Analysis of Preparation and Properties on Shape Memory Hydrogenated Epoxy Resin Used for Asphalt Mixtures
The objective of this investigation is to prepare the shape memory hydrogenated epoxy resin used for asphalt mixtures (SM-HEP-AM) and study its properties. The shape memory hydrogenated epoxy resin (SM-HEP) is prepared using hydrogenated bisphenol A epoxy resin (AL-3040), polypropylene glycol diglyc...
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MDPI AG
2017-05-01
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| Series: | Applied Sciences |
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| Online Access: | http://www.mdpi.com/2076-3417/7/6/523 |
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| author | Biao Ma Xueyan Zhou Kun Wei Yanzhen Bo Zhanping You |
| author_facet | Biao Ma Xueyan Zhou Kun Wei Yanzhen Bo Zhanping You |
| author_sort | Biao Ma |
| collection | DOAJ |
| description | The objective of this investigation is to prepare the shape memory hydrogenated epoxy resin used for asphalt mixtures (SM-HEP-AM) and study its properties. The shape memory hydrogenated epoxy resin (SM-HEP) is prepared using hydrogenated bisphenol A epoxy resin (AL-3040), polypropylene glycol diglycidylether diacrylate (JH-230), and isophorone diamine (IPDA). The formulations of the SM-HEP-AM are obtained by the linearly fitted method. The thermo-mechanical property, molecular structure, and shape-memory performance of the SM-HEP-AM are studied. The glass-transition temperature (Tg) is determined using the differential scanning calorimeter (DSC). The results proved that the Tg level increased when the JH-230 content decreased. The thermo-mechanical property of the SM-HEP-AM is measured by dynamical mechanical analysis (DMA). The storage modulus of the SM-HEP-AM decreased with the increase in the JH-230 content. The above phenomena are attributed to the change in the JH-230 content. The shape memory performance results of the SM-HEP-AM indicate that specimen deformation can completely recover after only several minutes at Tg + 10 °C and Tg + 20 °C. The shape recovery time of the SM-HEP-AM increases with increased JH-230 content, and the change between the shape recovery time and JH-230 content gradually decreased as the temperature increased. The deformation recovery performance of asphalt mixture with and without the SM-HEP-AM (Tg = 40 °C) was tested by the deformation recovery test. This was used to prove that the SM-HEP-AM helps to improve the deformation recovery performance of the asphalt mixture. |
| first_indexed | 2024-12-20T20:37:49Z |
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| id | doaj.art-fcba79e7d3f14f92a3020f385029c853 |
| institution | Directory Open Access Journal |
| issn | 2076-3417 |
| language | English |
| last_indexed | 2024-12-20T20:37:49Z |
| publishDate | 2017-05-01 |
| publisher | MDPI AG |
| record_format | Article |
| series | Applied Sciences |
| spelling | doaj.art-fcba79e7d3f14f92a3020f385029c8532022-12-21T19:27:12ZengMDPI AGApplied Sciences2076-34172017-05-017652310.3390/app7060523app7060523Analysis of Preparation and Properties on Shape Memory Hydrogenated Epoxy Resin Used for Asphalt MixturesBiao Ma0Xueyan Zhou1Kun Wei2Yanzhen Bo3Zhanping You4Key Laboratory for Special Area Highway Engineering of Ministry of Education, Chang’an University, Xi’an 710064, ChinaKey Laboratory for Special Area Highway Engineering of Ministry of Education, Chang’an University, Xi’an 710064, ChinaKey Laboratory for Special Area Highway Engineering of Ministry of Education, Chang’an University, Xi’an 710064, ChinaKey Laboratory for Special Area Highway Engineering of Ministry of Education, Chang’an University, Xi’an 710064, ChinaKey Laboratory for Special Area Highway Engineering of Ministry of Education, Chang’an University, Xi’an 710064, ChinaThe objective of this investigation is to prepare the shape memory hydrogenated epoxy resin used for asphalt mixtures (SM-HEP-AM) and study its properties. The shape memory hydrogenated epoxy resin (SM-HEP) is prepared using hydrogenated bisphenol A epoxy resin (AL-3040), polypropylene glycol diglycidylether diacrylate (JH-230), and isophorone diamine (IPDA). The formulations of the SM-HEP-AM are obtained by the linearly fitted method. The thermo-mechanical property, molecular structure, and shape-memory performance of the SM-HEP-AM are studied. The glass-transition temperature (Tg) is determined using the differential scanning calorimeter (DSC). The results proved that the Tg level increased when the JH-230 content decreased. The thermo-mechanical property of the SM-HEP-AM is measured by dynamical mechanical analysis (DMA). The storage modulus of the SM-HEP-AM decreased with the increase in the JH-230 content. The above phenomena are attributed to the change in the JH-230 content. The shape memory performance results of the SM-HEP-AM indicate that specimen deformation can completely recover after only several minutes at Tg + 10 °C and Tg + 20 °C. The shape recovery time of the SM-HEP-AM increases with increased JH-230 content, and the change between the shape recovery time and JH-230 content gradually decreased as the temperature increased. The deformation recovery performance of asphalt mixture with and without the SM-HEP-AM (Tg = 40 °C) was tested by the deformation recovery test. This was used to prove that the SM-HEP-AM helps to improve the deformation recovery performance of the asphalt mixture.http://www.mdpi.com/2076-3417/7/6/523road engineeringasphalt mixtureshape-memory hydrogenated epoxy resinglass-transition temperatureshape-memory performance |
| spellingShingle | Biao Ma Xueyan Zhou Kun Wei Yanzhen Bo Zhanping You Analysis of Preparation and Properties on Shape Memory Hydrogenated Epoxy Resin Used for Asphalt Mixtures Applied Sciences road engineering asphalt mixture shape-memory hydrogenated epoxy resin glass-transition temperature shape-memory performance |
| title | Analysis of Preparation and Properties on Shape Memory Hydrogenated Epoxy Resin Used for Asphalt Mixtures |
| title_full | Analysis of Preparation and Properties on Shape Memory Hydrogenated Epoxy Resin Used for Asphalt Mixtures |
| title_fullStr | Analysis of Preparation and Properties on Shape Memory Hydrogenated Epoxy Resin Used for Asphalt Mixtures |
| title_full_unstemmed | Analysis of Preparation and Properties on Shape Memory Hydrogenated Epoxy Resin Used for Asphalt Mixtures |
| title_short | Analysis of Preparation and Properties on Shape Memory Hydrogenated Epoxy Resin Used for Asphalt Mixtures |
| title_sort | analysis of preparation and properties on shape memory hydrogenated epoxy resin used for asphalt mixtures |
| topic | road engineering asphalt mixture shape-memory hydrogenated epoxy resin glass-transition temperature shape-memory performance |
| url | http://www.mdpi.com/2076-3417/7/6/523 |
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