Synthesis and crystal structure of (S,E)-4-hydroxy-3-(2-((4aR,6aS,7R,10aS,10bR)-3,3,6a,10b-tetramethyl-8-methylenedecahydro-1H-naphtho[2,1-d][1,3]dioxin-7-yl)ethylidene)dihydrofuran-2(3H)-one, C23H34O5
C23H34O5, orthorhombic, P212121 (no. 19), a = 11.1838(3) Å, b = 11.7824(3) Å, c = 16.3160(5) Å, V = 2149.99(10) Å3, Z = 4, Rgt ${R}_{\mathrm{g}\mathrm{t}}$ (F) = 0.0399, wRref $w{R}_{\mathrm{r}\mathrm{e}\mathrm{f}}$ (F 2) = 0.1097, T = 293 K.
Main Authors: | , , , , , |
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Format: | Article |
Language: | English |
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De Gruyter
2023-08-01
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Series: | Zeitschrift für Kristallographie - New Crystal Structures |
Subjects: | |
Online Access: | https://doi.org/10.1515/ncrs-2023-0179 |
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author | Li Shi-Qing Zhou Jian Dong Zhang-Chao Pan Bo Wen Shi Yang Zhou Ying |
author_facet | Li Shi-Qing Zhou Jian Dong Zhang-Chao Pan Bo Wen Shi Yang Zhou Ying |
author_sort | Li Shi-Qing |
collection | DOAJ |
description | C23H34O5, orthorhombic, P212121 (no. 19), a = 11.1838(3) Å, b = 11.7824(3) Å, c = 16.3160(5) Å, V = 2149.99(10) Å3, Z = 4, Rgt
${R}_{\mathrm{g}\mathrm{t}}$
(F) = 0.0399, wRref
$w{R}_{\mathrm{r}\mathrm{e}\mathrm{f}}$
(F
2) = 0.1097, T = 293 K. |
first_indexed | 2024-03-13T00:36:22Z |
format | Article |
id | doaj.art-f93ab08d6e6a428392eb56eb89e884ee |
institution | Directory Open Access Journal |
issn | 1433-7266 2197-4578 |
language | English |
last_indexed | 2024-03-13T00:36:22Z |
publishDate | 2023-08-01 |
publisher | De Gruyter |
record_format | Article |
series | Zeitschrift für Kristallographie - New Crystal Structures |
spelling | doaj.art-f93ab08d6e6a428392eb56eb89e884ee2023-07-10T06:04:06ZengDe GruyterZeitschrift für Kristallographie - New Crystal Structures1433-72662197-45782023-08-01238473573710.1515/ncrs-2023-0179Synthesis and crystal structure of (S,E)-4-hydroxy-3-(2-((4aR,6aS,7R,10aS,10bR)-3,3,6a,10b-tetramethyl-8-methylenedecahydro-1H-naphtho[2,1-d][1,3]dioxin-7-yl)ethylidene)dihydrofuran-2(3H)-one, C23H34O5Li Shi-Qing0Zhou Jian1Dong Zhang-Chao2Pan Bo Wen3Shi Yang4Zhou Ying5Guizhou University of Traditional Chinese Medicine, Guiyang550025, P.R. ChinaShanghai Engineering Research Center of Molecular Therapeutics and New Drug Development, Shanghai Key Laboratory of Green Chemistry and Chemical Processes, East China Normal University, Shanghai200062, P.R. ChinaGuizhou University of Traditional Chinese Medicine, Guiyang550025, P.R. ChinaGuizhou University of Traditional Chinese Medicine, Guiyang550025, P.R. ChinaGuizhou University of Traditional Chinese Medicine, Guiyang550025, P.R. ChinaGuizhou University of Traditional Chinese Medicine, Guiyang550025, P.R. ChinaC23H34O5, orthorhombic, P212121 (no. 19), a = 11.1838(3) Å, b = 11.7824(3) Å, c = 16.3160(5) Å, V = 2149.99(10) Å3, Z = 4, Rgt ${R}_{\mathrm{g}\mathrm{t}}$ (F) = 0.0399, wRref $w{R}_{\mathrm{r}\mathrm{e}\mathrm{f}}$ (F 2) = 0.1097, T = 293 K.https://doi.org/10.1515/ncrs-2023-01792254956 |
spellingShingle | Li Shi-Qing Zhou Jian Dong Zhang-Chao Pan Bo Wen Shi Yang Zhou Ying Synthesis and crystal structure of (S,E)-4-hydroxy-3-(2-((4aR,6aS,7R,10aS,10bR)-3,3,6a,10b-tetramethyl-8-methylenedecahydro-1H-naphtho[2,1-d][1,3]dioxin-7-yl)ethylidene)dihydrofuran-2(3H)-one, C23H34O5 Zeitschrift für Kristallographie - New Crystal Structures 2254956 |
title | Synthesis and crystal structure of (S,E)-4-hydroxy-3-(2-((4aR,6aS,7R,10aS,10bR)-3,3,6a,10b-tetramethyl-8-methylenedecahydro-1H-naphtho[2,1-d][1,3]dioxin-7-yl)ethylidene)dihydrofuran-2(3H)-one, C23H34O5 |
title_full | Synthesis and crystal structure of (S,E)-4-hydroxy-3-(2-((4aR,6aS,7R,10aS,10bR)-3,3,6a,10b-tetramethyl-8-methylenedecahydro-1H-naphtho[2,1-d][1,3]dioxin-7-yl)ethylidene)dihydrofuran-2(3H)-one, C23H34O5 |
title_fullStr | Synthesis and crystal structure of (S,E)-4-hydroxy-3-(2-((4aR,6aS,7R,10aS,10bR)-3,3,6a,10b-tetramethyl-8-methylenedecahydro-1H-naphtho[2,1-d][1,3]dioxin-7-yl)ethylidene)dihydrofuran-2(3H)-one, C23H34O5 |
title_full_unstemmed | Synthesis and crystal structure of (S,E)-4-hydroxy-3-(2-((4aR,6aS,7R,10aS,10bR)-3,3,6a,10b-tetramethyl-8-methylenedecahydro-1H-naphtho[2,1-d][1,3]dioxin-7-yl)ethylidene)dihydrofuran-2(3H)-one, C23H34O5 |
title_short | Synthesis and crystal structure of (S,E)-4-hydroxy-3-(2-((4aR,6aS,7R,10aS,10bR)-3,3,6a,10b-tetramethyl-8-methylenedecahydro-1H-naphtho[2,1-d][1,3]dioxin-7-yl)ethylidene)dihydrofuran-2(3H)-one, C23H34O5 |
title_sort | synthesis and crystal structure of s e 4 hydroxy 3 2 4ar 6as 7r 10as 10br 3 3 6a 10b tetramethyl 8 methylenedecahydro 1h naphtho 2 1 d 1 3 dioxin 7 yl ethylidene dihydrofuran 2 3h one c23h34o5 |
topic | 2254956 |
url | https://doi.org/10.1515/ncrs-2023-0179 |
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