Thermal and electrical characterization of a micro-hotplate for calorimetry

Thesis (M. Eng.)--Massachusetts Institute of Technology, Dept. of Electrical Engineering and Computer Science, 2004.

Bibliographic Details
Main Author: Baliga, Radhika
Other Authors: Amy E. Duwel and Joel Voldman.
Format: Thesis
Language:eng
Published: Massachusetts Institute of Technology 2006
Subjects:
Online Access:http://hdl.handle.net/1721.1/33101
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author Baliga, Radhika
author2 Amy E. Duwel and Joel Voldman.
author_facet Amy E. Duwel and Joel Voldman.
Baliga, Radhika
author_sort Baliga, Radhika
collection MIT
description Thesis (M. Eng.)--Massachusetts Institute of Technology, Dept. of Electrical Engineering and Computer Science, 2004.
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spelling mit-1721.1/331012022-01-13T07:54:29Z Thermal and electrical characterization of a micro-hotplate for calorimetry Baliga, Radhika Amy E. Duwel and Joel Voldman. Massachusetts Institute of Technology. Dept. of Electrical Engineering and Computer Science. Massachusetts Institute of Technology. Department of Electrical Engineering and Computer Science Electrical Engineering and Computer Science. Thesis (M. Eng.)--Massachusetts Institute of Technology, Dept. of Electrical Engineering and Computer Science, 2004. Includes bibliographical references (p. 104-105). This thesis characterizes a micro-hotplate designed at Draper Laboratory. This hotplate will be integrated into a calorimetry system that measures the heat released or absorbed by a reaction. An analytical thermal model is developed to quantify the heat transfer mechanisms between the hotplate and the environment. The analytical model is verified through experimental measurements conducted with the device operating in both ambient conditions and vacuum. In ambient conditions, the heat transfer is dominated by air conduction as predicted by the model. Air conduction can be reduced by operating the device in a medium with a lower thermal conductivity. The relatively short timescale over which the hotplate comes to thermal equilibrium with the environment limits the types of reactions that can be measured with the device. The performance of the hotplate can be improved by operating it in vacuum, by constructing it from a material with a lower emissivity, or by decreasing its surface area. The noise spectral density of the hotplate's resistive temperature sensor is characterized. The hotplate's ability to resolve temperature is limited by the flicker noise in the sensor. by Radhika Baliga. M.Eng. 2006-06-19T17:40:24Z 2006-06-19T17:40:24Z 2004 2004 Thesis http://hdl.handle.net/1721.1/33101 62221331 eng M.I.T. theses are protected by copyright. They may be viewed from this source for any purpose, but reproduction or distribution in any format is prohibited without written permission. See provided URL for inquiries about permission. http://dspace.mit.edu/handle/1721.1/7582 105 p. 4495374 bytes 4501109 bytes application/pdf application/pdf application/pdf Massachusetts Institute of Technology
spellingShingle Electrical Engineering and Computer Science.
Baliga, Radhika
Thermal and electrical characterization of a micro-hotplate for calorimetry
title Thermal and electrical characterization of a micro-hotplate for calorimetry
title_full Thermal and electrical characterization of a micro-hotplate for calorimetry
title_fullStr Thermal and electrical characterization of a micro-hotplate for calorimetry
title_full_unstemmed Thermal and electrical characterization of a micro-hotplate for calorimetry
title_short Thermal and electrical characterization of a micro-hotplate for calorimetry
title_sort thermal and electrical characterization of a micro hotplate for calorimetry
topic Electrical Engineering and Computer Science.
url http://hdl.handle.net/1721.1/33101
work_keys_str_mv AT baligaradhika thermalandelectricalcharacterizationofamicrohotplateforcalorimetry