RSM and ANN approach for optimization of ultrasonic assisted extraction of pumpkin seed oil and their quality assessment

The current study focuses on optimization of process parameters for ultrasonic assisted extraction (UAE) of pumpkin seed oil (PSO) using response surface methodology (RSM) and artificial neural network (ANN). Three parameters of UAE process, amplitude, time and solvent to seed (S:S) ratio were selec...

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Main Authors: Arunima Singh, Vivek Kumar
Format: Article
Language:English
Published: Elsevier 2023-12-01
Series:Food Chemistry Advances
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2772753X23003738
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author Arunima Singh
Vivek Kumar
author_facet Arunima Singh
Vivek Kumar
author_sort Arunima Singh
collection DOAJ
description The current study focuses on optimization of process parameters for ultrasonic assisted extraction (UAE) of pumpkin seed oil (PSO) using response surface methodology (RSM) and artificial neural network (ANN). Three parameters of UAE process, amplitude, time and solvent to seed (S:S) ratio were selected in the range of 20–40 %, 15–45 min and 2–6 mL/g respectively and optimized on the basis of responses viz. yield, total phenolic compounds (TPC), squalene content and induction time of oil. The optimum process conditions of UAE were obtained as amplitude- 34.76 %, time- 34.37 min and the S:S ratio 6 mL/g. Under these optimum conditions, the oil showed good yield 39.05 %, TPC 45.02 mg GAE/g, squalene content 447.4 mg/100 g and induction time 5.27 h. The ANN model was developed using multilayer perceptron (MLP) and trained with back propagation algorithm utilizing training data set. The results indicate that the predicted values of responses by ANN model were in good agreement with the experimental values than the RSM model. The UAE-PSO showed better retention of bioactive compounds along with far better oil stability as compared to SE-PSO. The Scanning electron microscopy (SEM) analysis showed the random porous pores and rupture cell wall matrix in UAE treated seed powder.
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spelling doaj.art-fa0ac226b4e242ff97b8442fe3cf4ffa2023-12-22T05:35:25ZengElsevierFood Chemistry Advances2772-753X2023-12-013100552RSM and ANN approach for optimization of ultrasonic assisted extraction of pumpkin seed oil and their quality assessmentArunima Singh0Vivek Kumar1Department of Food Technology, Harcourt Butler Technical University, Kanpur 208002 U.P., IndiaCorresponding author.; Department of Food Technology, Harcourt Butler Technical University, Kanpur 208002 U.P., IndiaThe current study focuses on optimization of process parameters for ultrasonic assisted extraction (UAE) of pumpkin seed oil (PSO) using response surface methodology (RSM) and artificial neural network (ANN). Three parameters of UAE process, amplitude, time and solvent to seed (S:S) ratio were selected in the range of 20–40 %, 15–45 min and 2–6 mL/g respectively and optimized on the basis of responses viz. yield, total phenolic compounds (TPC), squalene content and induction time of oil. The optimum process conditions of UAE were obtained as amplitude- 34.76 %, time- 34.37 min and the S:S ratio 6 mL/g. Under these optimum conditions, the oil showed good yield 39.05 %, TPC 45.02 mg GAE/g, squalene content 447.4 mg/100 g and induction time 5.27 h. The ANN model was developed using multilayer perceptron (MLP) and trained with back propagation algorithm utilizing training data set. The results indicate that the predicted values of responses by ANN model were in good agreement with the experimental values than the RSM model. The UAE-PSO showed better retention of bioactive compounds along with far better oil stability as compared to SE-PSO. The Scanning electron microscopy (SEM) analysis showed the random porous pores and rupture cell wall matrix in UAE treated seed powder.http://www.sciencedirect.com/science/article/pii/S2772753X23003738Pumpkin seed oilUltrasonic assisted extractionSqualene contentOil induction timeRSMANN
spellingShingle Arunima Singh
Vivek Kumar
RSM and ANN approach for optimization of ultrasonic assisted extraction of pumpkin seed oil and their quality assessment
Food Chemistry Advances
Pumpkin seed oil
Ultrasonic assisted extraction
Squalene content
Oil induction time
RSM
ANN
title RSM and ANN approach for optimization of ultrasonic assisted extraction of pumpkin seed oil and their quality assessment
title_full RSM and ANN approach for optimization of ultrasonic assisted extraction of pumpkin seed oil and their quality assessment
title_fullStr RSM and ANN approach for optimization of ultrasonic assisted extraction of pumpkin seed oil and their quality assessment
title_full_unstemmed RSM and ANN approach for optimization of ultrasonic assisted extraction of pumpkin seed oil and their quality assessment
title_short RSM and ANN approach for optimization of ultrasonic assisted extraction of pumpkin seed oil and their quality assessment
title_sort rsm and ann approach for optimization of ultrasonic assisted extraction of pumpkin seed oil and their quality assessment
topic Pumpkin seed oil
Ultrasonic assisted extraction
Squalene content
Oil induction time
RSM
ANN
url http://www.sciencedirect.com/science/article/pii/S2772753X23003738
work_keys_str_mv AT arunimasingh rsmandannapproachforoptimizationofultrasonicassistedextractionofpumpkinseedoilandtheirqualityassessment
AT vivekkumar rsmandannapproachforoptimizationofultrasonicassistedextractionofpumpkinseedoilandtheirqualityassessment