Microstructure and properties of SiC fibers coated with BN coating at different oxidation temperatures

The BN coating was deposited on the surface of typical domestic SiC fibers by chemical vapor permeation (CVI) process, and the fibers were oxidized at 800-1200 ℃ for 1 h. The morphology, structure and composition of BN coated SiC fibers after oxidation were characterized. The property changes of BN...

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Main Authors: ZHAO Wenqing, QI Zhe, SHI Xiaolei, WANG Yana, JIANG Zhuoyu, JIAO Jian
Format: Article
Language:zho
Published: Journal of Materials Engineering 2023-07-01
Series:Cailiao gongcheng
Subjects:
Online Access:http://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2022.001041
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author ZHAO Wenqing
QI Zhe
SHI Xiaolei
WANG Yana
JIANG Zhuoyu
JIAO Jian
author_facet ZHAO Wenqing
QI Zhe
SHI Xiaolei
WANG Yana
JIANG Zhuoyu
JIAO Jian
author_sort ZHAO Wenqing
collection DOAJ
description The BN coating was deposited on the surface of typical domestic SiC fibers by chemical vapor permeation (CVI) process, and the fibers were oxidized at 800-1200 ℃ for 1 h. The morphology, structure and composition of BN coated SiC fibers after oxidation were characterized. The property changes of BN coated SiC fibers after oxidation were evaluated by tensile strength of monofilament. The results show that when the oxidation temperature is lower than 1000 ℃, the BN coating and its oxide can effectively prevent the erosion of the inner SiC fibers by O2, and when the temperature continues to rise, the SiC fibers are oxidized. With the increase of oxidation temperature, the surface oxide of BN coated SiC fibers goes through the process of α-B2O3→SiCxOy→amorphous SiO2. The tensile strength of BN coated SiC fibers decreases with the increase of oxidation temperature. Direct exposure of BN coating to oxidizing environments reduces the oxidation resistance of SiC fibers. The failure source of fiber fracture first transitions from BN coating defects to B2O3 oxide layer defects and finally evolves into SiO2 oxide layer porosity defects.
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spelling doaj.art-f6e9482fa7954858869b8c69d53b76362024-02-02T00:45:50ZzhoJournal of Materials EngineeringCailiao gongcheng1001-43812023-07-0151712713510.11868/j.issn.1001-4381.2022.00104120230712Microstructure and properties of SiC fibers coated with BN coating at different oxidation temperaturesZHAO Wenqing0QI Zhe1SHI Xiaolei2WANG Yana3JIANG Zhuoyu4JIAO Jian5Surface Engineering Division, AECC Beijing Institute of Aeronautical Materials, Beijing 100095, ChinaSurface Engineering Division, AECC Beijing Institute of Aeronautical Materials, Beijing 100095, ChinaSurface Engineering Division, AECC Beijing Institute of Aeronautical Materials, Beijing 100095, ChinaSurface Engineering Division, AECC Beijing Institute of Aeronautical Materials, Beijing 100095, ChinaSurface Engineering Division, AECC Beijing Institute of Aeronautical Materials, Beijing 100095, ChinaSurface Engineering Division, AECC Beijing Institute of Aeronautical Materials, Beijing 100095, ChinaThe BN coating was deposited on the surface of typical domestic SiC fibers by chemical vapor permeation (CVI) process, and the fibers were oxidized at 800-1200 ℃ for 1 h. The morphology, structure and composition of BN coated SiC fibers after oxidation were characterized. The property changes of BN coated SiC fibers after oxidation were evaluated by tensile strength of monofilament. The results show that when the oxidation temperature is lower than 1000 ℃, the BN coating and its oxide can effectively prevent the erosion of the inner SiC fibers by O2, and when the temperature continues to rise, the SiC fibers are oxidized. With the increase of oxidation temperature, the surface oxide of BN coated SiC fibers goes through the process of α-B2O3→SiCxOy→amorphous SiO2. The tensile strength of BN coated SiC fibers decreases with the increase of oxidation temperature. Direct exposure of BN coating to oxidizing environments reduces the oxidation resistance of SiC fibers. The failure source of fiber fracture first transitions from BN coating defects to B2O3 oxide layer defects and finally evolves into SiO2 oxide layer porosity defects.http://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2022.001041sic fiberbn coatingoxidationmonofilament tensile
spellingShingle ZHAO Wenqing
QI Zhe
SHI Xiaolei
WANG Yana
JIANG Zhuoyu
JIAO Jian
Microstructure and properties of SiC fibers coated with BN coating at different oxidation temperatures
Cailiao gongcheng
sic fiber
bn coating
oxidation
monofilament tensile
title Microstructure and properties of SiC fibers coated with BN coating at different oxidation temperatures
title_full Microstructure and properties of SiC fibers coated with BN coating at different oxidation temperatures
title_fullStr Microstructure and properties of SiC fibers coated with BN coating at different oxidation temperatures
title_full_unstemmed Microstructure and properties of SiC fibers coated with BN coating at different oxidation temperatures
title_short Microstructure and properties of SiC fibers coated with BN coating at different oxidation temperatures
title_sort microstructure and properties of sic fibers coated with bn coating at different oxidation temperatures
topic sic fiber
bn coating
oxidation
monofilament tensile
url http://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2022.001041
work_keys_str_mv AT zhaowenqing microstructureandpropertiesofsicfiberscoatedwithbncoatingatdifferentoxidationtemperatures
AT qizhe microstructureandpropertiesofsicfiberscoatedwithbncoatingatdifferentoxidationtemperatures
AT shixiaolei microstructureandpropertiesofsicfiberscoatedwithbncoatingatdifferentoxidationtemperatures
AT wangyana microstructureandpropertiesofsicfiberscoatedwithbncoatingatdifferentoxidationtemperatures
AT jiangzhuoyu microstructureandpropertiesofsicfiberscoatedwithbncoatingatdifferentoxidationtemperatures
AT jiaojian microstructureandpropertiesofsicfiberscoatedwithbncoatingatdifferentoxidationtemperatures