Ultra-sensitive ppb-level methane detection based on NIR all-optical photoacoustic spectroscopy by using differential fiber-optic microphones with gold-chromium composite nanomembrane
In this paper, we propose and experimentally demonstrate an ultra-sensitive all-optical PAS gas sensor, incorporating with a near-infrared (NIR) diode laser, fiber-optic microphones (FOMs) and a double channel differential T-type photoacoustic cell. The FOM is realized by Fabry-Perot interferometry...
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Elsevier
2022-06-01
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Online Access: | http://www.sciencedirect.com/science/article/pii/S2213597922000222 |
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author | Hanping Xiao Jinbiao Zhao Chaotan Sima Ping Lu Yanhong Long Yan Ai Wanjin Zhang Yufeng Pan Jiangshan Zhang Deming Liu |
author_facet | Hanping Xiao Jinbiao Zhao Chaotan Sima Ping Lu Yanhong Long Yan Ai Wanjin Zhang Yufeng Pan Jiangshan Zhang Deming Liu |
author_sort | Hanping Xiao |
collection | DOAJ |
description | In this paper, we propose and experimentally demonstrate an ultra-sensitive all-optical PAS gas sensor, incorporating with a near-infrared (NIR) diode laser, fiber-optic microphones (FOMs) and a double channel differential T-type photoacoustic cell. The FOM is realized by Fabry-Perot interferometry and novel gold-chromium (Au-Cr) composite nanomembranes. To meet the demand of high sensitivity and flat frequency response for the FOMs, the Au-Cr composite diaphragm is deliberately designed and fabricated by E-beam evaporation deposition with 330 nm in thickness and 6.35 mm in radius. Experimental results show that the FOM has a sensitivity of about 30 V/Pa and a flat frequency response from 300 to 900 Hz with fluctuation below 1 dB. Moreover, a double channel differential T-type photoacoustic cell is designed and employed in the all-optical PAS gas sensor, with the first-order resonant frequency of 610 Hz. The all-optical gas sensor is established and verified for CH4 detection and the normalized noise equivalent absorption (NNEA) is 4.42 × 10−10 W∙cm−1∙Hz−1/2. The minimum detection limit (MDL) of 36.45 ppb is achieved with a 1 s integration time. The MDL could be further enhanced to 4.87 ppb with an integration time of 81 s, allowing ultra-sensitive trace gas detection. |
first_indexed | 2024-04-14T04:57:28Z |
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id | doaj.art-fa8c6924cafd4567a891d12c77e0ba80 |
institution | Directory Open Access Journal |
issn | 2213-5979 |
language | English |
last_indexed | 2024-04-14T04:57:28Z |
publishDate | 2022-06-01 |
publisher | Elsevier |
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series | Photoacoustics |
spelling | doaj.art-fa8c6924cafd4567a891d12c77e0ba802022-12-22T02:11:07ZengElsevierPhotoacoustics2213-59792022-06-0126100353Ultra-sensitive ppb-level methane detection based on NIR all-optical photoacoustic spectroscopy by using differential fiber-optic microphones with gold-chromium composite nanomembraneHanping Xiao0Jinbiao Zhao1Chaotan Sima2Ping Lu3Yanhong Long4Yan Ai5Wanjin Zhang6Yufeng Pan7Jiangshan Zhang8Deming Liu9Wuhan National Laboratory for Optoelectronics (WNLO) and National Engineering Laboratory for Next Generation Internet Access System, School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan 430074, China; Shenzhen Huazhong University of Science and Technology Research Institute, Shenzhen 518000, ChinaWuhan National Laboratory for Optoelectronics (WNLO) and National Engineering Laboratory for Next Generation Internet Access System, School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan 430074, China; Shenzhen Huazhong University of Science and Technology Research Institute, Shenzhen 518000, ChinaWuhan National Laboratory for Optoelectronics (WNLO) and National Engineering Laboratory for Next Generation Internet Access System, School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan 430074, China; Shenzhen Huazhong University of Science and Technology Research Institute, Shenzhen 518000, China; Corresponding authors at: Wuhan National Laboratory for Optoelectronics (WNLO) and National Engineering Laboratory for Next Generation Internet Access System, School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan 430074, ChinaWuhan National Laboratory for Optoelectronics (WNLO) and National Engineering Laboratory for Next Generation Internet Access System, School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan 430074, China; Shenzhen Huazhong University of Science and Technology Research Institute, Shenzhen 518000, China; Corresponding