Synthesis and crystal structure of (S,E)-4-hydroxy-3-(2-((4aR,6aS,7R,10aS,10bR)-3,3,6a,10b-tetramethyl-8-methylenedecahydro-1H-naphtho[2,1-d][1,3]dioxin-7-yl)ethylidene)dihydrofuran-2(3H)-one, C23H34O5

Synthesis and crystal structure of (S,E)-4-hydroxy-3-(2-((4aR,6aS,7R,10aS,10bR)-3,3,6a,10b-tetramethyl-8-methylenedecahydro-1H-naphtho[2,1-d][1,3]dioxin-7-yl)ethylidene)dihydrofuran-2(3H)-one, C23H34O5

C23H34O5, orthorhombic, P212121 (no. 19), a = 11.1838(3) Å, b = 11.7824(3) Å, c = 16.3160(5) Å, V = 2149.99(10) Å3, Z = 4, Rgt ${R}_{\mathrm{g}\mathrm{t}}$ (F) = 0.0399, wRref $w{R}_{\mathrm{r}\mathrm{e}\mathrm{f}}$ (F 2) = 0.1097, T = 293 K.

Bibliographic Details
Main Authors:	Li Shi-Qing, Zhou Jian, Dong Zhang-Chao, Pan Bo Wen, Shi Yang, Zhou Ying
Format:	Article
Language:	English
Published:	De Gruyter 2023-08-01
Series:	Zeitschrift für Kristallographie - New Crystal Structures
Subjects:	2254956
Online Access:	https://doi.org/10.1515/ncrs-2023-0179

Similar Items

(1S,3R,8R,9R,10S)-2,2-Dibromo-3,7,7,10-tetramethyl-9β,10β-epoxy-3,7,7,10-tetramethyltricyclo[6.4.0.01,3]dodecane
by: Abdelouahd Oukhrib, et al.
Published: (2013-04-01)

(1S,3R,8S,9R,10S)-2,2-Dichloro-3,7,7,10-tetramethyl-9,10-epoxytricyclo[6.4.0.01,3]dodecane
by: Moha Berraho, et al.
Published: (2010-12-01)

10-(1,3-Benzothiazol-2-yl)-1,1,7,7-tetramethyl-2,3,6,7-tetrahydro-1H,5H,11H-pyrano[3,2-g]pyrido[3,2,1-hi]quinoline
by: Ki-Min Park, et al.
Published: (2010-04-01)

10-Benzyl-9-(4-ethoxyphenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-dione
by: V. Sughanya, et al.
Published: (2012-09-01)

Crystal structure of (1R,3S,5R)-3-hydroxy-2-methylene-6-oxabicyclo[3.2.1.]octan-7-one, C8H10O3
by: Peters K., et al.
Published: (2004-04-01)

10-[2-(Dimethylamino)ethyl]-9-(4-methoxyphenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-dione
by: K. Sivakumar, et al.
Published: (2009-02-01)

1-[(1-{[(1S,2R,6R,8R,9S)-4,4,11,11-Tetramethyl-3,5,7,10,12-pentaoxatricyclo[7.3.0.02,6]dodecan-8-yl]methyl}-1H-1,2,3-triazol-4-yl)methyl]-2,3-dihydro-1H-indole-2,3-dione
by: Fatima-Zahrae Qachchachi, et al.
Published: (2017-05-01)

7-[2-(3-Furyl)ethyl]-7,8-dimethyl-3,5,6,6a,7,8,9,10-octahydro-1H-naphtho[1,8a-c]furan-3-one
by: Josef W. A. Frese, et al.
Published: (2010-10-01)

10-(4-Chlorophenyl)-9-(4-fluorophenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-dione
by: Da Teng, et al.
Published: (2008-09-01)

Crystal structure of (1S,3aR,3bR,10aR,10bR,12aR)-8-amino-3a,3b,6,6,10a-pentamethyl-1-((S)-2,6,6-trimethyltetrahydro-2H-pyran-2-yl)-2,3,3a,3b,4,5,5a,6,10,10a,10b,11,12,12a-tetradecahydro-1H-cyclopenta[7,8]phenanthro[2,3-d]thiazol-12-ol – a panaxadiol dervative, C31H50N2O2S
by: Wang Jia-Zhen, et al.
Published: (2019-03-01)

Crystal structure of 3R(S)-1’ S(R)-2,2-dimethoxycarbonyl-3-(2’ ,6’, 6’- trimethyl-2’ -cyclohexen-1’ -yl)-2,3-dihydrofuran, C18H26O5
by: Daut-Özdemir A., et al.
Published: (2002-12-01)

