Overhauser effects in insulating solids

Overhauser effects in insulating solids

We report magic angle spinning, dynamic nuclear polarization (DNP) experiments at magnetic fields of 9.4 T, 14.1 T, and 18.8 T using the narrow line polarizing agents 1,3-bisdiphenylene-2-phenylallyl (BDPA) dispersed in polystyrene, and sulfonated-BDPA (SA-BDPA) and trityl OX063 in glassy glycerol/w...

Full description

Bibliographic Details
Main Authors:	Caporini, M. A., Mentink-Vigier, F., Rosay, M., Maas, W. E., Baldus, M., Vega, S., Corzilius, Bjorn, Walish, Joseph John, Swager, Timothy M, Griffin, Robert Guy, Can, Thach V
Other Authors:	Massachusetts Institute of Technology. Department of Chemistry
Format:	Article
Language:	en_US
Published:	American Institute of Physics (AIP) 2017
Online Access:	http://hdl.handle.net/1721.1/109520 https://orcid.org/0000-0001-9092-612X https://orcid.org/0000-0003-1589-832X

Similar Items

Overhauser effects in non-conducting solids at 1.2 K
by: Ji, X., et al.
Published: (2020)

New methods for dynamic nuclear polarization in insulating solids : the Overhauser effect and time domain techniques
by: Can, Thach V. (Thach Van)
Published: (2017)

Frequency-Swept Integrated Solid Effect
by: Walish, Joseph J., et al.
Published: (2018)

Time domain DNP with the NOVEL sequence
by: Can, Thach V, et al.
Published: (2022)

Time domain DNP with the NOVEL sequence
by: Can, Thach V, et al.
Published: (2017)

Mechanisms of dynamic nuclear polarization in insulating solids
by: Ni, Qing Zhe, et al.
Published: (2017)

Overhauser Dynamic Nuclear Polarization with Selectively Deuterated BDPA Radicals
by: Delage-Laurin, Leo, et al.
Published: (2022)

Ramped-amplitude NOVEL
by: Weber, R. T., et al.
Published: (2018)

Overhauser Dynamic Nuclear Polarization with Selectively Deuterated BDPA Radicals
by: Delage-Laurin, Léo, et al.
Published: (2022)

Observation of strongly forbidden solid effect dynamic nuclear polarization transitions via electron-electron double resonance detected NMR
by: Smith, Albert A., et al.
Published: (2015)

Solid effect in magic angle spinning dynamic nuclear polarization
by: Smith, Albert A., et al.
Published: (2013)

Dynamic Nuclear Polarization Study of Inhibitor Binding to the M2[subscript 18–60] Proton Transporter from Influenza A
by: Andreas, Loren, et al.
Published: (2015)

Water-Soluble Narrow-Line Radicals for Dynamic Nuclear Polarization
by: Haze, Olesya, et al.
Published: (2013)

Dynamic Nuclear Polarization with a Water-Soluble Rigid Biradical
by: Kiesewetter, Matthew K., et al.
Published: (2013)

Solid effect dynamic nuclear polarization and polarization pathways
by: Corzilius, Bjorn, et al.
Published: (2012)

Dynamic Nuclear Polarization-Enhanced Solid-State NMR Spectroscopy of GNNQQNY Nanocrystals and Amyloid Fibrils
by: Debelouchina, Galia Tzvetanova, et al.
Published: (2012)

High-Field [superscript 13] C Dynamic Nuclear Polarization with a Radical Mixture
by: Michaelis, Vladimir K., et al.
Published: (2015)

Gd(iii) and Mn(ii) Complexes for Dynamic Nuclear Polarization: Small Molecular Chelate Polarizing Agents and Applications with Site-Directed Spin Labeling of Proteins
by: Kaushik, Monu, et al.
Published: (2018)

High Field Dynamic Nuclear Polarization NMR with Surfactant Sheltered Biradicals
by: Kiesewetter, Matthew K., et al.
Published: (2015)

Solvent-Free Dynamic Nuclear Polarization of Amorphous and Crystalline ortho-Terphenyl
by: Ong, Ta-Chung, et al.
Published: (2015)

Efficient cross-effect dynamic nuclear polarization without depolarization in high-resolution MAS NMR
by: Mentink-Vigier, Frédéric, et al.
Published: (2018)

Adiabatic Solid Effect
by: Tan, Kong Ooi, et al.
Published: (2022)

Adiabatic Solid Effect
by: Tan, Kong Ooi, et al.
Published: (2022)

TIME DEVELOPMENT OF PROTON NUCLEAR OVERHAUSER EFFECTS IN PROTEINS
by: Dobson, C, et al.
Published: (1982)

Measurement of temporal correlations of the overhauser field in a double quantum dot.
by: Reilly, D, et al.
Published: (2008)

Peptide and Protein Dynamics and Low-Temperature/DNP Magic Angle Spinning NMR
by: Daviso, Eugenio, et al.
Published: (2018)

Dynamic Nuclear Polarization of [superscript 17] O: Direct Polarization
by: Michaelis, Vladimir K., et al.
Published: (2015)

Chemically amplified 19F-1H nuclear Overhauser effects.
by: Kuprov, I, et al.
Published: (2004)

Fully-drawn carbon-based chemical sensors on organic and inorganic surfaces
by: Swager, Timothy M., et al.
Published: (2016)

Rigid Orthogonal Bis-TEMPO Biradicals with Improved Solubility for Dynamic Nuclear Polarization
by: Dane, Eric L., et al.
Published: (2013)

Conformation of bis-nitroxide polarizing agents by multi-frequency EPR spectroscopy
by: Gast, Peter, et al.
Published: (2018)

Solid-State Dynamic Nuclear Polarization at 263 GHz: Spectrometer Design and Experimental Results
by: Rosay, Melanie, et al.
Published: (2012)

Paramagnet induced signal quenching in MAS–DNP experiments in frozen homogeneous solutions
by: Corzilius, Bjorn, et al.
Published: (2017)

Equilibration of Tyrosyl Radicals (Y[• over 356], Y[• over 731], Y[• over 730]) in the Radical Propagation Pathway of the Escherichia coli Class Ia Ribonucleotide Reductase
by: Yokoyama, Kenichi, et al.
Published: (2013)

Synthesis and Properties of the 5,10,15-Trimesityltruxen-5-yl Radical
by: Frantz, Derik K., et al.
Published: (2014)

High frequency dynamic nuclear polarization: New directions for the 21st century
by: Griffin, Robert Guy, et al.
Published: (2021)

High Field Dynamic Nuclear Polarization with High-Spin Transition Metal Ions
by: Barnes, Alexander, et al.
Published: (2012)

DNP-Enhanced MAS NMR of Bovine Serum Albumin Sediments and Solutions
by: Ravera, Enrico, et al.
Published: (2015)

High Frequency Dynamic Nuclear Polarization
by: Ni, Qing Zhe, et al.
Published: (2015)

Atomic Resolution Structure of Monomorphic Aβ₄₂ Amyloid Fibrils
by: Sergeyev, Ivan, et al.
Published: (2018)