Microstructure Characterization by Means of X-ray Micro-CT and Nanoindentation Measurements

The aim of this paper is to present an example of the material microstructure characterization with the use of X-ray micro-CT and nanoindentation measurements. Firstly, the current scope of application of the aforementioned techniques is provided within different fields of science. Then, background...

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Main Authors: Rajczakowska Magdalena, Stefaniuk Damian, Łydżba Dariusz
Format: Article
Language:English
Published: Sciendo 2015-03-01
Series:Studia Geotechnica et Mechanica
Subjects:
Online Access:http://www.degruyter.com/view/j/sgem.2015.37.issue-1/sgem-2015-0009/sgem-2015-0009.xml?format=INT
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author Rajczakowska Magdalena
Stefaniuk Damian
Łydżba Dariusz
author_facet Rajczakowska Magdalena
Stefaniuk Damian
Łydżba Dariusz
author_sort Rajczakowska Magdalena
collection DOAJ
description The aim of this paper is to present an example of the material microstructure characterization with the use of X-ray micro-CT and nanoindentation measurements. Firstly, the current scope of application of the aforementioned techniques is provided within different fields of science. Then, background of each of the methods is presented. The methodology of X-ray micro-CT is described with the emphasis on the Beer’s law formulation. In addition, the basics of the nanoindentation technique are outlined and major formulas for the hardness and Young’s modulus calculation are given. Finally, example results for a concrete sample are presented. The microstructure of the selected material is firstly characterized in terms of geometry using the results from the microtomograhy measurements, e.g., porosity and attenuation profiles, pore and aggregate size distribution, shape factor of pores, etc. Next, the results of the nanoindentation tests are provided, namely the hardness and Young’s modulus versus the height of the sample. The influence of the number of tests and statistical analysis on the final results is underlined.
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spelling doaj.art-fef9a26a00d540c8a674cd064efc07a92022-12-22T02:57:15ZengSciendoStudia Geotechnica et Mechanica0137-63652083-831X2015-03-01371758410.1515/sgem-2015-0009sgem-2015-0009Microstructure Characterization by Means of X-ray Micro-CT and Nanoindentation MeasurementsRajczakowska Magdalena0Stefaniuk Damian1Łydżba Dariusz2Wrocław University of Technology, Faculty of Civil Engineering, Institute of Geotechnics and Hydrotechnics, Wybrzeże Wyspiańskiego 27, 50-370 Wrocław, PolandWrocław University of Technology, Faculty of Civil Engineering, Institute of Geotechnics and Hydrotechnics, Wybrzeże Wyspiańskiego 27, 50-370 Wrocław, PolandWrocław University of Technology, Faculty of Civil Engineering, Institute of Geotechnics and Hydrotechnics, Wybrzeże Wyspiańskiego 27, 50-370 Wrocław, PolandThe aim of this paper is to present an example of the material microstructure characterization with the use of X-ray micro-CT and nanoindentation measurements. Firstly, the current scope of application of the aforementioned techniques is provided within different fields of science. Then, background of each of the methods is presented. The methodology of X-ray micro-CT is described with the emphasis on the Beer’s law formulation. In addition, the basics of the nanoindentation technique are outlined and major formulas for the hardness and Young’s modulus calculation are given. Finally, example results for a concrete sample are presented. The microstructure of the selected material is firstly characterized in terms of geometry using the results from the microtomograhy measurements, e.g., porosity and attenuation profiles, pore and aggregate size distribution, shape factor of pores, etc. Next, the results of the nanoindentation tests are provided, namely the hardness and Young’s modulus versus the height of the sample. The influence of the number of tests and statistical analysis on the final results is underlined.http://www.degruyter.com/view/j/sgem.2015.37.issue-1/sgem-2015-0009/sgem-2015-0009.xml?format=INTmicro-CTnanoindentationmicrostructurecomposite
spellingShingle Rajczakowska Magdalena
Stefaniuk Damian
Łydżba Dariusz
Microstructure Characterization by Means of X-ray Micro-CT and Nanoindentation Measurements
Studia Geotechnica et Mechanica
micro-CT
nanoindentation
microstructure
composite
title Microstructure Characterization by Means of X-ray Micro-CT and Nanoindentation Measurements
title_full Microstructure Characterization by Means of X-ray Micro-CT and Nanoindentation Measurements
title_fullStr Microstructure Characterization by Means of X-ray Micro-CT and Nanoindentation Measurements
title_full_unstemmed Microstructure Characterization by Means of X-ray Micro-CT and Nanoindentation Measurements
title_short Microstructure Characterization by Means of X-ray Micro-CT and Nanoindentation Measurements
title_sort microstructure characterization by means of x ray micro ct and nanoindentation measurements
topic micro-CT
nanoindentation
microstructure
composite
url http://www.degruyter.com/view/j/sgem.2015.37.issue-1/sgem-2015-0009/sgem-2015-0009.xml?format=INT
work_keys_str_mv AT rajczakowskamagdalena microstructurecharacterizationbymeansofxraymicroctandnanoindentationmeasurements
AT stefaniukdamian microstructurecharacterizationbymeansofxraymicroctandnanoindentationmeasurements
AT łydzbadariusz microstructurecharacterizationbymeansofxraymicroctandnanoindentationmeasurements