Crystal structure of 3R(S)-1’ S(R)-2,2-dimethoxycarbonyl-3-(2’ ,6’, 6’- trimethyl-2’ -cyclohexen-1’ -yl)-2,3-dihydrofuran, C18H26O5
by: Daut-Özdemir A., et al.
Published: (2002-12-01)

(1S,3S,8R,9S,10R)-9,10-Epoxy-3,7,7,10-tetramethyltricyclo[6.4.0.01,3]dodecane
by: Abdoullah Bimoussa, et al.
Published: (2014-04-01)

(1S,3R,8R)-2,2-Dichloro-3,7,7,10-tetramethyl-11-methylenetricyclo[6.4.0.01,3]dodec-9-ene
by: Ahmed Benharref, et al.
Published: (2017-03-01)

(1S,3S,8R,10R,11R)-3,7,7,10-Tetramethyltricyclo[6.4.0.01,3]dodecan-11-ol
by: Moha Berraho, et al.
Published: (2013-08-01)

(1S,3R,8R,9S,11R)-2,2,10,10-Tetrachloro-3,7,7,11-tetramethyltetracyclo[6.5.0.01,3.09,11]tridecane
by: Najia Ourhriss, et al.
Published: (2013-02-01)

5-Fluoro-1-[(1-{[(1S,2R,6R,8S,9R)-4,4,11,11-tetramethyl-3,5,7,10,12-pentaoxatricyclo[7.3.0.02,6]dodecan-8-yl]methyl}-1H-1,2,3-triazol-4-yl)methyl]-2,3-dihydro-1H-indole-2,3-dione
by: Fatima-Zahrae Qachchachi, et al.
Published: (2017-05-01)

Crystal structure of 9-(3-bromo-5-chloro-2-hydroxyphenyl)-10-(2-hydroxyethyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-dione
by: Antar A. Abdelhamid, et al.
Published: (2014-08-01)

Crystal structure of (1R*,2S*,3R*,4R*)-ethyl 3-acetoxy-1,2,3,4,5,6,7,8,9,10,11,12,13,14-tetradecahydro-1,4-epoxybenzo-cyclodecene-2-carboxylate,C10H20[C6H4O](COOC2H5)(OCOCH3)
by: Peters Κ., et al.
Published: (1999-03-01)

(1S,2E,6R,7aR)-1,6-Dihydroxy-2-(4-nitrobenzylidene)-2,3,5,6,7,7a-hexahydro-1H-pyrrolizin-3-one
by: R. Aparicio, et al.
Published: (2012-05-01)

Crystal structure of (P)-1-(2-hydroxyphenyI)-2-naphthoicacid(1S,2R,5S)-(+)-menthylester,C10H6[C6H4(OH)][COOC6H9(CH3)(C3H7)]
by: Peters K., et al.
Published: (1999-12-01)

1H,3H-Imidazolium (R,S)-camphor-10-sulfonate
by: Abdul Rahman, Mohd Basyaruddin, et al.
Published: (2009)

1H,3H-Imidazolium (R,S)-camphor-10-sulfonate
by: Hoong-Kun Fun, et al.
Published: (2009-02-01)

(1S,3R,8R)-2,2-Dibromo-10-bromomethyl-3,7,7-trimethyltricyclo[6.4.0.01,3]dodec-9-ene
by: Abdelouahd Oukhrib, et al.
Published: (2012-12-01)

9-(2,4-Dichlorophenyl)-3,3,6,6-tetramethyl-3,4,5,6-tetrahydro-9H-xanthene-1,8(2H,7H)-dione
by: Hao Shi
Published: (2010-12-01)

(1S,2R,8R)-11-Amino-2,2-dichloro-3,7,7,10-tetramethyltricyclo[6.4.0.01,3]dodec-10-en-9-one
by: Mustapha Ait Elhad, et al.
Published: (2017-02-01)

Crystal structure of (2R,3S)-2-exo-[1R-(2S-lsopropyl-5R-methyl- cyclohexyloxy)]-2-endo,3-exo-di{carboxy-[1-(2S-isopropyl-5R-methylcyclohexyl)]} bicyclo[2.2.1]hept-5-ene, C7H7(OC10H19)(COOC10H19)2
by: Peters K., et al.
Published: (2000-02-01)

