Response surface methodology for optimization studies of hydro-distillation of essential oil from pixie mandarin (Citrus reticulata Blanco) peels
Essential oil extraction technique from mandarin pixie peels by hydro-distillation is optimized by response surface methodology (RSM). Mathematical techniques were used in experimental design to evaluate the impacts of factors that affect the extraction process and improve the yield of the extractio...
| Main Authors: | , , , , , |
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| Format: | Article |
| Language: | English |
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Sciendo
2021-12-01
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| Series: | Polish Journal of Chemical Technology |
| Subjects: | |
| Online Access: | https://doi.org/10.2478/pjct-2021-0034 |
| _version_ | 1818082850322251776 |
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| author | Dao Tan Phat Quyen Ngo Thi Cam Nhi Tran Thi Yen Nguyen Chi Cuong Nguyen Trung Thanh Le Xuan Tien |
| author_facet | Dao Tan Phat Quyen Ngo Thi Cam Nhi Tran Thi Yen Nguyen Chi Cuong Nguyen Trung Thanh Le Xuan Tien |
| author_sort | Dao Tan Phat |
| collection | DOAJ |
| description | Essential oil extraction technique from mandarin pixie peels by hydro-distillation is optimized by response surface methodology (RSM). Mathematical techniques were used in experimental design to evaluate the impacts of factors that affect the extraction process and improve the yield of the extraction process. A central mixed design based on influencing variables such as water ratio (3–5 mL/g), temperature (110–130 °C) and extraction time (90–150 min) was adopted with essential oil yield as the target function. Correlation analysis of the mathematical regression model showed that the quadratic polynomial model can be used to optimize hydro-distillation of pixie mandarin oil. The results showed that under the optimum extraction conditions, the highest quantity of essential oils was achieved (7.28 mL/100 g materials). In terms of statistical analysis, the significance levels (p-value <0.05) of the model showed that the experimental results had a good impact between factors. The coefficient of determination indicating the match between the experimental value and the predicted value of the model was high (R2>0.9). The chemical composition of the essential oil was analyzed by Gas Chromatography-Mass Spectrometry, revealing the dominance of limonene content (97.667%), which implies that the essential oil of pixie mandarin could be an alternative source of limonene. |
| first_indexed | 2024-12-10T19:28:39Z |
| format | Article |
| id | doaj.art-f90ca654919447c6a594fa7765db5e6a |
| institution | Directory Open Access Journal |
| issn | 1899-4741 |
| language | English |
| last_indexed | 2024-12-10T19:28:39Z |
| publishDate | 2021-12-01 |
| publisher | Sciendo |
| record_format | Article |
| series | Polish Journal of Chemical Technology |
| spelling | doaj.art-f90ca654919447c6a594fa7765db5e6a2022-12-22T01:36:18ZengSciendoPolish Journal of Chemical Technology1899-47412021-12-01234263410.2478/pjct-2021-0034Response surface methodology for optimization studies of hydro-distillation of essential oil from pixie mandarin (Citrus reticulata Blanco) peelsDao Tan Phat0Quyen Ngo Thi Cam1Nhi Tran Thi Yen2Nguyen Chi Cuong3Nguyen Trung Thanh4Le Xuan Tien5Institute of Environmental Technology and Sustainable Development, Nguyen Tat Thanh University, Ho Chi Minh City, VietnamInstitute of Environmental Technology and Sustainable Development, Nguyen Tat Thanh University, Ho Chi Minh City, VietnamInstitute of Environmental Technology and Sustainable Development, Nguyen Tat Thanh University, Ho Chi Minh City, VietnamFaculty of Food Science and Technology, Nong Lam University, Ho Chi Minh City, VietnamNanomaterial Laboratory, An Giang University, An Giang Province, VietnamVietnam National University Ho Chi Minh City, Ho Chi Minh City, VietnamEssential oil extraction technique from mandarin pixie peels by hydro-distillation is optimized by response surface methodology (RSM). Mathematical techniques were used in experimental design to evaluate the impacts of factors that affect the extraction process and improve the yield of the extraction process. A central mixed design based on influencing variables such as water ratio (3–5 mL/g), temperature (110–130 °C) and extraction time (90–150 min) was adopted with essential oil yield as the target function. Correlation analysis of the mathematical regression model showed that the quadratic polynomial model can be used to optimize hydro-distillation of pixie mandarin oil. The results showed that under the optimum extraction conditions, the highest quantity of essential oils was achieved (7.28 mL/100 g materials). In terms of statistical analysis, the significance levels (p-value <0.05) of the model showed that the experimental results had a good impact between factors. The coefficient of determination indicating the match between the experimental value and the predicted value of the model was high (R2>0.9). The chemical composition of the essential oil was analyzed by Gas Chromatography-Mass Spectrometry, revealing the dominance of limonene content (97.667%), which implies that the essential oil of pixie mandarin could be an alternative source of limonene.https://doi.org/10.2478/pjct-2021-0034hydro-distillationpixie mandarin oil (citrus reticulata blanco)rsmgc-ms |
| spellingShingle | Dao Tan Phat Quyen Ngo Thi Cam Nhi Tran Thi Yen Nguyen Chi Cuong Nguyen Trung Thanh Le Xuan Tien Response surface methodology for optimization studies of hydro-distillation of essential oil from pixie mandarin (Citrus reticulata Blanco) peels Polish Journal of Chemical Technology hydro-distillation pixie mandarin oil (citrus reticulata blanco) rsm gc-ms |
| title | Response surface methodology for optimization studies of hydro-distillation of essential oil from pixie mandarin (Citrus reticulata Blanco) peels |
| title_full | Response surface methodology for optimization studies of hydro-distillation of essential oil from pixie mandarin (Citrus reticulata Blanco) peels |
| title_fullStr | Response surface methodology for optimization studies of hydro-distillation of essential oil from pixie mandarin (Citrus reticulata Blanco) peels |
| title_full_unstemmed | Response surface methodology for optimization studies of hydro-distillation of essential oil from pixie mandarin (Citrus reticulata Blanco) peels |
| title_short | Response surface methodology for optimization studies of hydro-distillation of essential oil from pixie mandarin (Citrus reticulata Blanco) peels |
| title_sort | response surface methodology for optimization studies of hydro distillation of essential oil from pixie mandarin citrus reticulata blanco peels |
| topic | hydro-distillation pixie mandarin oil (citrus reticulata blanco) rsm gc-ms |
| url | https://doi.org/10.2478/pjct-2021-0034 |
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