A facile microwave-assisted “one-pot” synthesis of piperazino pyrimidinyl acetamides, a class of hybrid bis heterocycles and their structural elucidation Using NMR spectral techniques
An array of novel piperazino pyrimidinyl acetamides, a class of hybrid bis heterocycles are synthesized in “one-pot” by microwave irradiation method catalyzed by heterogeneous NaHSO4.SiO2 catalyst in dry media and are characterized by melting point, elemental analysis, MS, FT-IR, one-dimensional NMR...
Main Authors: | , , , |
---|---|
Other Authors: | |
Format: | Journal Article |
Language: | English |
Published: |
2013
|
Subjects: | |
Online Access: | https://hdl.handle.net/10356/103436 http://hdl.handle.net/10220/16932 |
_version_ | 1811695016186216448 |
---|---|
author | Ang, How Ghee Ng, Siu-Choon Kanagarajan, V. Gopalakrishnan, M. |
author2 | School of Chemical and Biomedical Engineering |
author_facet | School of Chemical and Biomedical Engineering Ang, How Ghee Ng, Siu-Choon Kanagarajan, V. Gopalakrishnan, M. |
author_sort | Ang, How Ghee |
collection | NTU |
description | An array of novel piperazino pyrimidinyl acetamides, a class of hybrid bis heterocycles are synthesized in “one-pot” by microwave irradiation method catalyzed by heterogeneous NaHSO4.SiO2 catalyst in dry media and are characterized by melting point, elemental analysis, MS, FT-IR, one-dimensional NMR (1H and 13C) and two-dimensional 1H-1H COSY and 1H-13C HSQC spectral data. |
first_indexed | 2024-10-01T07:16:46Z |
format | Journal Article |
id | ntu-10356/103436 |
institution | Nanyang Technological University |
language | English |
last_indexed | 2024-10-01T07:16:46Z |
publishDate | 2013 |
record_format | dspace |
spelling | ntu-10356/1034362020-03-07T11:40:23Z A facile microwave-assisted “one-pot” synthesis of piperazino pyrimidinyl acetamides, a class of hybrid bis heterocycles and their structural elucidation Using NMR spectral techniques Ang, How Ghee Ng, Siu-Choon Kanagarajan, V. Gopalakrishnan, M. School of Chemical and Biomedical Engineering Energetics Research Institute DRNTU::Engineering::Chemical engineering::Biochemical engineering An array of novel piperazino pyrimidinyl acetamides, a class of hybrid bis heterocycles are synthesized in “one-pot” by microwave irradiation method catalyzed by heterogeneous NaHSO4.SiO2 catalyst in dry media and are characterized by melting point, elemental analysis, MS, FT-IR, one-dimensional NMR (1H and 13C) and two-dimensional 1H-1H COSY and 1H-13C HSQC spectral data. 2013-10-25T08:12:20Z 2019-12-06T21:12:39Z 2013-10-25T08:12:20Z 2019-12-06T21:12:39Z 2013 2013 Journal Article Kanagarajan, V., Ang, H. G., Ng, S. C.,& Gopalakrishnan, M. (2013). A Facile microwave-assisted “one-pot” synthesis of piperazino pyrimidinyl acetamides, a class of hybrid bis heterocycles and their structural elucidation using NMR spectral techniques. Journal of heterocyclic chemistry, 50(2), 396-402. 1943-5193 https://hdl.handle.net/10356/103436 http://hdl.handle.net/10220/16932 10.1002/jhet.1046 en Journal of heterocyclic chemistry |
spellingShingle | DRNTU::Engineering::Chemical engineering::Biochemical engineering Ang, How Ghee Ng, Siu-Choon Kanagarajan, V. Gopalakrishnan, M. A facile microwave-assisted “one-pot” synthesis of piperazino pyrimidinyl acetamides, a class of hybrid bis heterocycles and their structural elucidation Using NMR spectral techniques |
title | A facile microwave-assisted “one-pot” synthesis of piperazino pyrimidinyl acetamides, a class of hybrid bis heterocycles and their structural elucidation Using NMR spectral techniques |
title_full | A facile microwave-assisted “one-pot” synthesis of piperazino pyrimidinyl acetamides, a class of hybrid bis heterocycles and their structural elucidation Using NMR spectral techniques |
title_fullStr | A facile microwave-assisted “one-pot” synthesis of piperazino pyrimidinyl acetamides, a class of hybrid bis heterocycles and their structural elucidation Using NMR spectral techniques |
title_full_unstemmed | A facile microwave-assisted “one-pot” synthesis of piperazino pyrimidinyl acetamides, a class of hybrid bis heterocycles and their structural elucidation Using NMR spectral techniques |
title_short | A facile microwave-assisted “one-pot” synthesis of piperazino pyrimidinyl acetamides, a class of hybrid bis heterocycles and their structural elucidation Using NMR spectral techniques |
title_sort | facile microwave assisted one pot synthesis of piperazino pyrimidinyl acetamides a class of hybrid bis heterocycles and their structural elucidation using nmr spectral techniques |
topic | DRNTU::Engineering::Chemical engineering::Biochemical engineering |
url | https://hdl.handle.net/10356/103436 http://hdl.handle.net/10220/16932 |
work_keys_str_mv | AT anghowghee afacilemicrowaveassistedonepotsynthesisofpiperazinopyrimidinylacetamidesaclassofhybridbisheterocyclesandtheirstructuralelucidationusingnmrspectraltechniques AT ngsiuchoon afacilemicrowaveassistedonepotsynthesisofpiperazinopyrimidinylacetamidesaclassofhybridbisheterocyclesandtheirstructuralelucidationusingnmrspectraltechniques AT kanagarajanv afacilemicrowaveassistedonepotsynthesisofpiperazinopyrimidinylacetamidesaclassofhybridbisheterocyclesandtheirstructuralelucidationusingnmrspectraltechniques AT gopalakrishnanm afacilemicrowaveassistedonepotsynthesisofpiperazinopyrimidinylacetamidesaclassofhybridbisheterocyclesandtheirstructuralelucidationusingnmrspectraltechniques AT anghowghee facilemicrowaveassistedonepotsynthesisofpiperazinopyrimidinylacetamidesaclassofhybridbisheterocyclesandtheirstructuralelucidationusingnmrspectraltechniques AT ngsiuchoon facilemicrowaveassistedonepotsynthesisofpiperazinopyrimidinylacetamidesaclassofhybridbisheterocyclesandtheirstructuralelucidationusingnmrspectraltechniques AT kanagarajanv facilemicrowaveassistedonepotsynthesisofpiperazinopyrimidinylacetamidesaclassofhybridbisheterocyclesandtheirstructuralelucidationusingnmrspectraltechniques AT gopalakrishnanm facilemicrowaveassistedonepotsynthesisofpiperazinopyrimidinylacetamidesaclassofhybridbisheterocyclesandtheirstructuralelucidationusingnmrspectraltechniques |