Synthesis of 2,2′-bis(1-(2-aryl)-1H-pyrazol-4-yl)-3,3,3′,3′-tetramethyl-3H,3′H-5,5′-biindoles and 2,7-bis(1-(3-aryl)-1H-pyrazol-4-yl)-1,1,6,6-tetramethyl-1,6-dihydroindolo[7,6-g]indoles
by: Mehdi Mohammad Baradarani, et al.
Published: (2011-01-01)

(3aR*,6S*,7aR*)-7a-Chloro-6-methyl-2-(4-methylphenylsulfonyl)-2,3,3a,6,7,7a-hexahydro-3a,6-epoxy-1H-isoindole
by: Ersin Temel, et al.
Published: (2012-04-01)

The crystal structure of (2a′S,2a1′S,3R,5a′S,7′R)-5-(furan-3-yl)-2a′,2a1′-dihydroxy-7′-methyldecahydro-2H-spiro[furan-3,6′-naphtho[1,8-bc]furan]-2,2′(2a′H)-dione, C19H22O7
by: Xu Xin-Ke, et al.
Published: (2021-12-01)

Crystal structure of 1,4-dimethyl-6H-benzo[b]naphtho[1,2-d]pyran-6-one, C10H6(COO)C6H2(CH3)2
by: Peters K., et al.
Published: (2000-03-01)

N′-[(1S,3R,8R)-2,2-Dichloro-3,7,7,10-tetramethyltricyclo[6.4.0.01,3]dodecan-11-yl]acetohydrazide
by: Ahmed Benharref, et al.
Published: (2016-04-01)

(1S,3R,8R)-2,2-Dibromo-3,7,7,10-tetramethyltricyclo[6.4.0.01,3]dodec-9-en-11-one
by: Abdelouahd Oukhrib, et al.
Published: (2012-12-01)

(1S,2R,3S,6S,7R)-3,7,11,11-Tetramethyl-6,7-epoxybicyclo[5.4.0]undecane-2-ol
by: Mohamed Loubidi, et al.
Published: (2014-05-01)

Synthesis and Dihydropteridine Reductase [EC 1.6.99.10] (Human) Activity of Reduced 2,7-Dimethylpteridin-4(3H)-one, 2-Methyl-2-desaminoneopterin [6-(1' S,2' R-1' ,2' ,3' -trihydroxypropyl)-2-methylpteridin-4(3H)one] and 2-Methyl-2-desaminobiopterin [6-(1' R,2' S-1',2'-dihydroxypropyl)- 2-methylpteridin-4(3 H)-one]
by: Matsuura Sadao, et al.
Published: (1989-05-01)

SOLUTION AND SOLID STATE MOLECULAR STRUCTURES OF DIALKYLTIN(IV) β-NAPHTHOATES : [R2Sn(OCOC10H7)}2O]2, R2Sn(OCOC10H7)2 AND (CH3)4N+[R2Sn(OCOC10H7)3]- (R= n-C4H9 and CH3). X-RAY CRYSTAL STRUCTURES OF [{n-C4H9)2Sn(OCOC10H7)}2O]2 AND [(n-C4H9)2Sn(OCOC10H7)2]
by: Kapoor, Ramesh, et al.
Published: (2002-10-01)

Crystal structure of (1R,2S,3R,5S,8S,9S,10S,155)-9,10,15-trihydroxy- 2,12,124rimethyl-6-methylene-7-oxo-17-oxapentacyclo-[7.6.2.15,8.01,11.02,8]octadec-3-yl acetate sesquihydrate,C22H30O7·1.5H2O
by: Shi Hao, et al.
Published: (2009-04-01)

(3aR,6R)-3,3,6-Trimethyl-3,3a,4,5,6,7-hexahydro-2H-indazole-2-carbothioamide
by: Abdellah N'Ait Ousidi, et al.
Published: (2016-04-01)

(2R,3aR,4S,7R,7aS,9R,10aR,11S,14R,14aS)-rel-3a,4,7,7a,10a,11,14,14a-Octahydro-4,14:7,11-diepoxy-2,9-propanonaphtho[1,2-f:5,6-f′]diisoindole-1,3,8,10-tetrone (9CI): a cyclophane derived from naphtho[1,2-c:5,6-c]difuran
by: Peter W. Dibble, et al.
Published: (2008-09-01)

(1S,3S,8R,9S,11R)-10,10-Dichloro-3,7,7,11-tetramethyltetracyclo[6.5.0.01,3.09,11]tridecane
by: Ahmed Benharref, et al.
Published: (2013-06-01)