Multi-scale investigations of the Resistance to helium embrittlement with Direct Energy Deposited Inconel 718

Thesis: S.B., Massachusetts Institute of Technology, Department of Nuclear Science and Engineering, February, 2021

Bibliographic Details
Main Author: Stapelberg, Myles Graham.
Other Authors: Michael P. Short and Ju Li.
Format: Thesis
Language:eng
Published: Massachusetts Institute of Technology 2021
Subjects:
Online Access:https://hdl.handle.net/1721.1/131002
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author Stapelberg, Myles Graham.
author2 Michael P. Short and Ju Li.
author_facet Michael P. Short and Ju Li.
Stapelberg, Myles Graham.
author_sort Stapelberg, Myles Graham.
collection MIT
description Thesis: S.B., Massachusetts Institute of Technology, Department of Nuclear Science and Engineering, February, 2021
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spelling mit-1721.1/1310022021-06-18T03:11:23Z Multi-scale investigations of the Resistance to helium embrittlement with Direct Energy Deposited Inconel 718 Stapelberg, Myles Graham. Michael P. Short and Ju Li. Massachusetts Institute of Technology. Department of Nuclear Science and Engineering. Massachusetts Institute of Technology. Department of Nuclear Science and Engineering Nuclear Science and Engineering. Thesis: S.B., Massachusetts Institute of Technology, Department of Nuclear Science and Engineering, February, 2021 Cataloged from the official PDF of thesis. Includes bibliographical references (pages 101-114). To address the high levels of helium production in advanced fission and fusion reactors, in an economical manner, Direct Energy Deposition (DED) was utilized with the existing alloy, Inconel 718. Based on previous works with DED and laser welding, it was hypothesized that nano-sized pores could be engineered within the matrix of the sample to maximize the number of available sinks for helium bubbles to migrate towards, instead of migrating towards grain boundaries. A sparse experimental matrix with 316L Stainless Steel, followed up with 2-Factor, 3 Level full factorial experiments with Inconel 718 was conducted to understand the input parameters for engineering nanoporosity. In-situ ion irradiation TEM was conducted to analyze the helium bubble kinetics in real time at the nanoscale and ex-situ ion irradiation followed by Vicker's microhardness tests, X-ray Diffraction, Energy Dispersion Spectroscopy, and Focused Ion Beam Analysis were conducted to gauge the effectiveness of the printed sample at inhibiting helium migration and embrittlement. Due to insufficient measurements and the sensitivity of Inconel 718's microstructure to temperature, no significant change between the control and helium implanted specimens were observed at the micro scale. However, at the nanoscale, nanopores were found and were able to suppress the nucleation of helium bubbles. As such, a followup study, investigating nuisance factors discussed in this work is warranted to better assert whether or not DED can effectively reduce the effects of helium embrittlement. by Myles Graham Stapelberg. S.B. S.B. Massachusetts Institute of Technology, Department of Nuclear Science and Engineering 2021-06-17T17:21:07Z 2021-06-17T17:21:07Z 2021 2021 Thesis https://hdl.handle.net/1721.1/131002 1256665509 eng MIT theses may be protected by copyright. Please reuse MIT thesis content according to the MIT Libraries Permissions Policy, which is available through the URL provided. http://dspace.mit.edu/handle/1721.1/7582 114 pages application/pdf Massachusetts Institute of Technology
spellingShingle Nuclear Science and Engineering.
Stapelberg, Myles Graham.
Multi-scale investigations of the Resistance to helium embrittlement with Direct Energy Deposited Inconel 718
title Multi-scale investigations of the Resistance to helium embrittlement with Direct Energy Deposited Inconel 718
title_full Multi-scale investigations of the Resistance to helium embrittlement with Direct Energy Deposited Inconel 718
title_fullStr Multi-scale investigations of the Resistance to helium embrittlement with Direct Energy Deposited Inconel 718
title_full_unstemmed Multi-scale investigations of the Resistance to helium embrittlement with Direct Energy Deposited Inconel 718
title_short Multi-scale investigations of the Resistance to helium embrittlement with Direct Energy Deposited Inconel 718
title_sort multi scale investigations of the resistance to helium embrittlement with direct energy deposited inconel 718
topic Nuclear Science and Engineering.
url https://hdl.handle.net/1721.1/131002
work_keys_str_mv AT stapelbergmylesgraham multiscaleinvestigationsoftheresistancetoheliumembrittlementwithdirectenergydepositedinconel718