microstructure and mechanical properties of NbC–Ni cermets, whereas the effect of dwell time is relatively small. With the increase of the sintering temperature, the microstructure of NbC–Ni cermets experienced sintering densification and grain growth. The strength and toughness increased first and then decreased, and the hardness increased with the increase of sintering temperature. According to the comprehensive mechanical properties, the optimized sintering process is 1,390°C and the dwell time is 15 min. At this time, no new phase formed, but the diffraction peak of the Ni phase shifted. Through analysis, it is found that the improvement mechanisms for comprehensive mechanical properties of NbC–Ni cermets mainly include grain refinement, crack deflection and bridging, and energy absorption of the ductile phase of Ni.
first_indexed 2024-04-11T10:47:11Z
format Article
id doaj.art-f6d6bb9c715e4f2fbfdfe8abee3a9a5d
institution Directory Open Access Journal
issn 2191-0324
language English
last_indexed 2024-04-11T10:47:11Z
publishDate 2022-08-01
publisher De Gruyter
record_format Article
series High Temperature Materials and Processes
spelling doaj.art-f6d6bb9c715e4f2fbfdfe8abee3a9a5d2022-12-22T04:29:00ZengDe GruyterHigh Temperature Materials and Processes2191-03242022-08-0141148249210.1515/htmp-2022-0049Microstructure and mechanical properties of NbC–Ni cermets prepared by microwave sinteringTang Siwen0Zhang Hao1Yang Zhifu2Liu Qian3Lv Zheng4Ouyang Cong5Qiu Xinyi6Hunan Provincial Key Laboratory of Health Maintenance for Mechanical Equipment, Hunan University of Science and Technology, Xiangtan 411201, ChinaHunan Provincial Key Laboratory of Health Maintenance for Mechanical Equipment, Hunan University of Science and Technology, Xiangtan 411201, ChinaHunan Provincial Key Laboratory of Health Maintenance for Mechanical Equipment, Hunan University of Science and Technology, Xiangtan 411201, ChinaEngineering Research Center of Mineral Resources Development Technology and Equipment for Deep Sea and Deep Earth, Ministry of Education, Hunan University of Science and Technology, Xiangtan 411201, ChinaEngineering Research Center of Mineral Resources Development Technology and Equipment for Deep Sea and Deep Earth, Ministry of Education, Hunan University of Science and Technology, Xiangtan 411201, ChinaEngineering Research Center of Mineral Resources Development Technology and Equipment for Deep Sea and Deep Earth, Ministry of Education, Hunan University of Science and Technology, Xiangtan 411201, ChinaHunan Provincial Key Laboratory of High Efficiency and Precision Machining of Difficult-to-Cut Material, Hunan University of Science and Technology, Xiangtan 411201, ChinaThis study shows the application of microwave sintering (MS) on preparing NbC–10Ni and NbC–12Ni cermets, as well as the effect of its microstructure, phase formation, and mechanical properties. Results indicated that NbC–Ni cermets with a fine and uniform structure can be obtained by MS in a relatively short time. And the sintering temperature greatly influenced the microstructure and mechanical properties of NbC–Ni cermets, whereas the effect of dwell time is relatively small. With the increase of the sintering temperature, the microstructure of NbC–Ni cermets experienced sintering densification and grain growth. The strength and toughness increased first and then decreased, and the hardness increased with the increase of sintering temperature. According to the comprehensive mechanical properties, the optimized sintering process is 1,390°C and the dwell time is 15 min. At this time, no new phase formed, but the diffraction peak of the Ni phase shifted. Through analysis, it is found that the improvement mechanisms for comprehensive mechanical properties of NbC–Ni cermets mainly include grain refinement, crack deflection and bridging, and energy absorption of the ductile phase of Ni.https://doi.org/10.1515/htmp-2022-0049nbc–ni cermetsmicrowave sinteringmicrostructuremechanical property
spellingShingle Tang Siwen
Zhang Hao
Yang Zhifu
Liu Qian
Lv Zheng
Ouyang Cong
Qiu Xinyi
Microstructure and mechanical properties of NbC–Ni cermets prepared by microwave sintering
High Temperature Materials and Processes
nbc–ni cermets
microwave sintering
microstructure
mechanical property
title Microstructure and mechanical properties of NbC–Ni cermets prepared by microwave sintering
title_full Microstructure and mechanical properties of NbC–Ni cermets prepared by microwave sintering
title_fullStr Microstructure and mechanical properties of NbC–Ni cermets prepared by microwave sintering
title_full_unstemmed Microstructure and mechanical properties of NbC–Ni cermets prepared by microwave sintering
title_short Microstructure and mechanical properties of NbC–Ni cermets prepared by microwave sintering
title_sort microstructure and mechanical properties of nbc ni cermets prepared by microwave sintering
topic nbc–ni cermets
microwave sintering
microstructure
mechanical property
url https://doi.org/10.1515/htmp-2022-0049
work_keys_str_mv AT tangsiwen microstructureandmechanicalpropertiesofnbcnicermetspreparedbymicrowavesintering
AT zhanghao microstructureandmechanicalpropertiesofnbcnicermetspreparedbymicrowavesintering
AT yangzhifu microstructureandmechanicalpropertiesofnbcnicermetspreparedbymicrowavesintering
AT liuqian microstructureandmechanicalpropertiesofnbcnicermetspreparedbymicrowavesintering
AT lvzheng microstructureandmechanicalpropertiesofnbcnicermetspreparedbymicrowavesintering
AT ouyangcong microstructureandmechanicalpropertiesofnbcnicermetspreparedbymicrowavesintering
AT qiuxinyi microstructureandmechanicalpropertiesofnbcnicermetspreparedbymicrowavesintering