Cryogenic sample exchange NMR probe for magic angle spinning dynamic nuclear polarization

Cryogenic sample exchange NMR probe for magic angle spinning dynamic nuclear polarization

We describe a cryogenic sample exchange system that dramatically improves the efficiency of magic angle spinning (MAS) dynamic nuclear polarization (DNP) experiments by reducing the time required to change samples and by improving long-term instrument stability. Changing samples in conventional cryo...

Full description

Bibliographic Details
Main Authors:	Barnes, Alexander, Mak-Jurkauskas, Melody L., Matsuki, Yoh, Bajaj, Vikram S., van der Wel, Patrick C.A., Sirigiri, Jagadishwar R., Temkin, Richard J., Lugtenburg, Johan, Herzfeld, Judith, DeRocher, Ronald C., Bryant, Jeffrey A., Griffin, Robert Guy
Other Authors:	Massachusetts Institute of Technology. Department of Chemistry
Format:	Article
Language:	en_US
Published:	Elsevier 2013
Online Access:	http://hdl.handle.net/1721.1/82050 https://orcid.org/0000-0003-1589-832X https://orcid.org/0000-0001-9813-0177

Similar Items

Resolution and Polarization Distribution in Cryogenic DNP/MAS Experiments
by: Barnes, Alexander, et al.
Published: (2012)

Functional and shunt states of bacteriorhodopsin resolved by 250 GHz dynamic nuclear polarization-enhanced solid-state NMR
by: Bajaj, Vikram S., et al.
Published: (2010)

Microwave field distribution in a magic angle spinning dynamic nuclear polarization NMR probe
by: Nanni, Emilio Alessandro, et al.
Published: (2015)

DNP Enhanced Frequency-Selective TEDOR Experiments in Bacteriorhodopsin
by: Bajaj, Vikram S., et al.
Published: (2012)

Rapid 3D MAS NMR Spectroscopy at Critical Sensitivity
by: Matsuki, Yoh, et al.
Published: (2012)

A 140 GHz pulsed EPR/212 MHz NMR spectrometer for DNP studies
by: Smith, Albert A., et al.
Published: (2015)

Structural Characterization of GNNQQNY Amyloid Fibrils by Magic Angle Spinning NMR
by: Griffin, Robert Guy, et al.
Published: (2012)

Optimization of THz Wave Coupling into Samples in DNP/NMR Spectroscopy
by: Barnes, Alexander, et al.
Published: (2012)

Selectively dispersed isotope labeling for protein structure determination by magic angle spinning NMR
by: Eddy, Matthew Thomas, et al.
Published: (2015)

Peptide and Protein Dynamics and Low-Temperature/DNP Magic Angle Spinning NMR
by: Daviso, Eugenio, et al.
Published: (2018)

Accurate Determination of Interstrand Distances and Alignment in Amyloid Fibrils by Magic Angle Spinning NMR
by: Bajaj, Vikram S., et al.
Published: (2012)

A Novel Wideband Gyrotron Traveling Wave Amplifier
by: Sirigiri, Jagadishwar
Published: (2015)

A novel wideband gyrotron travelling wave amplifier
by: Sirigiri, Jagadishwar R. (Jagadishwar Rao), 1973-
Published: (2014)

Design of an overmoded W-band TWT
by: Comfoltey, E. Nicholas, et al.
Published: (2010)

Demonstration of a 140-GHz 1-kW Confocal Gyro-Traveling-Wave Amplifier
by: Temkin, Richard J., et al.
Published: (2010)

THz Dynamic Nuclear Polarization NMR
by: Nanni, Emilio Alessandro, et al.
Published: (2012)

Cryogenic-compatible spherical rotors and stators for magic angle spinning dynamic nuclear polarization
by: L. E. Price, et al.
Published: (2023-09-01)

Continuously Tunable 250 GHz Gyrotron with a Double Disk Window for DNP-NMR Spectroscopy
by: Ni, Qing Zhe, et al.
Published: (2015)

Continuous-wave operation of a frequency-tunable 460-GHz second-harmonic gyrotron for enhanced nuclear magnetic resonance
by: Torrezan de Sousa, Antonio Carlos, et al.
Published: (2011)

THE NMR OF SB-116G CRYOGENICALLY ORIENTED ONLINE IN IRON
by: Green, V, et al.
Published: (1986)

Solid-Cryogen Cooling Technique for Superconducting Magnets of NMR and MRI
by: Iwasa, Yukikazu, et al.
Published: (2014)

Deterministic schedules for robust and reproducible non-uniform sampling in multidimensional NMR
by: Ruben, David, et al.
Published: (2015)

Active real-time imaging system employed with a CW 460-GHz gyrotron and a pyroelectric array camera
by: Han, Seong-Tae, et al.
Published: (2010)

High Resolution Structural Characterization of Aβ₄₂ Amyloid Fibrils by Magic Angle Spinning NMR
by: Frohm, Birgitta, et al.
Published: (2017)

Layer-by-layer assembly in confined geometries
by: DeRocher, Jonathan P
Published: (2012)

[superscript 15]N-[superscript 15]N Proton Assisted Recoupling in Magic Angle Spinning NMR
by: Lewandowski, Jozef R., et al.
Published: (2013)

Characterization of zeolite catalysts by magic-angle spinning nmr spectroscopy /
by: Halimaton Hamdan, 1956-, et al.

Dynamic nuclear polarization in biomolecular solid state NMR : methods and applications in peptides and membrane proteins
by: Bajaj, Vikram Singh
Published: (2008)

Solid-State NMR Characterization of Gas Vesicle Structure
by: Sivertsen, Astrid C., et al.
Published: (2015)

Amplification of Picosecond Pulses in a 140-GHz Gyrotron-Traveling Wave Tube
by: Temkin, Richard J., et al.
Published: (2011)

An overmoded 140 GHz, 1 kW quasioptical gyro-TWT with an internal mode converter
by: Kim, Hae Jin, et al.
Published: (2010)

High field DNP and cryogenic MAS NMR : novel instrumentation and applications
by: Markhasin, Evgeny
Published: (2014)

Rapid Proton-Detected NMR Assignment for Proteins with Fast Magic Angle Spinning
by: Barbet-Massin, Emeline, et al.
Published: (2017)

Magic-angle spinning NMR structure of Opa60 in lipid bilayers
by: Marcel C. Forster, et al.
Published: (2024-06-01)

High-Resolution Magic-Angle-Spinning NMR in Revealing Hepatoblastoma Hallmarks
by: Ljubica Tasic, et al.
Published: (2022-12-01)

Advances in Instrumentation for Dynamic Nuclear Polarization & Magic-Angle Spinning NMR
by: Banks, Daniel P.
Published: (2022)

Quantitative Cross Polarization Magic-Angle Spinning NMR Spectroscopy in Solids
by: LIANG Li-xin, et al.
Published: (2020-03-01)

Magic Angle Spinning NMR Analysis of β[subscript 2]-Microglobulin Amyloid Fibrils in Two Distinct Morphologies
by: Debelouchina, Galia Tzvetanova, et al.
Published: (2012)

Observation and Study of Low-Frequency Oscillations in a 1.5-MW 110-GHz Gyrotron
by: Cerfon, Antoine J., et al.
Published: (2010)

Magic-Angle-Spinning NMR of the Drug Resistant S31N M2 Proton Transporter from Influenza A
by: Chou, James J., et al.
Published: (2013)