Formation of delta ferrite in 9 wt.% Cr steel investigated by in-situ X-ray diffraction using synchrotron radiation

In-situ X-ray diffraction (XRD) measurements using high energy synchrotron radiation were performed to monitor in real time the formation of delta ferrite in a martensitic 9 wt pct chromium steel under simulated weld thermal cycles. Volume fractions of martensite, austenite, and delta ferrite were m...

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Main Authors: Mayr, Peter, Palmer, T. A., Elmer, J. W., Specht, E. D., Allen, Samuel Miller
Other Authors: Massachusetts Institute of Technology. Department of Materials Science and Engineering
Format: Article
Language:en_US
Published: Springer-Boston 2012
Online Access:http://hdl.handle.net/1721.1/70852
https://orcid.org/0000-0002-6082-332X
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author Mayr, Peter
Palmer, T. A.
Elmer, J. W.
Specht, E. D.
Allen, Samuel Miller
author2 Massachusetts Institute of Technology. Department of Materials Science and Engineering
author_facet Massachusetts Institute of Technology. Department of Materials Science and Engineering
Mayr, Peter
Palmer, T. A.
Elmer, J. W.
Specht, E. D.
Allen, Samuel Miller
author_sort Mayr, Peter
collection MIT
description In-situ X-ray diffraction (XRD) measurements using high energy synchrotron radiation were performed to monitor in real time the formation of delta ferrite in a martensitic 9 wt pct chromium steel under simulated weld thermal cycles. Volume fractions of martensite, austenite, and delta ferrite were measured as a function of temperature at a 10 K/s heating rate to 1573 K (1300 °C) and subsequent cooling. At the peak temperature, the delta ferrite concentration rose to 19 pct, of which 17 pct transformed back to austenite on subsequent cooling.
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spelling mit-1721.1/708522022-09-29T17:14:19Z Formation of delta ferrite in 9 wt.% Cr steel investigated by in-situ X-ray diffraction using synchrotron radiation Mayr, Peter Palmer, T. A. Elmer, J. W. Specht, E. D. Allen, Samuel Miller Massachusetts Institute of Technology. Department of Materials Science and Engineering Allen, Samuel Miller Allen, Samuel Miller Mayr, Peter In-situ X-ray diffraction (XRD) measurements using high energy synchrotron radiation were performed to monitor in real time the formation of delta ferrite in a martensitic 9 wt pct chromium steel under simulated weld thermal cycles. Volume fractions of martensite, austenite, and delta ferrite were measured as a function of temperature at a 10 K/s heating rate to 1573 K (1300 °C) and subsequent cooling. At the peak temperature, the delta ferrite concentration rose to 19 pct, of which 17 pct transformed back to austenite on subsequent cooling. Max Kade Foundation, Inc. Austrian Academy of Sciences United States. Dept. of Energy (Division of Materials Sciences and Engineering, Office of Science, and Office of Basic Energy Sciences) 2012-05-16T20:28:02Z 2012-05-16T20:28:02Z 2010-10 Article http://purl.org/eprint/type/JournalArticle 1073-5623 1543-1940 http://hdl.handle.net/1721.1/70852 Mayr, P. et al. “Formation of Delta Ferrite in 9 Wt Pct Cr Steel Investigated by In-Situ X-Ray Diffraction Using Synchrotron Radiation.” Metallurgical and Materials Transactions A 41.10 (2010): 2462–2465. Web. https://orcid.org/0000-0002-6082-332X en_US http://dx.doi.org/10.1007/s11661-010-0371-7 Metallurgical and Materials Transactions A Creative Commons Attribution-Noncommercial-Share Alike 3.0 http://creativecommons.org/licenses/by-nc-sa/3.0/ application/pdf Springer-Boston Prof. Allen via Angie Locknar
spellingShingle Mayr, Peter
Palmer, T. A.
Elmer, J. W.
Specht, E. D.
Allen, Samuel Miller
Formation of delta ferrite in 9 wt.% Cr steel investigated by in-situ X-ray diffraction using synchrotron radiation
title Formation of delta ferrite in 9 wt.% Cr steel investigated by in-situ X-ray diffraction using synchrotron radiation
title_full Formation of delta ferrite in 9 wt.% Cr steel investigated by in-situ X-ray diffraction using synchrotron radiation
title_fullStr Formation of delta ferrite in 9 wt.% Cr steel investigated by in-situ X-ray diffraction using synchrotron radiation
title_full_unstemmed Formation of delta ferrite in 9 wt.% Cr steel investigated by in-situ X-ray diffraction using synchrotron radiation
title_short Formation of delta ferrite in 9 wt.% Cr steel investigated by in-situ X-ray diffraction using synchrotron radiation
title_sort formation of delta ferrite in 9 wt cr steel investigated by in situ x ray diffraction using synchrotron radiation
url http://hdl.handle.net/1721.1/70852
https://orcid.org/0000-0002-6082-332X
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