Rapid 3D MAS NMR Spectroscopy at Critical Sensitivity
Sensitive SIFTing: Multidimensional non-uniform sampling (NUS) NMR spectroscopy is extended to the severely sensitivity-limited regime typical of MAS NMR of biomacromolecules by the use of spectroscopy by the integration of frequency and time domain information (SIFT). A three-dimensional MAS NMR ex...
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| Other Authors: | |
| Format: | Article |
| Language: | en_US |
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Wiley-Blackwell Pubishers
2012
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| Online Access: | http://hdl.handle.net/1721.1/74584 https://orcid.org/0000-0002-3349-6212 https://orcid.org/0000-0003-1589-832X |
| _version_ | 1826193580594561024 |
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| author | Matsuki, Yoh Eddy, Matthew Thomas Griffin, Robert Guy Herzfeld, Judith |
| author2 | Massachusetts Institute of Technology. Department of Chemistry |
| author_facet | Massachusetts Institute of Technology. Department of Chemistry Matsuki, Yoh Eddy, Matthew Thomas Griffin, Robert Guy Herzfeld, Judith |
| author_sort | Matsuki, Yoh |
| collection | MIT |
| description | Sensitive SIFTing: Multidimensional non-uniform sampling (NUS) NMR spectroscopy is extended to the severely sensitivity-limited regime typical of MAS NMR of biomacromolecules by the use of spectroscopy by the integration of frequency and time domain information (SIFT). A three-dimensional MAS NMR experiment is expedited (here 3.4-fold) without losing sensitivity or resolution. |
| first_indexed | 2024-09-23T09:41:22Z |
| format | Article |
| id | mit-1721.1/74584 |
| institution | Massachusetts Institute of Technology |
| language | en_US |
| last_indexed | 2024-09-23T09:41:22Z |
| publishDate | 2012 |
| publisher | Wiley-Blackwell Pubishers |
| record_format | dspace |
| spelling | mit-1721.1/745842022-09-26T13:06:38Z Rapid 3D MAS NMR Spectroscopy at Critical Sensitivity Rapid Three-Dimensional MAS NMR Spectroscopy at Critical Sensitivity Matsuki, Yoh Eddy, Matthew Thomas Griffin, Robert Guy Herzfeld, Judith Massachusetts Institute of Technology. Department of Chemistry Francis Bitter Magnet Laboratory (Massachusetts Institute of Technology) Griffin, Robert Guy Griffin, Robert Guy Eddy, Matthew Thomas Matsuki, Yoh Sensitive SIFTing: Multidimensional non-uniform sampling (NUS) NMR spectroscopy is extended to the severely sensitivity-limited regime typical of MAS NMR of biomacromolecules by the use of spectroscopy by the integration of frequency and time domain information (SIFT). A three-dimensional MAS NMR experiment is expedited (here 3.4-fold) without losing sensitivity or resolution. National Institutes of Health (U.S.) (NIH grant EB001035) National Institutes of Health (U.S.) (NIH grant EB003151) National Institutes of Health (U.S.) (NIH grant EB002026) Naito Foundation 2012-11-06T22:44:28Z 2012-11-06T22:44:28Z 2010-10 Article http://purl.org/eprint/type/JournalArticle 0570-0833 1521-3773 http://hdl.handle.net/1721.1/74584 Matsuki, Yoh et al. “Rapid Three-Dimensional MAS NMR Spectroscopy at Critical Sensitivity.” Angewandte Chemie International Edition 49.48 (2010): 9215–9218. Web. https://orcid.org/0000-0002-3349-6212 https://orcid.org/0000-0003-1589-832X en_US http://dx.doi.org/10.1002/anie.201003329 Angewandte Chemie International Edition Creative Commons Attribution-Noncommercial-Share Alike 3.0 http://creativecommons.org/licenses/by-nc-sa/3.0/ application/pdf Wiley-Blackwell Pubishers Prof. Griffin via Erja Kajosalo |
| spellingShingle | Matsuki, Yoh Eddy, Matthew Thomas Griffin, Robert Guy Herzfeld, Judith Rapid 3D MAS NMR Spectroscopy at Critical Sensitivity |
| title | Rapid 3D MAS NMR Spectroscopy at Critical Sensitivity |
| title_full | Rapid 3D MAS NMR Spectroscopy at Critical Sensitivity |
| title_fullStr | Rapid 3D MAS NMR Spectroscopy at Critical Sensitivity |
| title_full_unstemmed | Rapid 3D MAS NMR Spectroscopy at Critical Sensitivity |
| title_short | Rapid 3D MAS NMR Spectroscopy at Critical Sensitivity |
| title_sort | rapid 3d mas nmr spectroscopy at critical sensitivity |
| url | http://hdl.handle.net/1721.1/74584 https://orcid.org/0000-0002-3349-6212 https://orcid.org/0000-0003-1589-832X |
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