Quasi-Static Tests of Hybrid Adhesive Bonds Based on Biological Reinforcement in the Form of Eggshell Microparticles

The paper is focused on the research of the cyclic loading of hybrid adhesive bonds based on eggshell microparticles in polymer composite. The aim of the research was to characterize the behavior of hybrid adhesive bonds with composite adhesive layer in quasi-static tests. An epoxy resin was used as...

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Main Authors: Viktor Kolář, Miroslav Müller, Rajesh Mishra, Anna Rudawska, Vladimír Šleger, Martin Tichý, Monika Hromasová, Petr Valášek
Format: Article
Language:English
Published: MDPI AG 2020-06-01
Series:Polymers
Subjects:
Online Access:https://www.mdpi.com/2073-4360/12/6/1391
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author Viktor Kolář
Miroslav Müller
Rajesh Mishra
Anna Rudawska
Vladimír Šleger
Martin Tichý
Monika Hromasová
Petr Valášek
author_facet Viktor Kolář
Miroslav Müller
Rajesh Mishra
Anna Rudawska
Vladimír Šleger
Martin Tichý
Monika Hromasová
Petr Valášek
author_sort Viktor Kolář
collection DOAJ
description The paper is focused on the research of the cyclic loading of hybrid adhesive bonds based on eggshell microparticles in polymer composite. The aim of the research was to characterize the behavior of hybrid adhesive bonds with composite adhesive layer in quasi-static tests. An epoxy resin was used as the matrix and microparticles of eggshells were used as the filler. The adhesive bonds were exposed to cyclic loading and their service life and mechanical properties were evaluated. Testing was performed by 1000 cycles at 5–30% (165–989 N) and 5–70% (165–2307 N) of the maximum load of the filler-free bond in the static test. The results of the research show the importance of cyclic loading on the service life and mechanical properties of adhesive bonds. Quasi-static tests demonstrated significant differences between measured intervals of cyclic loading. All adhesive bonds resisted 1000 cycles of the quasi-static test with an interval loading 5–30%. The number of completed quasi-static tests with the interval loading 5–70% was significantly lower. The filler positively influenced the service life of adhesive bonds at a higher amount of quasi-static tests, i.e., the safety of adhesive bonds increased. The filler had a positive effect on adhesive bonds ABF2, where the strength significantly increased up to 20.26% at the loading of 5–30% against adhesive bonds ABF0. A viscoelasticity characteristic (creep) of the adhesive layer occurred at higher values of loading, i.e., between loading 5–70%. The viscoelasticity behavior did not occur at lower values of loading, i.e., between loading 5–30%.
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spelling doaj.art-f85d6c43c603498db4eceb40f285f68c2023-11-20T04:33:46ZengMDPI AGPolymers2073-43602020-06-01126139110.3390/polym12061391Quasi-Static Tests of Hybrid Adhesive Bonds Based on Biological Reinforcement in the Form of Eggshell MicroparticlesViktor Kolář0Miroslav Müller1Rajesh Mishra2Anna Rudawska3Vladimír Šleger4Martin Tichý5Monika Hromasová6Petr Valášek7Department of Material Science and Manufacturing Technology, Faculty of Engineering, Czech University of Life Sciences Prague, Kamycka 129, 165 00 Prague 6-Suchdol, Czech RepublicDepartment of Material Science and Manufacturing Technology, Faculty of Engineering, Czech University of Life Sciences Prague, Kamycka 129, 165 00 Prague 6-Suchdol, Czech RepublicDepartment of Material Science and Manufacturing Technology, Faculty of Engineering, Czech University of Life Sciences Prague, Kamycka 129, 165 00 Prague 6-Suchdol, Czech RepublicFaculty of Mechanical Engineering, Lublin University of Technology, Nabystyczyka 36 Str., 20-618 Lublin, PolandDepartment of Mechanical Engineering, Faculty of Engineering, Czech University of Life Sciences Prague, Kamycka 129, 165 00 Prague 6-Suchdol, Czech RepublicDepartment of Material Science and Manufacturing Technology, Faculty of Engineering, Czech University of Life Sciences Prague, Kamycka 129, 165 00 Prague 6-Suchdol, Czech RepublicDepartment of Electrical Engineering and Automation, Faculty of Engineering, Czech University of Life Sciences Prague, Kamycka 129, 165 00 Prague 6-Suchdol, Czech RepublicDepartment of Material Science and Manufacturing Technology, Faculty of Engineering, Czech University of Life Sciences Prague, Kamycka 129, 165 00 Prague 6-Suchdol, Czech RepublicThe paper is focused on the research of the cyclic loading of hybrid adhesive bonds based on eggshell microparticles in polymer composite. The aim of the research was to characterize the behavior of hybrid adhesive bonds with composite adhesive layer in quasi-static tests. An epoxy resin was used as the matrix and microparticles of eggshells were used as the filler. The adhesive bonds were exposed to cyclic loading and their service life and mechanical properties were evaluated. Testing was performed by 1000 cycles at 5–30% (165–989 N) and 5–70% (165–2307 N) of the maximum load of the filler-free bond in the static test. The results of the research show the importance of cyclic loading on the service life and mechanical properties of adhesive bonds. Quasi-static tests demonstrated significant differences between measured intervals of cyclic loading. All adhesive bonds resisted 1000 cycles of the quasi-static test with an interval loading 5–30%. The number of completed quasi-static tests with the interval loading 5–70% was significantly lower. The filler positively influenced the service life of adhesive bonds at a higher amount of quasi-static tests, i.e., the safety of adhesive bonds increased. The filler had a positive effect on adhesive bonds ABF2, where the strength significantly increased up to 20.26% at the loading of 5–30% against adhesive bonds ABF0. A viscoelasticity characteristic (creep) of the adhesive layer occurred at higher values of loading, i.e., between loading 5–70%. The viscoelasticity behavior did not occur at lower values of loading, i.e., between loading 5–30%.https://www.mdpi.com/2073-4360/12/6/1391cyclic loadinghybrid adhesive bondmechanical propertiespolymer compositeservice life
spellingShingle Viktor Kolář
Miroslav Müller
Rajesh Mishra
Anna Rudawska
Vladimír Šleger
Martin Tichý
Monika Hromasová
Petr Valášek
Quasi-Static Tests of Hybrid Adhesive Bonds Based on Biological Reinforcement in the Form of Eggshell Microparticles
Polymers
cyclic loading
hybrid adhesive bond
mechanical properties
polymer composite
service life
title Quasi-Static Tests of Hybrid Adhesive Bonds Based on Biological Reinforcement in the Form of Eggshell Microparticles
title_full Quasi-Static Tests of Hybrid Adhesive Bonds Based on Biological Reinforcement in the Form of Eggshell Microparticles
title_fullStr Quasi-Static Tests of Hybrid Adhesive Bonds Based on Biological Reinforcement in the Form of Eggshell Microparticles
title_full_unstemmed Quasi-Static Tests of Hybrid Adhesive Bonds Based on Biological Reinforcement in the Form of Eggshell Microparticles
title_short Quasi-Static Tests of Hybrid Adhesive Bonds Based on Biological Reinforcement in the Form of Eggshell Microparticles
title_sort quasi static tests of hybrid adhesive bonds based on biological reinforcement in the form of eggshell microparticles
topic cyclic loading
hybrid adhesive bond
mechanical properties
polymer composite
service life
url https://www.mdpi.com/2073-4360/12/6/1391
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