Formation of delta ferrite in 9 wt.% Cr steel investigated by in-situ X-ray diffraction using synchrotron radiation
In-situ X-ray diffraction (XRD) measurements using high energy synchrotron radiation were performed to monitor in real time the formation of delta ferrite in a martensitic 9 wt pct chromium steel under simulated weld thermal cycles. Volume fractions of martensite, austenite, and delta ferrite were m...
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Springer-Boston
2012
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Online Access: | http://hdl.handle.net/1721.1/70852 https://orcid.org/0000-0002-6082-332X |
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author | Mayr, Peter Palmer, T. A. Elmer, J. W. Specht, E. D. Allen, Samuel Miller |
author2 | Massachusetts Institute of Technology. Department of Materials Science and Engineering |
author_facet | Massachusetts Institute of Technology. Department of Materials Science and Engineering Mayr, Peter Palmer, T. A. Elmer, J. W. Specht, E. D. Allen, Samuel Miller |
author_sort | Mayr, Peter |
collection | MIT |
description | In-situ X-ray diffraction (XRD) measurements using high energy synchrotron radiation were performed to monitor in real time the formation of delta ferrite in a martensitic 9 wt pct chromium steel under simulated weld thermal cycles. Volume fractions of martensite, austenite, and delta ferrite were measured as a function of temperature at a 10 K/s heating rate to 1573 K (1300 °C) and subsequent cooling. At the peak temperature, the delta ferrite concentration rose to 19 pct, of which 17 pct transformed back to austenite on subsequent cooling. |
first_indexed | 2024-09-23T15:56:50Z |
format | Article |
id | mit-1721.1/70852 |
institution | Massachusetts Institute of Technology |
language | en_US |
last_indexed | 2024-09-23T15:56:50Z |
publishDate | 2012 |
publisher | Springer-Boston |
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spelling | mit-1721.1/708522022-09-29T17:14:19Z Formation of delta ferrite in 9 wt.% Cr steel investigated by in-situ X-ray diffraction using synchrotron radiation Mayr, Peter Palmer, T. A. Elmer, J. W. Specht, E. D. Allen, Samuel Miller Massachusetts Institute of Technology. Department of Materials Science and Engineering Allen, Samuel Miller Allen, Samuel Miller Mayr, Peter In-situ X-ray diffraction (XRD) measurements using high energy synchrotron radiation were performed to monitor in real time the formation of delta ferrite in a martensitic 9 wt pct chromium steel under simulated weld thermal cycles. Volume fractions of martensite, austenite, and delta ferrite were measured as a function of temperature at a 10 K/s heating rate to 1573 K (1300 °C) and subsequent cooling. At the peak temperature, the delta ferrite concentration rose to 19 pct, of which 17 pct transformed back to austenite on subsequent cooling. Max Kade Foundation, Inc. Austrian Academy of Sciences United States. Dept. of Energy (Division of Materials Sciences and Engineering, Office of Science, and Office of Basic Energy Sciences) 2012-05-16T20:28:02Z 2012-05-16T20:28:02Z 2010-10 Article http://purl.org/eprint/type/JournalArticle 1073-5623 1543-1940 http://hdl.handle.net/1721.1/70852 Mayr, P. et al. “Formation of Delta Ferrite in 9 Wt Pct Cr Steel Investigated by In-Situ X-Ray Diffraction Using Synchrotron Radiation.” Metallurgical and Materials Transactions A 41.10 (2010): 2462–2465. Web. https://orcid.org/0000-0002-6082-332X en_US http://dx.doi.org/10.1007/s11661-010-0371-7 Metallurgical and Materials Transactions A Creative Commons Attribution-Noncommercial-Share Alike 3.0 http://creativecommons.org/licenses/by-nc-sa/3.0/ application/pdf Springer-Boston Prof. Allen via Angie Locknar |
spellingShingle | Mayr, Peter Palmer, T. A. Elmer, J. W. Specht, E. D. Allen, Samuel Miller Formation of delta ferrite in 9 wt.% Cr steel investigated by in-situ X-ray diffraction using synchrotron radiation |
title | Formation of delta ferrite in 9 wt.% Cr steel investigated by in-situ X-ray diffraction using synchrotron radiation |
title_full | Formation of delta ferrite in 9 wt.% Cr steel investigated by in-situ X-ray diffraction using synchrotron radiation |
title_fullStr | Formation of delta ferrite in 9 wt.% Cr steel investigated by in-situ X-ray diffraction using synchrotron radiation |
title_full_unstemmed | Formation of delta ferrite in 9 wt.% Cr steel investigated by in-situ X-ray diffraction using synchrotron radiation |
title_short | Formation of delta ferrite in 9 wt.% Cr steel investigated by in-situ X-ray diffraction using synchrotron radiation |
title_sort | formation of delta ferrite in 9 wt cr steel investigated by in situ x ray diffraction using synchrotron radiation |
url | http://hdl.handle.net/1721.1/70852 https://orcid.org/0000-0002-6082-332X |
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