Effect of homogenization on microstructure evolution and mechanical properties of aged Mg-Nd-Sm-Zn-Zr alloy

As an indispensable pre-treatment for aging, homogenization treatment has a significant effect on precipitation behavior of the Mg-RE alloys. Herein, the influence of homogenization temperature on the microstructure evolution and mechanical performance of a novel Mg-2.0Nd-2.0Sm-0.4Zn-0.4Zr (wt.%) al...

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Main Authors: Tao Ma, Sicong Zhao, Liping Wang, Zhiwei Wang, Erjun Guo, Yicheng Feng, Dongrong Liu, Changtong Wu, Jingfang Li
Format: Article
Language:English
Published: IOP Publishing 2021-01-01
Series:Materials Research Express
Subjects:
Online Access:https://doi.org/10.1088/2053-1591/ac3fdb
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author Tao Ma
Sicong Zhao
Liping Wang
Zhiwei Wang
Erjun Guo
Yicheng Feng
Dongrong Liu
Changtong Wu
Jingfang Li
author_facet Tao Ma
Sicong Zhao
Liping Wang
Zhiwei Wang
Erjun Guo
Yicheng Feng
Dongrong Liu
Changtong Wu
Jingfang Li
author_sort Tao Ma
collection DOAJ
description As an indispensable pre-treatment for aging, homogenization treatment has a significant effect on precipitation behavior of the Mg-RE alloys. Herein, the influence of homogenization temperature on the microstructure evolution and mechanical performance of a novel Mg-2.0Nd-2.0Sm-0.4Zn-0.4Zr (wt.%) alloy has been studied systematically. The results indicated that the as-cast alloy was mainly composed of α -Mg matrix, β -Mg _12 (Nd,Sm,Zn) phase and Zr-containing particles. Upon increasing the homogenization temperature from 500 °C to 525 °C for 8 h, the average grain size of as-homogenized alloy increased from 76 μ m to 156 μ m, and the content of β phase decreased gradually. It was worth noting that the homogenization temperature exceeded 515 °C, the β phase at the grain boundaries was completely dissolved. After aging at 200 °C for 18 h, numerous of plate-like β ′ phases were observed in α -Mg matrix. The rise in homogenization temperature was conducive to nucleation and growth of the β ′ phase. However, excessive homogenization temperature significantly coarsened grain size. The aged alloy under homogenization treatment at 515 °C for 8 h achieved optimal mechanical properties. The values of ultimate tensile strength, yield strength and elongation were 261 MPa, 154 MPa and 5.8%, respectively. The fracture mode of the aged alloy mainly exhibited a typical transgranular cleavage fracture.
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spelling doaj.art-f7ec125358234412862b4e475aebdaae2023-08-09T15:58:50ZengIOP PublishingMaterials Research Express2053-15912021-01-0181212651510.1088/2053-1591/ac3fdbEffect of homogenization on microstructure evolution and mechanical properties of aged Mg-Nd-Sm-Zn-Zr alloyTao Ma0Sicong Zhao1https://orcid.org/0000-0003-0689-399XLiping Wang2https://orcid.org/0000-0002-6856-7527Zhiwei Wang3Erjun Guo4Yicheng Feng5https://orcid.org/0000-0002-4562-5827Dongrong Liu6Changtong Wu7Jingfang Li8https://orcid.org/0000-0002-7674-516XSchool of Material Science and Chemical Engineering, Harbin University of Science and Technology , Harbin150040, People’s Republic of China; Key Laboratory of Advanced Manufacturing and Intelligent Technology (MOE), Harbin University of Science and Technology , Harbin150040, People’s Republic of ChinaSchool of Material Science and Chemical Engineering, Harbin University of Science and Technology , Harbin150040, People’s Republic of China; Key Laboratory of Advanced Manufacturing and Intelligent Technology (MOE), Harbin University of Science and Technology , Harbin150040, People’s Republic of ChinaSchool of Material Science and Chemical Engineering, Harbin University of Science and Technology , Harbin150040, People’s Republic of China; Key Laboratory of Advanced Manufacturing and Intelligent Technology (MOE), Harbin University of Science and Technology , Harbin150040, People’s Republic of ChinaAECC Harbin Dongan Engine Co., Ltd, Harbin150000, People’s Republic of ChinaSchool of Material Science and Chemical Engineering, Harbin University