An Efficient and One Spot Synthesis of Silica Supported Synthesis of Fluorinated 1,3,4-Thiadiazole Derivative Under Microwave Irradiation
An efficient and one pot reaction of fluorinated 1,3,4-Thiadiazole derivatives was synthesis by fluorinated aromatic carboxylic with thiosemicabazide in the presence of phosphorus oxychloride as a catalyst under Microwave irradiation with silica supported. The synthesis compound was characterized...
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| Format: | Article |
| Language: | English |
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PURKH
2020-06-01
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| Series: | To Chemistry Journal |
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| Online Access: | https://purkh.com/index.php/tochem/article/view/789 |
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| author | Bharat K Dhotre Bhagwan Singh Dobhalb Santosh Raut Amol Kalea Pathan Mohd Arif |
| author_facet | Bharat K Dhotre Bhagwan Singh Dobhalb Santosh Raut Amol Kalea Pathan Mohd Arif |
| author_sort | Bharat K Dhotre |
| collection | DOAJ |
| description | An efficient and one pot reaction of fluorinated 1,3,4-Thiadiazole derivatives was synthesis by fluorinated aromatic carboxylic with thiosemicabazide in the presence of phosphorus oxychloride as a catalyst under Microwave irradiation with silica supported. The synthesis compound was characterized by 1H NMR, IR, and mass spectroscopic techniques. The present approach offers the advantages such as short reaction time, simplicity of the workup procedure, low cost and mild reaction condition. |
| first_indexed | 2024-12-18T14:19:51Z |
| format | Article |
| id | doaj.art-f7088f3462974e33b13dee611b9830ff |
| institution | Directory Open Access Journal |
| issn | 2581-7507 |
| language | English |
| last_indexed | 2024-12-18T14:19:51Z |
| publishDate | 2020-06-01 |
| publisher | PURKH |
| record_format | Article |
| series | To Chemistry Journal |
| spelling | doaj.art-f7088f3462974e33b13dee611b9830ff2022-12-21T21:04:54ZengPURKHTo Chemistry Journal2581-75072020-06-016An Efficient and One Spot Synthesis of Silica Supported Synthesis of Fluorinated 1,3,4-Thiadiazole Derivative Under Microwave IrradiationBharat K Dhotre0Bhagwan Singh Dobhalb1Santosh Raut2Amol Kalea3Pathan Mohd Arif 4Swami Vivekanand Senior College, Mantha, Jalna, Maharashtra, IndiaBadrinarayan Barwale Mahavidyalaya, Jalna, IndiaMaulana Azad College, Aurangabad, Maharashtra, IndiaSwami Vivekanand Senior College, Mantha, Jalna, Maharashtra, IndiaMaulana Azad College, Aurangabad, Maharashtra, IndiaAn efficient and one pot reaction of fluorinated 1,3,4-Thiadiazole derivatives was synthesis by fluorinated aromatic carboxylic with thiosemicabazide in the presence of phosphorus oxychloride as a catalyst under Microwave irradiation with silica supported. The synthesis compound was characterized by 1H NMR, IR, and mass spectroscopic techniques. The present approach offers the advantages such as short reaction time, simplicity of the workup procedure, low cost and mild reaction condition.https://purkh.com/index.php/tochem/article/view/789Microwave irradiationSilica supportedthiosemicarbazide |
| spellingShingle | Bharat K Dhotre Bhagwan Singh Dobhalb Santosh Raut Amol Kalea Pathan Mohd Arif An Efficient and One Spot Synthesis of Silica Supported Synthesis of Fluorinated 1,3,4-Thiadiazole Derivative Under Microwave Irradiation To Chemistry Journal Microwave irradiation Silica supported thiosemicarbazide |
| title | An Efficient and One Spot Synthesis of Silica Supported Synthesis of Fluorinated 1,3,4-Thiadiazole Derivative Under Microwave Irradiation |
| title_full | An Efficient and One Spot Synthesis of Silica Supported Synthesis of Fluorinated 1,3,4-Thiadiazole Derivative Under Microwave Irradiation |
| title_fullStr | An Efficient and One Spot Synthesis of Silica Supported Synthesis of Fluorinated 1,3,4-Thiadiazole Derivative Under Microwave Irradiation |
| title_full_unstemmed | An Efficient and One Spot Synthesis of Silica Supported Synthesis of Fluorinated 1,3,4-Thiadiazole Derivative Under Microwave Irradiation |
| title_short | An Efficient and One Spot Synthesis of Silica Supported Synthesis of Fluorinated 1,3,4-Thiadiazole Derivative Under Microwave Irradiation |
| title_sort | efficient and one spot synthesis of silica supported synthesis of fluorinated 1 3 4 thiadiazole derivative under microwave irradiation |
| topic | Microwave irradiation Silica supported thiosemicarbazide |
| url | https://purkh.com/index.php/tochem/article/view/789 |
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