Correcting for contact area changes in nanoindentation using surface acoustic waves

Nanoindentation is extensively used to quantify nano-scale mechanical behaviour. A widely-used assumption is that a well-defined, material-independent relationship exists between the indentation depth and indenter contact area. Here we demonstrate that this assumption is violated by ion-implanted tu...

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Main Authors: Beck, Christian E., Hofmann, Felix, Armstrong, David E.J., Eliason, Jeffrey Kristian, Maznev, Alexei, Nelson, Keith Adam
Other Authors: Massachusetts Institute of Technology. Department of Chemistry
Format: Article
Published: Elsevier 2018
Online Access:http://hdl.handle.net/1721.1/113389
https://orcid.org/0000-0001-7804-5418
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author Beck, Christian E.
Hofmann, Felix
Armstrong, David E.J.
Eliason, Jeffrey Kristian
Maznev, Alexei
Nelson, Keith Adam
author2 Massachusetts Institute of Technology. Department of Chemistry
author_facet Massachusetts Institute of Technology. Department of Chemistry
Beck, Christian E.
Hofmann, Felix
Armstrong, David E.J.
Eliason, Jeffrey Kristian
Maznev, Alexei
Nelson, Keith Adam
author_sort Beck, Christian E.
collection MIT
description Nanoindentation is extensively used to quantify nano-scale mechanical behaviour. A widely-used assumption is that a well-defined, material-independent relationship exists between the indentation depth and indenter contact area. Here we demonstrate that this assumption is violated by ion-implanted tungsten, where pileup around the indenter tip leads to substantial changes in contact area. Using high accuracy surface acoustic wave measurements of elastic modulus, we are able to correct for this effect. Importantly we demonstrate that a priori knowledge of elastic properties can be readily used to compensate for pileup effects in nanoindentation without the need for any further measurements. Keywords: nanoindentation; pile-up; ion implantation; irradiation; surface acoustic waves
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spelling mit-1721.1/1133892022-10-01T18:51:30Z Correcting for contact area changes in nanoindentation using surface acoustic waves Beck, Christian E. Hofmann, Felix Armstrong, David E.J. Eliason, Jeffrey Kristian Maznev, Alexei Nelson, Keith Adam Massachusetts Institute of Technology. Department of Chemistry Eliason, Jeffrey Kristian Maznev, Alexei Nelson, Keith Adam Nanoindentation is extensively used to quantify nano-scale mechanical behaviour. A widely-used assumption is that a well-defined, material-independent relationship exists between the indentation depth and indenter contact area. Here we demonstrate that this assumption is violated by ion-implanted tungsten, where pileup around the indenter tip leads to substantial changes in contact area. Using high accuracy surface acoustic wave measurements of elastic modulus, we are able to correct for this effect. Importantly we demonstrate that a priori knowledge of elastic properties can be readily used to compensate for pileup effects in nanoindentation without the need for any further measurements. Keywords: nanoindentation; pile-up; ion implantation; irradiation; surface acoustic waves National Science Foundation (U.S.) (Grant CHE-1111557) 2018-02-02T14:18:44Z 2018-02-02T14:18:44Z 2016-10 2016-09 2018-01-31T15:09:01Z Article http://purl.org/eprint/type/JournalArticle 1359-6462 http://hdl.handle.net/1721.1/113389 Beck, Christian E. et al. “Correcting for Contact Area Changes in Nanoindentation Using Surface Acoustic Waves.” Scripta Materialia 128 (February 2017): 83–86 © 2016 Acta Materialia Inc https://orcid.org/0000-0001-7804-5418 http://dx.doi.org/10.1016/J.SCRIPTAMAT.2016.09.037 Scripta Materialia Creative Commons Attribution 4.0 International License http://creativecommons.org/licenses/by/4.0/ application/pdf Elsevier Elsevier
spellingShingle Beck, Christian E.
Hofmann, Felix
Armstrong, David E.J.
Eliason, Jeffrey Kristian
Maznev, Alexei
Nelson, Keith Adam
Correcting for contact area changes in nanoindentation using surface acoustic waves
title Correcting for contact area changes in nanoindentation using surface acoustic waves
title_full Correcting for contact area changes in nanoindentation using surface acoustic waves
title_fullStr Correcting for contact area changes in nanoindentation using surface acoustic waves
title_full_unstemmed Correcting for contact area changes in nanoindentation using surface acoustic waves
title_short Correcting for contact area changes in nanoindentation using surface acoustic waves
title_sort correcting for contact area changes in nanoindentation using surface acoustic waves
url http://hdl.handle.net/1721.1/113389
https://orcid.org/0000-0001-7804-5418
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