Structural and spectral properties of YAG:Nd, YAG:Ce and YAG:Yb nanocrystalline powders synthesized via modified Pechini method

Synthesis of nanocrystalline yttrium-aluminum garnet doped with neodymium was performed via modified Pechini methods. Evolution of material during synthesis was studied using differential thermal analysis; the structure and morphology of synthesized nanopowders were studied using scanning electron...

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Main Authors: Amir Moussaoui, Dmitry V. Bulyga, Aleksandr I. Ignatiev, Sergey K. Evstropiev, Nikolay V. Nikonorov
Format: Article
Language:English
Published: Saint Petersburg National Research University of Information Technologies, Mechanics and Optics (ITMO University) 2024-02-01
Series:Naučno-tehničeskij Vestnik Informacionnyh Tehnologij, Mehaniki i Optiki
Subjects:
Online Access:https://ntv.ifmo.ru/file/article/22573.pdf
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author Amir Moussaoui
Dmitry V. Bulyga
Aleksandr I. Ignatiev
Sergey K. Evstropiev
Nikolay V. Nikonorov
author_facet Amir Moussaoui
Dmitry V. Bulyga
Aleksandr I. Ignatiev
Sergey K. Evstropiev
Nikolay V. Nikonorov
author_sort Amir Moussaoui
collection DOAJ
description Synthesis of nanocrystalline yttrium-aluminum garnet doped with neodymium was performed via modified Pechini methods. Evolution of material during synthesis was studied using differential thermal analysis; the structure and morphology of synthesized nanopowders were studied using scanning electron microscopy and x-ray diffraction. It was shown that the use of an additional low-temperature stabilizer leads to formation of crystalline yttrium-aluminum garnet phase at lower temperatures. It was shown that the formation of nanocrystals occurs at the temperature of about 883 °C. Obtained powders can be used as precursors for ceramics sintering or be introduced into the optical fiber in order to fabricate optical amplifiers.
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spelling doaj.art-fda58a47b5b347c6a354e54b690039aa2024-02-13T09:53:50ZengSaint Petersburg National Research University of Information Technologies, Mechanics and Optics (ITMO University)Naučno-tehničeskij Vestnik Informacionnyh Tehnologij, Mehaniki i Optiki2226-14942500-03732024-02-0124111010.17586/2226-1494-2024-24-1-1-10Structural and spectral properties of YAG:Nd, YAG:Ce and YAG:Yb nanocrystalline powders synthesized via modified Pechini methodAmir Moussaoui0https://orcid.org/0000-0002-7858-7417Dmitry V. Bulyga1https://orcid.org/0000-0001-8861-2527Aleksandr I. Ignatiev2https://orcid.org/0000-0002-6114-0248Sergey K. Evstropiev3https://orcid.org/0000-0002-0160-8443Nikolay V. Nikonorov4https://orcid.org/0000-0002-1341-067XPhD Student, ITMO University, Saint Petersburg, 197101, Russian FederationPhD Student, ITMO University, Saint Petersburg, 197101, Russian Federation; Senior Researcher, JVC “RPA Vavilov State Optical Institute”, Saint Petersburg, 192171, Russian Federation, sc 57217158694Leading Engineer, ITMO University, Saint Petersburg, 197101, Russian Federation, sc 57189902013D.Sc. (Chemistry), Leading Researcher, ITMO University, Saint Petersburg, 197101, Russian Federation; Head of Department, JVC “RPA Vavilov State Optical Institute”, Saint Petersburg, 192171, Russian Federation; Professor, Saint Petersburg State Institute of Technology, Saint Petersburg, 190013, Russian Federation, sc 6507317768D.Sc. (Physics & Mathematics), Full Professor, ITMO University, Saint Petersburg, 197101, Russian Federation, sc 7003772604Synthesis of nanocrystalline yttrium-aluminum garnet doped with neodymium was performed via modified Pechini methods. Evolution of material during synthesis was studied using differential thermal analysis; the structure and morphology of synthesized nanopowders were studied using scanning electron microscopy and x-ray diffraction. It was shown that the use of an additional low-temperature stabilizer leads to formation of crystalline yttrium-aluminum garnet phase at lower temperatures. It was shown that the formation of nanocrystals occurs at the temperature of about 883 °C. Obtained powders can be used as precursors for ceramics sintering or be introduced into the optical fiber in order to fabricate optical amplifiers.https://ntv.ifmo.ru/file/article/22573.pdfyagluminescencepechini methodpolyvinylpyrrolidone
spellingShingle Amir Moussaoui
Dmitry V. Bulyga
Aleksandr I. Ignatiev
Sergey K. Evstropiev
Nikolay V. Nikonorov
Structural and spectral properties of YAG:Nd, YAG:Ce and YAG:Yb nanocrystalline powders synthesized via modified Pechini method
Naučno-tehničeskij Vestnik Informacionnyh Tehnologij, Mehaniki i Optiki
yag
luminescence
pechini method
polyvinylpyrrolidone
title Structural and spectral properties of YAG:Nd, YAG:Ce and YAG:Yb nanocrystalline powders synthesized via modified Pechini method
title_full Structural and spectral properties of YAG:Nd, YAG:Ce and YAG:Yb nanocrystalline powders synthesized via modified Pechini method
title_fullStr Structural and spectral properties of YAG:Nd, YAG:Ce and YAG:Yb nanocrystalline powders synthesized via modified Pechini method
title_full_unstemmed Structural and spectral properties of YAG:Nd, YAG:Ce and YAG:Yb nanocrystalline powders synthesized via modified Pechini method
title_short Structural and spectral properties of YAG:Nd, YAG:Ce and YAG:Yb nanocrystalline powders synthesized via modified Pechini method
title_sort structural and spectral properties of yag nd yag ce and yag yb nanocrystalline powders synthesized via modified pechini method
topic yag
luminescence
pechini method
polyvinylpyrrolidone
url https://ntv.ifmo.ru/file/article/22573.pdf
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