Effect of Freezing Ball Milling Treatment on the Structure, Properties and Digestibility of Waxy Rice Starch

This study investigated the effect of freezing ball milling treatment on the structure, properties and digestibility of waxy rice starch, prepared by alkaline extraction. The effects of treatment time on the particle size distribution, microstructure, crystalline structure, short-range ordered struc...

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Main Author: HAO Zongwei, YU Zhenyu, HU Yao, WANG Naifu, XIAO Yaqing, LIU Yingnan, ZHANG Qiang, LIU Kang, WANG Feng, HAN Shengjun, ZHOU Yibin
Format: Article
Language:English
Published: China Food Publishing Company 2023-06-01
Series:Shipin Kexue
Subjects:
Online Access:https://www.spkx.net.cn/fileup/1002-6630/PDF/2023-44-11-006.pdf
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author HAO Zongwei, YU Zhenyu, HU Yao, WANG Naifu, XIAO Yaqing, LIU Yingnan, ZHANG Qiang, LIU Kang, WANG Feng, HAN Shengjun, ZHOU Yibin
author_facet HAO Zongwei, YU Zhenyu, HU Yao, WANG Naifu, XIAO Yaqing, LIU Yingnan, ZHANG Qiang, LIU Kang, WANG Feng, HAN Shengjun, ZHOU Yibin
author_sort HAO Zongwei, YU Zhenyu, HU Yao, WANG Naifu, XIAO Yaqing, LIU Yingnan, ZHANG Qiang, LIU Kang, WANG Feng, HAN Shengjun, ZHOU Yibin
collection DOAJ
description This study investigated the effect of freezing ball milling treatment on the structure, properties and digestibility of waxy rice starch, prepared by alkaline extraction. The effects of treatment time on the particle size distribution, microstructure, crystalline structure, short-range ordered structure, pasting properties, thermodynamic properties and digestibility of waxy rice starch were examined. The results showed that after freezing ball milling treatment, the integrity of starch granules was damaged with cracks appearing on the surface, the particle size tended to increase, and the crystalline structure and short-range ordered structure were severely damaged. The water absorption index increased from 2.15 to 7.31 g/g, and the cold water solubility and swelling power increased significantly from 2.97% and 3.25% to 46.33% and 15.50%, respectively in the 80 min ball milling group compared with untreated samples (P < 0.05). The enthalpy change (ΔH) decreased from 9.33 to 1.79 J/g, and the degree of gelatinization significantly increased (P < 0.05). The birefringence of the starch gradually disappeared with increasing treatment time. The rapidly digestible starch (RDS) content of waxy rice starch increased significantly (P < 0.05), while the contents of resistant starch (RS) and slowly digestible starch (SDS) decreased significantly (P < 0.05). This study provides basic data and references for the production of modified starch products with novel structures and properties.
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spelling doaj.art-fd5ce7841f6745e38159face3ae02e7a2023-07-25T06:04:40ZengChina Food Publishing CompanyShipin Kexue1002-66302023-06-014411394710.7506/spkx1002-6630-20220423-298Effect of Freezing Ball Milling Treatment on the Structure, Properties and Digestibility of Waxy Rice StarchHAO Zongwei, YU Zhenyu, HU Yao, WANG Naifu, XIAO Yaqing, LIU Yingnan, ZHANG Qiang, LIU Kang, WANG Feng, HAN Shengjun, ZHOU Yibin0(Anhui Engineering Laboratory for Agro-products Processing, Food Processing Research Institute, School of Tea and Food Science and Technology, Anhui Agricultural University, Hefei 230036, China)This study investigated the effect of freezing ball milling treatment on the structure, properties and digestibility of waxy rice starch, prepared by alkaline extraction. The effects of treatment time on the particle size distribution, microstructure, crystalline structure, short-range ordered structure, pasting properties, thermodynamic properties and digestibility of waxy rice starch were examined. The results showed that after freezing ball milling treatment, the integrity of starch granules was damaged with cracks appearing on the surface, the particle size tended to increase, and the crystalline structure and short-range ordered structure were severely damaged. The water absorption index increased from 2.15 to 7.31 g/g, and the cold water solubility and swelling power increased significantly from 2.97% and 3.25% to 46.33% and 15.50%, respectively in the 80 min ball milling group compared with untreated samples (P < 0.05). The enthalpy change (ΔH) decreased from 9.33 to 1.79 J/g, and the degree of gelatinization significantly increased (P < 0.05). The birefringence of the starch gradually disappeared with increasing treatment time. The rapidly digestible starch (RDS) content of waxy rice starch increased significantly (P < 0.05), while the contents of resistant starch (RS) and slowly digestible starch (SDS) decreased significantly (P < 0.05). This study provides basic data and references for the production of modified starch products with novel structures and properties.https://www.spkx.net.cn/fileup/1002-6630/PDF/2023-44-11-006.pdfwaxy rice starch; freezing ball milling; structure; digestibility
spellingShingle HAO Zongwei, YU Zhenyu, HU Yao, WANG Naifu, XIAO Yaqing, LIU Yingnan, ZHANG Qiang, LIU Kang, WANG Feng, HAN Shengjun, ZHOU Yibin
Effect of Freezing Ball Milling Treatment on the Structure, Properties and Digestibility of Waxy Rice Starch
Shipin Kexue
waxy rice starch; freezing ball milling; structure; digestibility
title Effect of Freezing Ball Milling Treatment on the Structure, Properties and Digestibility of Waxy Rice Starch
title_full Effect of Freezing Ball Milling Treatment on the Structure, Properties and Digestibility of Waxy Rice Starch
title_fullStr Effect of Freezing Ball Milling Treatment on the Structure, Properties and Digestibility of Waxy Rice Starch
title_full_unstemmed Effect of Freezing Ball Milling Treatment on the Structure, Properties and Digestibility of Waxy Rice Starch
title_short Effect of Freezing Ball Milling Treatment on the Structure, Properties and Digestibility of Waxy Rice Starch
title_sort effect of freezing ball milling treatment on the structure properties and digestibility of waxy rice starch
topic waxy rice starch; freezing ball milling; structure; digestibility
url https://www.spkx.net.cn/fileup/1002-6630/PDF/2023-44-11-006.pdf
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