Synthesis and crystal structure of (S,E)-4-hydroxy-3-(2-((4aR,6aS,7R,10aS,10bR)-3,3,6a,10b-tetramethyl-8-methylenedecahydro-1H-naphtho[2,1-d][1,3]dioxin-7-yl)ethylidene)dihydrofuran-2(3H)-one, C23H34O5

C23H34O5, orthorhombic, P212121 (no. 19), a = 11.1838(3) Å, b = 11.7824(3) Å, c = 16.3160(5) Å, V = 2149.99(10) Å3, Z = 4, Rgt ${R}_{\mathrm{g}\mathrm{t}}$ (F) = 0.0399, wRref $w{R}_{\mathrm{r}\mathrm{e}\mathrm{f}}$ (F 2) = 0.1097, T = 293 K.

Bibliographic Details
Main Authors: Li Shi-Qing, Zhou Jian, Dong Zhang-Chao, Pan Bo Wen, Shi Yang, Zhou Ying
Format: Article
Language:English
Published: De Gruyter 2023-08-01
Series:Zeitschrift für Kristallographie - New Crystal Structures
Subjects:
Online Access:https://doi.org/10.1515/ncrs-2023-0179
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author Li Shi-Qing
Zhou Jian
Dong Zhang-Chao
Pan Bo Wen
Shi Yang
Zhou Ying
author_facet Li Shi-Qing
Zhou Jian
Dong Zhang-Chao
Pan Bo Wen
Shi Yang
Zhou Ying
author_sort Li Shi-Qing
collection DOAJ
description C23H34O5, orthorhombic, P212121 (no. 19), a = 11.1838(3) Å, b = 11.7824(3) Å, c = 16.3160(5) Å, V = 2149.99(10) Å3, Z = 4, Rgt ${R}_{\mathrm{g}\mathrm{t}}$ (F) = 0.0399, wRref $w{R}_{\mathrm{r}\mathrm{e}\mathrm{f}}$ (F 2) = 0.1097, T = 293 K.
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spelling doaj.art-f93ab08d6e6a428392eb56eb89e884ee2023-07-10T06:04:06ZengDe GruyterZeitschrift für Kristallographie - New Crystal Structures1433-72662197-45782023-08-01238473573710.1515/ncrs-2023-0179Synthesis and crystal structure of (S,E)-4-hydroxy-3-(2-((4aR,6aS,7R,10aS,10bR)-3,3,6a,10b-tetramethyl-8-methylenedecahydro-1H-naphtho[2,1-d][1,3]dioxin-7-yl)ethylidene)dihydrofuran-2(3H)-one, C23H34O5Li Shi-Qing0Zhou Jian1Dong Zhang-Chao2Pan Bo Wen3Shi Yang4Zhou Ying5Guizhou University of Traditional Chinese Medicine, Guiyang550025, P.R. ChinaShanghai Engineering Research Center of Molecular Therapeutics and New Drug Development, Shanghai Key Laboratory of Green Chemistry and Chemical Processes, East China Normal University, Shanghai200062, P.R. ChinaGuizhou University of Traditional Chinese Medicine, Guiyang550025, P.R. ChinaGuizhou University of Traditional Chinese Medicine, Guiyang550025, P.R. ChinaGuizhou University of Traditional Chinese Medicine, Guiyang550025, P.R. ChinaGuizhou University of Traditional Chinese Medicine, Guiyang550025, P.R. ChinaC23H34O5, orthorhombic, P212121 (no. 19), a = 11.1838(3) Å, b = 11.7824(3) Å, c = 16.3160(5) Å, V = 2149.99(10) Å3, Z = 4, Rgt ${R}_{\mathrm{g}\mathrm{t}}$ (F) = 0.0399, wRref $w{R}_{\mathrm{r}\mathrm{e}\mathrm{f}}$ (F 2) = 0.1097, T = 293 K.https://doi.org/10.1515/ncrs-2023-01792254956
spellingShingle Li Shi-Qing
Zhou Jian
Dong Zhang-Chao
Pan Bo Wen
Shi Yang
Zhou Ying
Synthesis and crystal structure of (S,E)-4-hydroxy-3-(2-((4aR,6aS,7R,10aS,10bR)-3,3,6a,10b-tetramethyl-8-methylenedecahydro-1H-naphtho[2,1-d][1,3]dioxin-7-yl)ethylidene)dihydrofuran-2(3H)-one, C23H34O5
Zeitschrift für Kristallographie - New Crystal Structures
2254956
title Synthesis and crystal structure of (S,E)-4-hydroxy-3-(2-((4aR,6aS,7R,10aS,10bR)-3,3,6a,10b-tetramethyl-8-methylenedecahydro-1H-naphtho[2,1-d][1,3]dioxin-7-yl)ethylidene)dihydrofuran-2(3H)-one, C23H34O5
title_full Synthesis and crystal structure of (S,E)-4-hydroxy-3-(2-((4aR,6aS,7R,10aS,10bR)-3,3,6a,10b-tetramethyl-8-methylenedecahydro-1H-naphtho[2,1-d][1,3]dioxin-7-yl)ethylidene)dihydrofuran-2(3H)-one, C23H34O5
title_fullStr Synthesis and crystal structure of (S,E)-4-hydroxy-3-(2-((4aR,6aS,7R,10aS,10bR)-3,3,6a,10b-tetramethyl-8-methylenedecahydro-1H-naphtho[2,1-d][1,3]dioxin-7-yl)ethylidene)dihydrofuran-2(3H)-one, C23H34O5
title_full_unstemmed Synthesis and crystal structure of (S,E)-4-hydroxy-3-(2-((4aR,6aS,7R,10aS,10bR)-3,3,6a,10b-tetramethyl-8-methylenedecahydro-1H-naphtho[2,1-d][1,3]dioxin-7-yl)ethylidene)dihydrofuran-2(3H)-one, C23H34O5
title_short Synthesis and crystal structure of (S,E)-4-hydroxy-3-(2-((4aR,6aS,7R,10aS,10bR)-3,3,6a,10b-tetramethyl-8-methylenedecahydro-1H-naphtho[2,1-d][1,3]dioxin-7-yl)ethylidene)dihydrofuran-2(3H)-one, C23H34O5
title_sort synthesis and crystal structure of s e 4 hydroxy 3 2 4ar 6as 7r 10as 10br 3 3 6a 10b tetramethyl 8 methylenedecahydro 1h naphtho 2 1 d 1 3 dioxin 7 yl ethylidene dihydrofuran 2 3h one c23h34o5
topic 2254956
url https://doi.org/10.1515/ncrs-2023-0179
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