The Effects of Deposition Time on Phase and Structure of FeCoNi Films

This study aims to determine the effects of deposition time on the phase and structure of FeCoNi. FeCoNi was prepared by electrodeposition method at room temperature. X-ray diffraction measurement shows the formation of a single phase of FeCoNi at 5 and 10 minutes of deposition, while at 20, 35, and...

Full description

Bibliographic Details
Main Authors: Muhamad Mulyadi, Afrizal
Format: Article
Language:English
Published: The Center for Science Innovation 2022-06-01
Series:Chemistry and Materials
Subjects:
Online Access:https://piscience.org/index.php/cma/article/view/23
_version_ 1797777532122038272
author Muhamad Mulyadi
Afrizal
author_facet Muhamad Mulyadi
Afrizal
author_sort Muhamad Mulyadi
collection DOAJ
description This study aims to determine the effects of deposition time on the phase and structure of FeCoNi. FeCoNi was prepared by electrodeposition method at room temperature. X-ray diffraction measurement shows the formation of a single phase of FeCoNi at 5 and 10 minutes of deposition, while at 20, 35, and 50 minutes, a new phase was formed, namely CoNi. The obtained FeCoNi and CoNi show a crystal plane at 2θ = 44.05° (111); 51.33° (002); and 75.59° (022) in all different deposition times, indicating the face centered cubic crystal structure. The effect of deposition time on the chemicals composition shows an anomalous co-deposition because Fe has a larger ratio than Co and Ni. The deposition rate and the value of current efficiency were found to be optimum at FeCoNi synthesized for 20 minutes, namely 0.00214 mg/cm2s and 97.00%.
first_indexed 2024-03-12T23:05:16Z
format Article
id doaj.art-fd39daa611bc4091bd844491cedfa228
institution Directory Open Access Journal
issn 2828-271X
2828-2310
language English
last_indexed 2024-03-12T23:05:16Z
publishDate 2022-06-01
publisher The Center for Science Innovation
record_format Article
series Chemistry and Materials
spelling doaj.art-fd39daa611bc4091bd844491cedfa2282023-07-19T02:26:46ZengThe Center for Science InnovationChemistry and Materials2828-271X2828-23102022-06-0112404410.56425/cma.v1i2.2323The Effects of Deposition Time on Phase and Structure of FeCoNi FilmsMuhamad Mulyadi0Afrizal1Universitas Negeri JakartaUniversitas Negeri JakartaThis study aims to determine the effects of deposition time on the phase and structure of FeCoNi. FeCoNi was prepared by electrodeposition method at room temperature. X-ray diffraction measurement shows the formation of a single phase of FeCoNi at 5 and 10 minutes of deposition, while at 20, 35, and 50 minutes, a new phase was formed, namely CoNi. The obtained FeCoNi and CoNi show a crystal plane at 2θ = 44.05° (111); 51.33° (002); and 75.59° (022) in all different deposition times, indicating the face centered cubic crystal structure. The effect of deposition time on the chemicals composition shows an anomalous co-deposition because Fe has a larger ratio than Co and Ni. The deposition rate and the value of current efficiency were found to be optimum at FeCoNi synthesized for 20 minutes, namely 0.00214 mg/cm2s and 97.00%.https://piscience.org/index.php/cma/article/view/23feconiphasestructurecurrent efficiencydeposition rate
spellingShingle Muhamad Mulyadi
Afrizal
The Effects of Deposition Time on Phase and Structure of FeCoNi Films
Chemistry and Materials
feconi
phase
structure
current efficiency
deposition rate
title The Effects of Deposition Time on Phase and Structure of FeCoNi Films
title_full The Effects of Deposition Time on Phase and Structure of FeCoNi Films
title_fullStr The Effects of Deposition Time on Phase and Structure of FeCoNi Films
title_full_unstemmed The Effects of Deposition Time on Phase and Structure of FeCoNi Films
title_short The Effects of Deposition Time on Phase and Structure of FeCoNi Films
title_sort effects of deposition time on phase and structure of feconi films
topic feconi
phase
structure
current efficiency
deposition rate
url https://piscience.org/index.php/cma/article/view/23
work_keys_str_mv AT muhamadmulyadi theeffectsofdepositiontimeonphaseandstructureoffeconifilms
AT afrizal theeffectsofdepositiontimeonphaseandstructureoffeconifilms
AT muhamadmulyadi effectsofdepositiontimeonphaseandstructureoffeconifilms
AT afrizal effectsofdepositiontimeonphaseandstructureoffeconifilms