of Science and Technology , Harbin150040, People’s Republic of China; Key Laboratory of Advanced Manufacturing and Intelligent Technology (MOE), Harbin University of Science and Technology , Harbin150040, People’s Republic of ChinaSchool of Material Science and Chemical Engineering, Harbin University of Science and Technology , Harbin150040, People’s Republic of China; Key Laboratory of Advanced Manufacturing and Intelligent Technology (MOE), Harbin University of Science and Technology , Harbin150040, People’s Republic of ChinaSchool of Material Science and Chemical Engineering, Harbin University of Science and Technology , Harbin150040, People’s Republic of China; Key Laboratory of Advanced Manufacturing and Intelligent Technology (MOE), Harbin University of Science and Technology , Harbin150040, People’s Republic of ChinaSchool of Material Science and Chemical Engineering, Harbin University of Science and Technology , Harbin150040, People’s Republic of China; Key Laboratory of Advanced Manufacturing and Intelligent Technology (MOE), Harbin University of Science and Technology , Harbin150040, People’s Republic of ChinaKey Laboratory of Functional Inorganic Material Chemistry (MOE), School of Chemistry and Materials Science, Heilongjiang University, Harbin, 150080, People’s Republic of ChinaAs an indispensable pre-treatment for aging, homogenization treatment has a significant effect on precipitation behavior of the Mg-RE alloys. Herein, the influence of homogenization temperature on the microstructure evolution and mechanical performance of a novel Mg-2.0Nd-2.0Sm-0.4Zn-0.4Zr (wt.%) alloy has been studied systematically. The results indicated that the as-cast alloy was mainly composed of α -Mg matrix, β -Mg _12 (Nd,Sm,Zn) phase and Zr-containing particles. Upon increasing the homogenization temperature from 500 °C to 525 °C for 8 h, the average grain size of as-homogenized alloy increased from 76 μ m to 156 μ m, and the content of β phase decreased gradually. It was worth noting that the homogenization temperature exceeded 515 °C, the β phase at the grain boundaries was completely dissolved. After aging at 200 °C for 18 h, numerous of plate-like β ′ phases were observed in α -Mg matrix. The rise in homogenization temperature was conducive to nucleation and growth of the β ′ phase. However, excessive homogenization temperature significantly coarsened grain size. The aged alloy under homogenization treatment at 515 °C for 8 h achieved optimal mechanical properties. The values of ultimate tensile strength, yield strength and elongation were 261 MPa, 154 MPa and 5.8%, respectively. The fracture mode of the aged alloy mainly exhibited a typical transgranular cleavage fracture.https://doi.org/10.1088/2053-1591/ac3fdbMg-Nd-Sm-Zn-Zr alloyhomogenization temperaturemicrostructure evolutionmechanical properties
spellingShingle Tao Ma
Sicong Zhao
Liping Wang
Zhiwei Wang
Erjun Guo
Yicheng Feng
Dongrong Liu
Changtong Wu
Jingfang Li
Effect of homogenization on microstructure evolution and mechanical properties of aged Mg-Nd-Sm-Zn-Zr alloy
Materials Research Express
Mg-Nd-Sm-Zn-Zr alloy
homogenization temperature
microstructure evolution
mechanical properties
title Effect of homogenization on microstructure evolution and mechanical properties of aged Mg-Nd-Sm-Zn-Zr alloy
title_full Effect of homogenization on microstructure evolution and mechanical properties of aged Mg-Nd-Sm-Zn-Zr alloy
title_fullStr Effect of homogenization on microstructure evolution and mechanical properties of aged Mg-Nd-Sm-Zn-Zr alloy
title_full_unstemmed Effect of homogenization on microstructure evolution and mechanical properties of aged Mg-Nd-Sm-Zn-Zr alloy
title_short Effect of homogenization on microstructure evolution and mechanical properties of aged Mg-Nd-Sm-Zn-Zr alloy
title_sort effect of homogenization on microstructure evolution and mechanical properties of aged mg nd sm zn zr alloy
topic Mg-Nd-Sm-Zn-Zr alloy
homogenization temperature
microstructure evolution
mechanical properties
url https://doi.org/10.1088/2053-1591/ac3fdb
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