CHARACTERIZATION OF MALAYSIAN JATROPHA SEED OIL USING FTIR AND GCMS

Flow assurance problems such as wax deposition impacted the oil and gas industry in various points of oil transport hence a cure is widely researched. This paper aims to establish a cure by using Jatropha curcas seed oil (non-edible) originated from Malaysia and its sustainability as a wax inhibitor...

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Main Authors: Mathanraj Jayagobi, Amni Haslinda Alpandi, Hazlina Husin
Format: Article
Language:English
Published: UTP Press 2021-12-01
Series:Platform, a Journal of Engineering
Subjects:
Online Access:https://myjms.mohe.gov.my/index.php/paje/article/view/v5n4-3/8802
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author Mathanraj Jayagobi
Amni Haslinda Alpandi
Hazlina Husin
author_facet Mathanraj Jayagobi
Amni Haslinda Alpandi
Hazlina Husin
author_sort Mathanraj Jayagobi
collection DOAJ
description Flow assurance problems such as wax deposition impacted the oil and gas industry in various points of oil transport hence a cure is widely researched. This paper aims to establish a cure by using Jatropha curcas seed oil (non-edible) originated from Malaysia and its sustainability as a wax inhibitor component. Extraction and characterization of Jatropha seed oil using Fourier Transform Infrared Spectroscopy (FTIR) and Gas Chromatography-Mass Spectrometry (GCMS) were conducted to identify the properties of Jatropha seed oil such as the presence of oleic acid which is the main component required in wax inhibitor. Jatropha seed oil extraction was conducted using a soxhlet extractor and n-Hexane solvent which was heated at 70°C. The obtained results illustrated that at the peak of 1746.48 cm–1, FTIR analysis indicated the presence of C=O stretching carboxyl which was the ester fatty acid group while at a retention time of 36.834 min, 44.91% of the oleic acid was present via GCMS analysis. The analysis revealed the presence of high oleic acid in Jatropha seed oil has great potential as wax inhibitor to improve the flowability retarded by wax precipitation.
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spelling doaj.art-fdef8ef563f542acab5e569dc8a31f262023-08-21T04:42:31ZengUTP PressPlatform, a Journal of Engineering2636-98772021-12-01542328CHARACTERIZATION OF MALAYSIAN JATROPHA SEED OIL USING FTIR AND GCMS Mathanraj Jayagobi0Amni Haslinda Alpandi 1Hazlina Husin2Department of Petroleum Engineering, Universiti Teknologi PETRONAS, Perak, Malaysia Department of Petroleum Engineering, Universiti Teknologi PETRONAS, Perak, Malaysia Department of Petroleum Engineering, Universiti Teknologi PETRONAS, Perak, Malaysia Flow assurance problems such as wax deposition impacted the oil and gas industry in various points of oil transport hence a cure is widely researched. This paper aims to establish a cure by using Jatropha curcas seed oil (non-edible) originated from Malaysia and its sustainability as a wax inhibitor component. Extraction and characterization of Jatropha seed oil using Fourier Transform Infrared Spectroscopy (FTIR) and Gas Chromatography-Mass Spectrometry (GCMS) were conducted to identify the properties of Jatropha seed oil such as the presence of oleic acid which is the main component required in wax inhibitor. Jatropha seed oil extraction was conducted using a soxhlet extractor and n-Hexane solvent which was heated at 70°C. The obtained results illustrated that at the peak of 1746.48 cm–1, FTIR analysis indicated the presence of C=O stretching carboxyl which was the ester fatty acid group while at a retention time of 36.834 min, 44.91% of the oleic acid was present via GCMS analysis. The analysis revealed the presence of high oleic acid in Jatropha seed oil has great potential as wax inhibitor to improve the flowability retarded by wax precipitation.https://myjms.mohe.gov.my/index.php/paje/article/view/v5n4-3/8802jatropha seed oilfatty acidoleic acidwax inhibitorsoxhlet extractor
spellingShingle Mathanraj Jayagobi
Amni Haslinda Alpandi
Hazlina Husin
CHARACTERIZATION OF MALAYSIAN JATROPHA SEED OIL USING FTIR AND GCMS
Platform, a Journal of Engineering
jatropha seed oil
fatty acid
oleic acid
wax inhibitor
soxhlet extractor
title CHARACTERIZATION OF MALAYSIAN JATROPHA SEED OIL USING FTIR AND GCMS
title_full CHARACTERIZATION OF MALAYSIAN JATROPHA SEED OIL USING FTIR AND GCMS
title_fullStr CHARACTERIZATION OF MALAYSIAN JATROPHA SEED OIL USING FTIR AND GCMS
title_full_unstemmed CHARACTERIZATION OF MALAYSIAN JATROPHA SEED OIL USING FTIR AND GCMS
title_short CHARACTERIZATION OF MALAYSIAN JATROPHA SEED OIL USING FTIR AND GCMS
title_sort characterization of malaysian jatropha seed oil using ftir and gcms
topic jatropha seed oil
fatty acid
oleic acid
wax inhibitor
soxhlet extractor
url https://myjms.mohe.gov.my/index.php/paje/article/view/v5n4-3/8802
work_keys_str_mv AT mathanrajjayagobi characterizationofmalaysianjatrophaseedoilusingftirandgcms
AT amnihaslindaalpandi characterizationofmalaysianjatrophaseedoilusingftirandgcms
AT hazlinahusin characterizationofmalaysianjatrophaseedoilusingftirandgcms