多功能净化柱-光化学衍生高效液相色谱法测定成品植物油和花生原油中黄曲霉毒素B1Determination of aflatoxin B1 in finished vegetable oil and crude peanut oil by multifunctional clean-up column-photochemical derivatization and high performance liquid chromatography

多功能净化柱-光化学衍生高效液相色谱法测定成品植物油和花生原油中黄曲霉毒素B1Determination of aflatoxin B1 in finished vegetable oil and crude peanut oil by multifunctional clean-up column-photochemical derivatization and high performance liquid chromatography

为了快速、准确测定成品植物油和花生原油中黄曲霉毒素B1（AFB1）的含量，建立了采用多功能净化柱对油样进行前处理，再结合光化学衍生高效液相色谱法测定植物油中AFB1含量的方法，对前处理提取剂、高效液相色谱法的分析条件（色谱柱、进样量）进行优化，再通过与国标中免疫亲和柱法进行比较，对所建立的方法进行评价。结果表明：优化的条件为以乙腈-水溶液（84+16）为提取剂，采用Zorbax Eclipse XDB-C18色谱柱（4.6 mm×150 mm，5 μm），进样量10 μL；建立的方法加标回收率和精密度良好，定量限为0.2 μg/kg，低于GB 2761—2017规定的最低限量值要求，可满足企业...

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Bibliographic Details
Main Author:	姜德铭1，刘晓萌1，邹球龙1，印铁1，张晓琳1，张刚2，刘配莲2 JIANG Deming1, LIU Xiaomeng1, ZOU Qiulong1, YIN Tie1, ZHANG Xiaolin1, ZHANG Gang2, LIU Peilian2
Format:	Article
Language:	English
Published:	中粮工科（西安）国际工程有限公司 2023-03-01
Series:	Zhongguo youzhi
Subjects:	黄曲霉毒素b1；多功能净化柱；植物油；高效液相色谱 aflatoxin b1; multifunctional clean-up column; vegetable oil; high performance liquid chromatography
Online Access:	http://tg.chinaoils.cn/ch/reader/create_pdf.aspx?file_no=20230318&year_id=2023&quarter_id=3&falg=1

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