Isolation, Modification and Characterization of Tiger-Nut, Maize, Cassava and Potato Starch

Four different sources of starchy foods were used for the isolation of starch using commercially cheap and readily available chemical-hypo (3.5 % active Chlorine). The isolated starch was modified through NaIO4 oxidation under mild reaction conditions. Carbonyl functional group test was employed fo...

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Bibliographic Details
Main Authors: Y Azeh, YB Paiko, AY Abubakar, B Garba, OAE Ameh
Format: Article
Language:English
Published: Joint Coordination Centre of the World Bank assisted National Agricultural Research Programme (NARP) 2018-06-01
Series:Journal of Applied Sciences and Environmental Management
Subjects:
Online Access:https://www.ajol.info/index.php/jasem/article/view/172686
Description
Summary:Four different sources of starchy foods were used for the isolation of starch using commercially cheap and readily available chemical-hypo (3.5 % active Chlorine). The isolated starch was modified through NaIO4 oxidation under mild reaction conditions. Carbonyl functional group test was employed for confirmation of the success of oxidation. FT-IR and Scanning Electron Microscopy (SEM) were used for functional group identification and morphological examination of both modified and native samples to further confirm the success of modification. The appearance of the carbonyl band at 1747-1746 cm-1 and 1647 – 1637 cm-1 indicated the successful synthesis of oxidized starch. Proximate results showed that the isolated starches were rich in mineral content: 0.25-2.13; crude fibre: 0.85-3.31; fat: 0.23-0.28 and energy: 1331-1410. The study showed that commercial hypo could be a useful replacement for metabisulphite for starch isolation without side effects on starch properties. SEM images showed that morphological architecture of granules was not destroyed during surface functionalization. Characteristic and nutritional features of the oxidized starch showed that it could find useful applications in food and pharmaceutical industries.
ISSN:2659-1502
2659-1499