An Exploration of Modified Microwave-assisted Rapid Hydrothermal Liquefaction Process for Conversion of Palm Kernel Shells to Bio-oil

Bio-oil is one of the potential resources to address the sustainable energy development and environmental issues. Microwave-assisted Rapid Hydrothermal Liquefaction Process is one of the popular techniques that is used to extract bio-oil from biomass. In this paper, the bio-oil has been extracted f...

Full description

Bibliographic Details
Main Authors: Abu Saleh, Hasanuzzaman M., Cassidy H., Dayang S. H., Shahril M.
Format: Article
Language:English
Published: Deer Hill Publications 2023-04-01
Series:International Journal of Engineering Materials and Manufacture
Online Access:http://deerhillpublishing.com/index.php/ijemm/article/view/248
_version_ 1797844091605614592
author Abu Saleh
Hasanuzzaman M.
Cassidy H.
Dayang S. H.
Shahril M.
author_facet Abu Saleh
Hasanuzzaman M.
Cassidy H.
Dayang S. H.
Shahril M.
author_sort Abu Saleh
collection DOAJ
description Bio-oil is one of the potential resources to address the sustainable energy development and environmental issues. Microwave-assisted Rapid Hydrothermal Liquefaction Process is one of the popular techniques that is used to extract bio-oil from biomass. In this paper, the bio-oil has been extracted from Palm Kernel Shells by using microwave-assisted and conventional heating pyrolysis processes. A modified heating mantle apparatus are used to conduct the experiment for extracting the bio-oil. The experiments are conducted by varying the hydrothermal temperature and time for both techniques to achieve the conversion of the bio-oil from the raw material. It is found that the yield of bio-oil for microwave-assisted Rapid Hydrothermal Liquefaction Process at 350°C and 400°C are from 10.70 wt% to 25.60 wt% within hydrothermal time 6, 9 and 12 minutes. The pH value of the bio-oil is acidic with the range from 3 to 4. The calorific value of the bio-oil is varied from 24 to 26 MJ/kg for both conversion methods. Fourier Transform Infrared Spectroscopy (FTIR) result reveals that multiple functional groups (alcohol, aldehydes, carboxylic acid and ketones) are present in the PKS bio-oil.
first_indexed 2024-04-09T17:17:53Z
format Article
id doaj.art-f7f427d6837c454f911b20b1389d41ba
institution Directory Open Access Journal
issn 0128-1852
language English
last_indexed 2024-04-09T17:17:53Z
publishDate 2023-04-01
publisher Deer Hill Publications
record_format Article
series International Journal of Engineering Materials and Manufacture
spelling doaj.art-f7f427d6837c454f911b20b1389d41ba2023-04-19T17:10:46ZengDeer Hill PublicationsInternational Journal of Engineering Materials and Manufacture0128-18522023-04-018210.26776/ijemm.07.02.2023.02An Exploration of Modified Microwave-assisted Rapid Hydrothermal Liquefaction Process for Conversion of Palm Kernel Shells to Bio-oilAbu Saleh0Hasanuzzaman M.1Cassidy H.2Dayang S. H.3Shahril M.4Centre for Research of Innovation and Sustainable Development, School of Engineering and Technology, University of Technology Sarawak, 96000 Sibu, Sarawak, MalaysiaUniversiti Malaya Power Energy Dedicated Advanced Centre (UMPEDAC), 59990 Kuala Lumpur, MalaysiaCentre for Research of Innovation and Sustainable Development, School of Engineering and Technology, University of Technology Sarawak, 96000 Sibu, Sarawak, MalaysiaCentre for Research of Innovation and Sustainable Development, School of Engineering and Technology, University of Technology Sarawak, 96000 Sibu, Sarawak, MalaysiaCentre for Research of Innovation and Sustainable Development, School of Engineering and Technology, University of Technology Sarawak, 96000 Sibu, Sarawak, Malaysia Bio-oil is one of the potential