1,2-Bis(N′-benzoylthioureido)benzene
The title compound, C22H18N4O2S2, was characterized by 1H and 13C NMR, solid-state IR spectroscopy and X-ray crystallographic techniques. The crystal structure determination reveals that the twisting modes of the two side arms are different [C—N—C—O and C—N&am...
| Main Authors: | , , , , |
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2008-05-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536808008374 |
| _version_ | 1798025808316465152 |
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| author | Aliou Hamady Barry Abdou Salam Sall Mohamed Gaye Mayoro Diop Elhadj Ibrahima Thiam |
| author_facet | Aliou Hamady Barry Abdou Salam Sall Mohamed Gaye Mayoro Diop Elhadj Ibrahima Thiam |
| author_sort | Aliou Hamady Barry |
| collection | DOAJ |
| description | The title compound, C22H18N4O2S2, was characterized by 1H and 13C NMR, solid-state IR spectroscopy and X-ray crystallographic techniques. The crystal structure determination reveals that the twisting modes of the two side arms are different [C—N—C—O and C—N—C—N torsion angles = −1.2 (3) and 1.1 (3)°, respectively, in one arm and 24.1 (3) and −5.1 (3)°, respectively, in the other]. The crystal structure involves N—H...O and N—H...S hydrogen bonds. |
| first_indexed | 2024-04-11T18:24:50Z |
| format | Article |
| id | doaj.art-f92e7188cda6448ba97d0a11fdddf0d0 |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-04-11T18:24:50Z |
| publishDate | 2008-05-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-f92e7188cda6448ba97d0a11fdddf0d02022-12-22T04:09:40ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682008-05-01645o776o77610.1107/S16005368080083741,2-Bis(N′-benzoylthioureido)benzeneAliou Hamady BarryAbdou Salam SallMohamed GayeMayoro DiopElhadj Ibrahima ThiamThe title compound, C22H18N4O2S2, was characterized by 1H and 13C NMR, solid-state IR spectroscopy and X-ray crystallographic techniques. The crystal structure determination reveals that the twisting modes of the two side arms are different [C—N—C—O and C—N—C—N torsion angles = −1.2 (3) and 1.1 (3)°, respectively, in one arm and 24.1 (3) and −5.1 (3)°, respectively, in the other]. The crystal structure involves N—H...O and N—H...S hydrogen bonds.http://scripts.iucr.org/cgi-bin/paper?S1600536808008374 |
| spellingShingle | Aliou Hamady Barry Abdou Salam Sall Mohamed Gaye Mayoro Diop Elhadj Ibrahima Thiam 1,2-Bis(N′-benzoylthioureido)benzene Acta Crystallographica Section E |
| title | 1,2-Bis(N′-benzoylthioureido)benzene |
| title_full | 1,2-Bis(N′-benzoylthioureido)benzene |
| title_fullStr | 1,2-Bis(N′-benzoylthioureido)benzene |
| title_full_unstemmed | 1,2-Bis(N′-benzoylthioureido)benzene |
| title_short | 1,2-Bis(N′-benzoylthioureido)benzene |
| title_sort | 1 2 bis n 8242 benzoylthioureido benzene |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536808008374 |
| work_keys_str_mv | AT aliouhamadybarry 12bisn8242benzoylthioureidobenzene AT abdousalamsall 12bisn8242benzoylthioureidobenzene AT mohamedgaye 12bisn8242benzoylthioureidobenzene AT mayorodiop 12bisn8242benzoylthioureidobenzene AT elhadjibrahimathiam 12bisn8242benzoylthioureidobenzene |