Synthesis and Characterization of Functionalized SBA-15 Mesoporous Silica by N, N´-Bis(salicylidene)ethylenediamine Schiff-Base
In this work, BSEA-SBA-15 was prepared for the first time, which was prepared by covalently anchoring Schiff-base compound (N,N´-bis(salicylidene)ethylenediamine (BSEA) on SBA-15 by hydrothermal method. The structure and physicochemical properties were determined by elemental analysis, XRD, nitrogen...
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| Format: | Article |
| Language: | English |
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Nanoscience and Nanotechnology Research Center, University of Kashan
2013-12-01
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| Series: | Journal of Nanostructures |
| Subjects: | |
| Online Access: | http://jns.kashanu.ac.ir/article_5935_b1bcde28f64418f34a93b81a7a8eaaf0.pdf |
| _version_ | 1831729552675569664 |
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| author | A. Tadjarodi V. Jalalat R. Zare-Dorabei |
| author_facet | A. Tadjarodi V. Jalalat R. Zare-Dorabei |
| author_sort | A. Tadjarodi |
| collection | DOAJ |
| description | In this work, BSEA-SBA-15 was prepared for the first time, which was prepared by covalently anchoring Schiff-base compound (N,N´-bis(salicylidene)ethylenediamine (BSEA) on SBA-15 by hydrothermal method. The structure and physicochemical properties were determined by elemental analysis, XRD, nitrogen adsorption–desorption, thermogravimetric analysis and FTIR spectroscopy, SEM, BET surface area and BJH pore size. The average pore diameter after the modification is 69Å. It is expected that BSEA-SBA-15 can be used as an effective adsorbent for the removal of metal ions due to having porous structure and active functional groups. |
| first_indexed | 2024-12-21T07:13:41Z |
| format | Article |
| id | doaj.art-fe1947754c194afd8befe71f4aef48ca |
| institution | Directory Open Access Journal |
| issn | 2251-7871 2251-788X |
| language | English |
| last_indexed | 2024-12-21T07:13:41Z |
| publishDate | 2013-12-01 |
| publisher | Nanoscience and Nanotechnology Research Center, University of Kashan |
| record_format | Article |
| series | Journal of Nanostructures |
| spelling | doaj.art-fe1947754c194afd8befe71f4aef48ca2022-12-21T19:11:55ZengNanoscience and Nanotechnology Research Center, University of KashanJournal of Nanostructures2251-78712251-788X2013-12-013447748210.7508/jns.2013.04.0135935Synthesis and Characterization of Functionalized SBA-15 Mesoporous Silica by N, N´-Bis(salicylidene)ethylenediamine Schiff-BaseA. Tadjarodi0V. Jalalat1R. Zare-Dorabei2Department of Chemistry, Iran University of Science and Technology, Narmak, Tehran, 16846-13114, IranDepartment of Chemistry, Iran University of Science and Technology, Narmak, Tehran, 16846-13114, IranDepartment of Chemistry, Iran University of Science and Technology, Narmak, Tehran, 16846-13114, IranIn this work, BSEA-SBA-15 was prepared for the first time, which was prepared by covalently anchoring Schiff-base compound (N,N´-bis(salicylidene)ethylenediamine (BSEA) on SBA-15 by hydrothermal method. The structure and physicochemical properties were determined by elemental analysis, XRD, nitrogen adsorption–desorption, thermogravimetric analysis and FTIR spectroscopy, SEM, BET surface area and BJH pore size. The average pore diameter after the modification is 69Å. It is expected that BSEA-SBA-15 can be used as an effective adsorbent for the removal of metal ions due to having porous structure and active functional groups.http://jns.kashanu.ac.ir/article_5935_b1bcde28f64418f34a93b81a7a8eaaf0.pdfFunctional SBA-15Schiff-baseHydrothermalChemical synthesis |
| spellingShingle | A. Tadjarodi V. Jalalat R. Zare-Dorabei Synthesis and Characterization of Functionalized SBA-15 Mesoporous Silica by N, N´-Bis(salicylidene)ethylenediamine Schiff-Base Journal of Nanostructures Functional SBA-15 Schiff-base Hydrothermal Chemical synthesis |
| title | Synthesis and Characterization of Functionalized SBA-15 Mesoporous Silica by N, N´-Bis(salicylidene)ethylenediamine Schiff-Base |
| title_full | Synthesis and Characterization of Functionalized SBA-15 Mesoporous Silica by N, N´-Bis(salicylidene)ethylenediamine Schiff-Base |
| title_fullStr | Synthesis and Characterization of Functionalized SBA-15 Mesoporous Silica by N, N´-Bis(salicylidene)ethylenediamine Schiff-Base |
| title_full_unstemmed | Synthesis and Characterization of Functionalized SBA-15 Mesoporous Silica by N, N´-Bis(salicylidene)ethylenediamine Schiff-Base |
| title_short | Synthesis and Characterization of Functionalized SBA-15 Mesoporous Silica by N, N´-Bis(salicylidene)ethylenediamine Schiff-Base |
| title_sort | synthesis and characterization of functionalized sba 15 mesoporous silica by n n´ bis salicylidene ethylenediamine schiff base |
| topic | Functional SBA-15 Schiff-base Hydrothermal Chemical synthesis |
| url | http://jns.kashanu.ac.ir/article_5935_b1bcde28f64418f34a93b81a7a8eaaf0.pdf |
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