Solid Phase Microextraction for Measuring Agricultural Pesticides in Natural Samples

Introduction: Fungicides are a group of pesticides which are widely used and have negative effects on human health and the environment; Pesticide residues resulted from applying fungicides is a very important issue due to environmental pollution and human health risk and should be seriously consider...

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Main Authors: Torkan Mehrdiba, Marziyeh Piriyaei, Leila Kanaani
Format: Article
Language:English
Published: West Asia Organization for Cancer Prevention 2016-09-01
Series:Asian Pacific Journal of Cancer Biology
Subjects:
Online Access:http://www.waocp.com/journal/index.php/apjcb/article/view/201
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author Torkan Mehrdiba
Marziyeh Piriyaei
Leila Kanaani
author_facet Torkan Mehrdiba
Marziyeh Piriyaei
Leila Kanaani
author_sort Torkan Mehrdiba
collection DOAJ
description Introduction: Fungicides are a group of pesticides which are widely used and have negative effects on human health and the environment; Pesticide residues resulted from applying fungicides is a very important issue due to environmental pollution and human health risk and should be seriously considered. In order to achieve such insight summing up the dangers of pesticides is necessary so that attributes to predict social costs and benefits and monitor new policies applied. Methods: In this study, the possibility of extracting Triazole, a fungicide was evaluated by utilizing nanostructures, PW/SiO2, using new synthetic microextraction methods. Triazole is one of the most important pesticides with worldwide use for the protection of a variety of vegetables, fruits and grains and the destruction of many fungal pathogens because of its broad-spectrum and systemic properties. Results: In this study, a new synthetic microextraction is used in which the PW/SiO2 with nano-holes is applied for extraction and identification Triazole; the high specific surface area, selectivity, shape, and size are the main characteristics of these compounds leading to numerous catalytic applications, filtration, separation, and extraction of pesticides. Conclusion: The optimization conditions for this process include the extraction temperature: 80° C, extraction duration: 45 minutes, desorption temperature: 300° C, desorption duration: 2 minutes. Also, the correlation coefficient was high (0.998) and linear range was broad (0.01 to 200 ng/ml).
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spelling doaj.art-fe817c76506747cea022a3ba557d6d192024-01-29T05:41:26ZengWest Asia Organization for Cancer PreventionAsian Pacific Journal of Cancer Biology2538-46352016-09-0113677410.31557/apjcb.2016.1.3.67-74201Solid Phase Microextraction for Measuring Agricultural Pesticides in Natural SamplesTorkan Mehrdiba0Marziyeh Piriyaei1Leila KanaaniDepartment of Toxicology, Faculty of Pharmacy, Islamic Azad University, Ahar Branch, ahar, Iran.Department of Analytical Chemistry, Tabriz University, Tabriz, Iran.Introduction: Fungicides are a group of pesticides which are widely used and have negative effects on human health and the environment; Pesticide residues resulted from applying fungicides is a very important issue due to environmental pollution and human health risk and should be seriously considered. In order to achieve such insight summing up the dangers of pesticides is necessary so that attributes to predict social costs and benefits and monitor new policies applied. Methods: In this study, the possibility of extracting Triazole, a fungicide was evaluated by utilizing nanostructures, PW/SiO2, using new synthetic microextraction methods. Triazole is one of the most important pesticides with worldwide use for the protection of a variety of vegetables, fruits and grains and the destruction of many fungal pathogens because of its broad-spectrum and systemic properties. Results: In this study, a new synthetic microextraction is used in which the PW/SiO2 with nano-holes is applied for extraction and identification Triazole; the high specific surface area, selectivity, shape, and size are the main characteristics of these compounds leading to numerous catalytic applications, filtration, separation, and extraction of pesticides. Conclusion: The optimization conditions for this process include the extraction temperature: 80° C, extraction duration: 45 minutes, desorption temperature: 300° C, desorption duration: 2 minutes. Also, the correlation coefficient was high (0.998) and linear range was broad (0.01 to 200 ng/ml).http://www.waocp.com/journal/index.php/apjcb/article/view/201nanostructure- triazole pesticide- pw/sio2- microextraction
spellingShingle Torkan Mehrdiba
Marziyeh Piriyaei
Leila Kanaani
Solid Phase Microextraction for Measuring Agricultural Pesticides in Natural Samples
Asian Pacific Journal of Cancer Biology
nanostructure- triazole pesticide- pw/sio2- microextraction
title Solid Phase Microextraction for Measuring Agricultural Pesticides in Natural Samples
title_full Solid Phase Microextraction for Measuring Agricultural Pesticides in Natural Samples
title_fullStr Solid Phase Microextraction for Measuring Agricultural Pesticides in Natural Samples
title_full_unstemmed Solid Phase Microextraction for Measuring Agricultural Pesticides in Natural Samples
title_short Solid Phase Microextraction for Measuring Agricultural Pesticides in Natural Samples
title_sort solid phase microextraction for measuring agricultural pesticides in natural samples
topic nanostructure- triazole pesticide- pw/sio2- microextraction
url http://www.waocp.com/journal/index.php/apjcb/article/view/201
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AT marziyehpiriyaei solidphasemicroextractionformeasuringagriculturalpesticidesinnaturalsamples
AT leilakanaani solidphasemicroextractionformeasuringagriculturalpesticidesinnaturalsamples