Atomic-Resolution Imaging of Micron-Sized Samples Realized by High Magnetic Field Scanning Tunneling Microscopy

Scanning tunneling microscopy (STM) can image material surfaces with atomic resolution, making it a useful tool in the areas of physics and materials. Many materials are synthesized at micron size, especially few-layer materials. Limited by their complex structure, very few STMs are capable of direc...

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Main Authors: Weixuan Li, Jihao Wang, Jing Zhang, Wenjie Meng, Caihong Xie, Yubin Hou, Zhigang Xia, Qingyou Lu
Format: Article
Language:English
Published: MDPI AG 2023-01-01
Series:Micromachines
Subjects:
Online Access:https://www.mdpi.com/2072-666X/14/2/287
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author Weixuan Li
Jihao Wang
Jing Zhang
Wenjie Meng
Caihong Xie
Yubin Hou
Zhigang Xia
Qingyou Lu
author_facet Weixuan Li
Jihao Wang
Jing Zhang
Wenjie Meng
Caihong Xie
Yubin Hou
Zhigang Xia
Qingyou Lu
author_sort Weixuan Li
collection DOAJ
description Scanning tunneling microscopy (STM) can image material surfaces with atomic resolution, making it a useful tool in the areas of physics and materials. Many materials are synthesized at micron size, especially few-layer materials. Limited by their complex structure, very few STMs are capable of directly positioning and imaging a micron-sized sample with atomic resolution. Traditional STMs are designed to study the material behavior induced by temperature variation, while the physical properties induced by magnetic fields are rarely studied. In this paper, we present the design and construction of an atomic-resolution STM that can operate in a 9 T high magnetic field. More importantly, the homebuilt STM is capable of imaging micron-sized samples. The performance of the STM is demonstrated by high-quality atomic images obtained on a graphite surface, with low drift rates in the X–Y plane and Z direction. The atomic-resolution image obtained on a 32-μm graphite flake illustrates the new STM’s ability of positioning and imaging micron-sized samples. Finally, we present atomic resolution images at a magnetic field range from 0 T to 9 T. The above advantages make our STM a promising tool for investigating the quantum hall effect of micron-sized layered materials.
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spelling doaj.art-ff90595dcd464b26ad6b1fc65f2a2b7c2023-11-16T22:10:06ZengMDPI AGMicromachines2072-666X2023-01-0114228710.3390/mi14020287Atomic-Resolution Imaging of Micron-Sized Samples Realized by High Magnetic Field Scanning Tunneling MicroscopyWeixuan Li0Jihao Wang1Jing Zhang2Wenjie Meng3Caihong Xie4Yubin Hou5Zhigang Xia6Qingyou Lu7College of Metrology and Measurement Engineering, China Jiliang University (CJLU), Hangzhou 310018, ChinaAnhui Province Key Laboratory of Condensed Matter Physics at Extreme Conditions, High Magnetic Field Laboratory, Hefei Institutes of Physical Science, Chinese Academy of Sciences, Hefei 230031, ChinaAnhui Province Key Laboratory of Condensed Matter Physics at Extreme Conditions, High Magnetic Field Laboratory, Hefei Institutes of Physical Science, Chinese Academy of Sciences, Hefei 230031, ChinaAnhui Province Key Laboratory of Condensed Matter Physics at Extreme Conditions, High Magnetic Field Laboratory, Hefei Institutes of Physical Science, Chinese Academy of Sciences, Hefei 230031, ChinaAnhui Province Key Laboratory of Condensed Matter Physics at Extreme Conditions, High Magnetic Field Laboratory, Hefei Institutes of Physical Science, Chinese Academy of Sciences, Hefei 230031, ChinaAnhui Province Key Laboratory of Condensed Matter Physics at Extreme Conditions, High Magnetic Field Laboratory, Hefei Institutes of Physical Science, Chinese Academy of Sciences, Hefei 230031, ChinaCollege of Metrology and Measurement Engineering, China Jiliang University (CJLU), Hangzhou 310018, ChinaAnhui Province Key Laboratory of Condensed Matter Physics at Extreme Conditions, High Magnetic Field Laboratory, Hefei Institutes of Physical Science, Chinese Academy of Sciences, Hefei 230031, ChinaScanning tunneling microscopy (STM) can image material surfaces with atomic resolution, making it a useful tool in the areas of physics and materials. Many materials are synthesized at micron size, especially few-layer materials. Limited by their complex structure, very few STMs are capable of directly positioning and imaging a micron-sized sample with atomic resolution. Traditional STMs are designed to study the material behavior induced by temperature variation, while the physical properties induced by magnetic fields are rarely studied. In this paper, we present the design and construction of an atomic-resolution STM that can operate in a 9 T high magnetic field. More importantly, the homebuilt STM is capable of imaging micron-sized samples. The performance of the STM is demonstrated by high-quality atomic images obtained on a graphite surface, with low drift rates in the X–Y plane and Z direction. The atomic-resolution image obtained on a 32-μm graphite flake illustrates the new STM’s ability of positioning and imaging micron-sized samples. Finally, we present atomic resolution images at a magnetic field range from 0 T to 9 T. The above advantages make our STM a promising tool for investigating the quantum hall effect of micron-sized layered materials.https://www.mdpi.com/2072-666X/14/2/287Scanning tunneling microscopyhigh magnetic fieldmicron-sized sample
spellingShingle Weixuan Li
Jihao Wang
Jing Zhang
Wenjie Meng
Caihong Xie
Yubin Hou
Zhigang Xia
Qingyou Lu
Atomic-Resolution Imaging of Micron-Sized Samples Realized by High Magnetic Field Scanning Tunneling Microscopy
Micromachines
Scanning tunneling microscopy
high magnetic field
micron-sized sample
title Atomic-Resolution Imaging of Micron-Sized Samples Realized by High Magnetic Field Scanning Tunneling Microscopy
title_full Atomic-Resolution Imaging of Micron-Sized Samples Realized by High Magnetic Field Scanning Tunneling Microscopy
title_fullStr Atomic-Resolution Imaging of Micron-Sized Samples Realized by High Magnetic Field Scanning Tunneling Microscopy
title_full_unstemmed Atomic-Resolution Imaging of Micron-Sized Samples Realized by High Magnetic Field Scanning Tunneling Microscopy
title_short Atomic-Resolution Imaging of Micron-Sized Samples Realized by High Magnetic Field Scanning Tunneling Microscopy
title_sort atomic resolution imaging of micron sized samples realized by high magnetic field scanning tunneling microscopy
topic Scanning tunneling microscopy
high magnetic field
micron-sized sample
url https://www.mdpi.com/2072-666X/14/2/287
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