authors at: Wuhan National Laboratory for Optoelectronics (WNLO) and National Engineering Laboratory for Next Generation Internet Access System, School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan 430074, ChinaWuhan National Laboratory for Optoelectronics (WNLO) and National Engineering Laboratory for Next Generation Internet Access System, School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan 430074, ChinaWuhan National Laboratory for Optoelectronics (WNLO) and National Engineering Laboratory for Next Generation Internet Access System, School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan 430074, ChinaWuhan National Laboratory for Optoelectronics (WNLO) and National Engineering Laboratory for Next Generation Internet Access System, School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan 430074, ChinaWuhan National Laboratory for Optoelectronics (WNLO) and National Engineering Laboratory for Next Generation Internet Access System, School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan 430074, ChinaDepartment of Electronics and Information Engineering, Huazhong University of Science and Technology, Wuhan 430074, ChinaWuhan National Laboratory for Optoelectronics (WNLO) and National Engineering Laboratory for Next Generation Internet Access System, School of Optical and Electronic Information, Huazhong University of Science and Technology, Wuhan 430074, ChinaIn this paper, we propose and experimentally demonstrate an ultra-sensitive all-optical PAS gas sensor, incorporating with a near-infrared (NIR) diode laser, fiber-optic microphones (FOMs) and a double channel differential T-type photoacoustic cell. The FOM is realized by Fabry-Perot interferometry and novel gold-chromium (Au-Cr) composite nanomembranes. To meet the demand of high sensitivity and flat frequency response for the FOMs, the Au-Cr composite diaphragm is deliberately designed and fabricated by E-beam evaporation deposition with 330 nm in thickness and 6.35 mm in radius. Experimental results show that the FOM has a sensitivity of about 30 V/Pa and a flat frequency response from 300 to 900 Hz with fluctuation below 1 dB. Moreover, a double channel differential T-type photoacoustic cell is designed and employed in the all-optical PAS gas sensor, with the first-order resonant frequency of 610 Hz. The all-optical gas sensor is established and verified for CH4 detection and the normalized noise equivalent absorption (NNEA) is 4.42 × 10−10 W∙cm−1∙Hz−1/2. The minimum detection limit (MDL) of 36.45 ppb is achieved with a 1 s integration time. The MDL could be further enhanced to 4.87 ppb with an integration time of 81 s, allowing ultra-sensitive trace gas detection.http://www.sciencedirect.com/science/article/pii/S2213597922000222InfraredPhotoacoustic spectroscopyFiber-optic microphoneGas detection |
spellingShingle | Hanping Xiao Jinbiao Zhao Chaotan Sima Ping Lu Yanhong Long Yan Ai Wanjin Zhang Yufeng Pan Jiangshan Zhang Deming Liu Ultra-sensitive ppb-level methane detection based on NIR all-optical photoacoustic spectroscopy by using differential fiber-optic microphones with gold-chromium composite nanomembrane Photoacoustics Infrared Photoacoustic spectroscopy Fiber-optic microphone Gas detection |
title | Ultra-sensitive ppb-level methane detection based on NIR all-optical photoacoustic spectroscopy by using differential fiber-optic microphones with gold-chromium composite nanomembrane |
title_full | Ultra-sensitive ppb-level methane detection based on NIR all-optical photoacoustic spectroscopy by using differential fiber-optic microphones with gold-chromium composite nanomembrane |
title_fullStr | Ultra-sensitive ppb-level methane detection based on NIR all-optical photoacoustic spectroscopy by using differential fiber-optic microphones with gold-chromium composite nanomembrane |
title_full_unstemmed | Ultra-sensitive ppb-level methane detection based on NIR all-optical photoacoustic spectroscopy by using differential fiber-optic microphones with gold-chromium composite nanomembrane |
title_short | Ultra-sensitive ppb-level methane detection based on NIR all-optical photoacoustic spectroscopy by using differential fiber-optic microphones with gold-chromium composite nanomembrane |
title_sort | ultra sensitive ppb level methane detection based on nir all optical photoacoustic spectroscopy by using differential fiber optic microphones with gold chromium composite nanomembrane |
topic | Infrared Photoacoustic spectroscopy Fiber-optic microphone Gas detection |
url | http://www.sciencedirect.com/science/article/pii/S2213597922000222 |
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