resources to address the sustainable energy development and environmental issues. Microwave-assisted Rapid Hydrothermal Liquefaction Process is one of the popular techniques that is used to extract bio-oil from biomass. In this paper, the bio-oil has been extracted from Palm Kernel Shells by using microwave-assisted and conventional heating pyrolysis processes. A modified heating mantle apparatus are used to conduct the experiment for extracting the bio-oil. The experiments are conducted by varying the hydrothermal temperature and time for both techniques to achieve the conversion of the bio-oil from the raw material. It is found that the yield of bio-oil for microwave-assisted Rapid Hydrothermal Liquefaction Process at 350°C and 400°C are from 10.70 wt% to 25.60 wt% within hydrothermal time 6, 9 and 12 minutes. The pH value of the bio-oil is acidic with the range from 3 to 4. The calorific value of the bio-oil is varied from 24 to 26 MJ/kg for both conversion methods. Fourier Transform Infrared Spectroscopy (FTIR) result reveals that multiple functional groups (alcohol, aldehydes, carboxylic acid and ketones) are present in the PKS bio-oil. http://deerhillpublishing.com/index.php/ijemm/article/view/248
spellingShingle Abu Saleh
Hasanuzzaman M.
Cassidy H.
Dayang S. H.
Shahril M.
An Exploration of Modified Microwave-assisted Rapid Hydrothermal Liquefaction Process for Conversion of Palm Kernel Shells to Bio-oil
International Journal of Engineering Materials and Manufacture
title An Exploration of Modified Microwave-assisted Rapid Hydrothermal Liquefaction Process for Conversion of Palm Kernel Shells to Bio-oil
title_full An Exploration of Modified Microwave-assisted Rapid Hydrothermal Liquefaction Process for Conversion of Palm Kernel Shells to Bio-oil
title_fullStr An Exploration of Modified Microwave-assisted Rapid Hydrothermal Liquefaction Process for Conversion of Palm Kernel Shells to Bio-oil
title_full_unstemmed An Exploration of Modified Microwave-assisted Rapid Hydrothermal Liquefaction Process for Conversion of Palm Kernel Shells to Bio-oil
title_short An Exploration of Modified Microwave-assisted Rapid Hydrothermal Liquefaction Process for Conversion of Palm Kernel Shells to Bio-oil
title_sort exploration of modified microwave assisted rapid hydrothermal liquefaction process for conversion of palm kernel shells to bio oil
url http://deerhillpublishing.com/index.php/ijemm/article/view/248
work_keys_str_mv AT abusaleh anexplorationofmodifiedmicrowaveassistedrapidhydrothermalliquefactionprocessforconversionofpalmkernelshellstobiooil
AT hasanuzzamanm anexplorationofmodifiedmicrowaveassistedrapidhydrothermalliquefactionprocessforconversionofpalmkernelshellstobiooil
AT cassidyh anexplorationofmodifiedmicrowaveassistedrapidhydrothermalliquefactionprocessforconversionofpalmkernelshellstobiooil
AT dayangsh anexplorationofmodifiedmicrowaveassistedrapidhydrothermalliquefactionprocessforconversionofpalmkernelshellstobiooil
AT shahrilm anexplorationofmodifiedmicrowaveassistedrapidhydrothermalliquefactionprocessforconversionofpalmkernelshellstobiooil
AT abusaleh explorationofmodifiedmicrowaveassistedrapidhydrothermalliquefactionprocessforconversionofpalmkernelshellstobiooil
AT hasanuzzamanm explorationofmodifiedmicrowaveassistedrapidhydrothermalliquefactionprocessforconversionofpalmkernelshellstobiooil
AT cassidyh explorationofmodifiedmicrowaveassistedrapidhydrothermalliquefactionprocessforconversionofpalmkernelshellstobiooil
AT dayangsh explorationofmodifiedmicrowaveassistedrapidhydrothermalliquefactionprocessforconversionofpalmkernelshellstobiooil
AT shahrilm explorationofmodifiedmicrowaveassistedrapidhydrothermalliquefactionprocessforconversionofpalmkernelshellstobiooil